Chemical Engineering Commons^™

Analysis And Study Of The Content Of Chloride Salts In Oil, Natalia Evgenievna Sheina, Muborak Akramovna Mirshomilova

Technical science and innovation

The article addresses the critical issue of crude oil quality control, specifically focusing on the determination of chloride salts (sodium, calcium, and magnesium), which exert a destructive impact on processing equipment. The paper provides a detailed analysis of the adverse effects of salts, which lead to severe equipment corrosion, scaling, and a reduced yield of valuable oil fractions. The chemical principles and specific applications of two standardized methods for analyzing aqueous extracts according to GOST 21534-2021 and ASTM D3230 are described: indicator (argentometric and mercurimetric) and potentiometric titration. The experimental section presents the results of a comparative analysis of crude …

Determination Of The Content Of Water-Soluble Vitamins In The Composition Of Beet Beetroot Composition, Jasur Esirgapovich Safarov, Shakhnoza Abduvaxitovna Sultanova, Muhammad Rasul Oglu Najafli, Doston Ishmuhammat Ugli Samandarov

Chemical Technology, Control and Management

The aim of this study was to determine the content of water-soluble vitamins in various parts of beetroot (pulp, leaves and stems) that had been subjected to various drying methods in a bid to explore the effect of physical processes, i.e., the application of ultrasound, on micronutrient preservation. The experiments were performed at the Department of Service Technologies of Tashkent State Technical University, and chromatographic analysis was performed in the Institute of Bioorganic Chemistry of the Academy of Sciences of the Republic of Uzbekistan. Chromatography was performed on Agilent-1200 chromatograph with Exlipse XDB C18 column and diode array detector using …

Modeling Of A Two-Stage Extractive Distillation Process For The Separation Of 1,3-Butadiene From Pyrolysis-Derived C₄ Fractions, Muxriddin Xudoyor Og‘Li Ibodullayev, Jonibek Farxod O‘G‘Li Norqulov, Olim Rustamovich Abduraxmonov, Orifjon Sharipovich Kodirov

Chemical Technology, Control and Management

The separation of 1,3-butadiene from pyrolysis-derived C₄ fractions represents a challenging task due to the multicomponent nature of the feed and the close boiling points of accompanying hydrocarbons. In this study, a two-stage extractive distillation process was investigated using an acetonitrile–water solvent system to address these challenges. A semi-industrial experimental unit consisting of two extractive distillation columns connected in series was developed and analyzed, and the process configuration was supported by Aspen Plus simulation. The feedstock composition was characterized in detail, revealing that 1,3-butadiene constitutes approximately 40 wt.% of the C₄ fraction, accompanied by significant amounts of propylene, butanes, butanes, …

Methods For Treating Wastewater Generated During The Production Of Basalt Fiber Using Modified Bentonite Clay, Abdurasul O'Ktamovich Husenov, Baxtiyor Toxtayevich Sabirov, Diyor Asadullayevich Xadjibayev

Chemical Technology, Control and Management

This scientific article notes that in technological processes, wastewater is contaminated with various organic and mineral substances, including poisonous and toxic substances. Sources of environmental pollution include organic and inorganic substances formed during the production of basalt fiber. In this research work, the task is set to purify wastewater formed during the production of basalt fiber from organic substances. Bentonite clay is a very good natural sorbent and has the ability to purify some cations. When conducting laboratory experiments, bentonite clays from the "Azkamar" and "Navbahor" deposits were selected to purify wastewater formed during the production of basalt fiber from …

Mathematical Models Of Magnetoelastic Acceleration Transducers Developed Based On The Theory Of Lumped Parameter Circuits, Amirov Fayzullayevich Sulton, Kamila Kamilovna Jurayeva, Shovkat Dilshodovich Turayev

Chemical Technology, Control and Management

In this article, based on the theory of lumped-parameter circuits, algebraic and differential equations describing the mechanical, electrical, and magnetic circuits of new magnetoelastic acceleration transducers, their analytical solutions, as well as mathematical models establishing the relationship between the electromotive forces at the outputs of the transducers and acceleration, which is the input quantity of the transducer, have been developed. Analysis of these mathematical models and the graphs constructed on their basis shows that under the influence of acceleration applied to the transducers, with an increase in the mechanical stresses arising in the magnetic circuit of the transducer, a redistribution …

Optimal Procedure For Measuring The Parameters Of Optical Signals Considering Noise, Yuriy Gennadyevich Shipulin, Azimjon Mamadaliyevich Xusanov

Chemical Technology, Control and Management

It has been shown that to achieve the required level of measurement accuracy and reliability, it is necessary to transition from quality control of finished products to quality management based on cost-effective methods during the stages when product properties are formed. It is shown that the complexity of measuring optical signal parameters during analysis or synthesis requires them to be considered as part of a general information processing system. Based on the nonlinear filtration method, an optimal procedure for measuring a variable position in time against a background of spatial noise was obtained. Structural diagrams of optimal measuring instruments for …

Development And Uncertainty Assessment Of Secondary Method For Ph Measurement In Physicochemical Measurements, Sarvar Rakhmatullaev, Dostonbek Xujakulov, Mohinur Nigmatova

Chemical Technology, Control and Management

In physicochemical measurements across various industries, laboratory analyses commonly require the determination of pH as an indicator of hydrogen ion activity in aqueous solutions. Ensuring the accuracy and reliability of these measurements, obtaining precise readings from pH measuring instruments, and maintaining overall measurement quality represent critical challenges in guaranteeing the safety of both products and processes. This requires constant monitoring, accuracy assessment, calibration, metrological verification, and control of measuring instruments. In this case, it should be carried out not with solutions prepared in any laboratory, but with certified reference materials (СRM) with appropriate regulatory framework, ensuring metrological observation. …

Robust-Adaptive Estimation Of Unmeasurable States And External Disturbances Of A Dynamic Object Based On An Augmented Kalman Filter, Husan Igamberdiev, Uktam Farkhodovich Mamirov, Lu Liu, Bohong Wang, Bunyod Buronov

Chemical Technology, Control and Management

The paper addresses the problem of joint estimation of the directly unmeasurable states of a dynamic object and of external disturbances when information is available only on the control inputs and on the measured output signals. To solve this problem, a robust-adaptive algorithm based on an augmented Kalman filter is proposed, in which the external disturbance is included in the extended state vector. Two operating modes of the algorithm are considered. For slowly varying disturbances, a random-walk model with a constant process-noise covariance is used, whereas for rapidly varying inputs a signal adaptation  driven by the normalized innovation is proposed. …

Fast Algorithms For Combined Synthesis Of Dynamic Object Control Systems, Isomiddin Khakimovich Siddikov, Gulchexra Alimova

Chemical Technology, Control and Management

The paper considers the issues of combined synthesis of a control system for a nonlinear dynamic object. The combined synthesis algorithms are based on the hybrid application of the theory of ordinary differential equations in the Cauchy form and the theory of automatic control. In this case, the dynamics of the control system are described in the input-output representation and by state-space equations. Algorithms for solving stabilization problems, finite control, and the inverse dynamics problem are presented in explicit form. These algorithms are based on the concept of reducibility of a general Cauchy-form system to the block-canonical Frobenius form. The …

Nonlinear System Identification Based On Fuzzy Radial Basis Neural Network With Multi-Connected Weight Connections, Kabul Khudaybergenov

Chemical Technology, Control and Management

This paper builds on our earlier radial basis function network with multiple connections (RBFMC) by placing it within a fuzzy inference framework for nonlinear system identification. The idea is inspired by the diversity of neurotransmitters found in biological neurons: instead of a single hidden-to-output weight, RBFMC gives each hidden unit a multi-dimensional connection whose components act as independent filters. Once fuzzy logic is added, each hidden neuron becomes a fuzzy rule, and its antecedent is built from several Gaussian membership functions, one per connection. The resulting Fuzzy RBFMC produces an interpretable, multi-filter description of local regions of the input space …

Performance Evaluation Of Controllers Using Fuzzy Delphi And Ahp Techniques, Kamala. R. Aliyeva, Nihad Mehdiyev, Shamil Mehdi

Chemical Technology, Control and Management

This study introduces an enhanced decision-support framework that integrates the Fuzzy Delphi method with the Analytic Hierarchy Process (AHP) to improve controller tuning and performance evaluation in uncertain environments. Traditional tuning techniques typically depend on crisp expert judgments and deterministic performance indices; however, industrial control systems are characterized by nonlinear behaviors, uncertain parameter variations, and subjective expert evaluations that are often vague or inconsistent. The Fuzzy Delphi procedure is applied to systematically gather, filter, and consolidate expert insights, enabling a refined set of performance criteria such as stability margins, robustness to disturbances, settling time, overshoot, control effort, and energy consumption …

Documentation And Project Change Management System – Honeywell Trace, Farukh Adilov, N.R Yusupbekov, Maksim Fedorovich Astafurov, Kamola Rustamovna Abdullayeva

Chemical Technology, Control and Management

The article examines modern approaches to organizing documentation and managing changes in industrial automation projects using the Honeywell Trace software platform. The evolution of documentation tools from the Documentation Tool utility within the TDC 2000/3000 system to modern intelligent solutions is described. The architecture, functional capabilities, and supported interfaces of Honeywell Trace are analyzed. Particular attention is paid to automated configuration change tracking, comprehensive search by process tags, and the detection of potential errors. The possibilities of integrating the system with industrial process control systems, controllers, auxiliary systems, and industrial communication protocols are considered. The application of Honeywell Trace during …

Neural Network Technologies In The Automatical Control Systems Of Absorption Process For Pureficating Natural Gas, Abdishukurov Maqsudovich Shavkat Mr, Xuecheng Li Li Xuecheng Mr

Technical science and innovation

Analysis of methods and algorithms for synthesizing adaptive control systems for technological processes based on the neural network approach is carried out in this search. The stages of mathematical modeling of complex technological processes using neural network technology were considered. Additionally, an algorithm for solving the interpolation and extrapolation problem that arises in the training process a neural network to control system was proposed. At the final stage of this article, algorithms based on neural network technology are synthesized for the control system for the parameters of the technological process of natural gas purification by absorption

Increasing The Prediction Accuracy Of Plant Oil Production Processes Through Adjusting The Parameters Of Machine Learning Models, Umidjon Ruziev, M.K. Shodiev, A.T. Rajabov

Chemical Technology, Control and Management

Vegetable oil production is characterized by high variability in output indicators due to nonlinear interactions between raw material parameters, equipment modes, and heat and mass transfer conditions. Existing approaches to applying machine learning in this field, as a rule, do not account for the impact of hyperparameter adjustments on forecasting quality across specific technological stages. The article presents a systematic methodology for adjusting model parameters (Ridge regression, SVR, GBM, LSTM) applied to three key tasks: predicting residual oil content in oil cake, color index during bleaching, and free fatty acid content during deodorization. In a set of 1000 observations, including …

Intelligent Manufacturing Of Edible Oil: From Smart Sensing To Big Data Platform, Ru Jiang, Nadirbek Yusupbekov

Chemical Technology, Control and Management

With the rapid advancement of Industry 4.0 technologies, intelligent manufacturing and big data platforms are profoundly transforming the production models of the traditional edible oil industry. The edible oil production process involves multiple complex unit operations such as refining, decolorization, and deodorization, which impose high requirements on process control and product quality monitoring. This paper presents a systematic review of key technological advances in the field of intelligent manufacturing of edible oil, establishing a comprehensive technical framework encompassing four dimensions: smart sensing, artificial intelligence applications, IoT communication, and big data platforms. The review begins by analyzing the global background and …

Reliability Analysis Of Separator Control Systems, D.P. Muxitdinov, O.U. Sattarov, M.Sh. Nematov

Chemical Technology, Control and Management

This article aims to enhance the reliability, efficiency, and diagnostic capabilities of gas-liquid separators operating in hazardous technological processes. In the study, the separator is considered as a critical functional unit of an industrial system and is analyzed through structural and functional decomposition. The main operating parameters of the separator, including pressure drop (ΔP), separation efficiency and operational state are described on the basis of a mathematical model. In addition, a state model is developed for normal operation, foaming, liquid droplet carryover with the gas flow, and failure conditions. Emphasis is placed on diagnostic and monitoring issues, …

Data-Driven Neuro-Fuzzy Modeling And Rule Optimization For Intelligent Prediction Of Bioreactor Dynamics, Kamala Najaf Mammadzada

Chemical Technology, Control and Management

Modeling wastewater bioreactors is a challenging problem in environmental engineering because the processes are constantly changing and the microorganisms do not behave in a linear or predictable way. This makes it difficult to predict and control the system behavior. This research investigates three artificial intelligence approaches for modeling wastewater bioreactors: the Mamdani Fuzzy Inference System (FIS), the Adaptive Neuro-Fuzzy Inference System (ANFIS), and clustering-based fuzzy models. These models help us predict what is happening in the bioreactors. For instance they help us predict how the amount of substances in the water is changing over time like dS₀/dt dSs/dt …

Optimization Of Renewable Energy-Based Alkaline Electrolysis Systems For Sustainable Hydrogen Production, Shokhrukhbek Kozimjon Ugli Bakhramov

Chemical Technology, Control and Management

This paper presents a comprehensive optimization study of hydrogen production systems through alkaline water electrolysis powered by photovoltaic energy sources, with a specific focus on Central Asian applications. The research systematically investigates critical operating parameters including KOH electrolyte concentration (25-30 wt%), temperature effects (25-80°C), current density optimization (100-500 mA/cm²), and electrode material performance using cost-effective 316L stainless steel. Experimental results demonstrate that optimized systems achieve solar-to-hydrogen efficiency of 13-15%, with hydrogen production costs ranging from $2-8/kg depending on system scale. The study reveals that maximum performance occurs at 30 wt% KOH concentration, 60-80°C operating temperature, and 200-400 mA/cm² current density. …

Analysis Of Automatic Control Of The Channels And Ditches Cleaning Mechanism Based On Dynamic Indicators, Nasiba Siraj Amirbayova

Chemical Technology, Control and Management

The article deals with the automated design and experimental investigation of reinforced concrete irrigation channels and ditches, their interrelated channel-cleaning mechanisms, which are complex mechatronic systems integrating hydraulic, mechanical, and electronic components. A thorough methodology is suggested, hydrodynamic modeling, combining parametric analysis, and information-based design support to enhance channel concrete cover thickness, geometry, and cleaning system performance. Main structural parameters—involving channel depth, slope, bottom width, and concrete cover—are systematically defined and shown in matrix form to facilitate automated calculation and decision-making. Experimental prototypes and Solid Edge-based digital models are employed to verify the methodology, revealing vital interdependencies between structural parameters, …

Regular Synthesis Algorithms Of Control Devices In Nonlinear Control Systems, Husan Zakirovich Igamberdiyev, Iskandar Yusupovich Abdurakhmanov, Uktam Farkhodovich Mamirov

Chemical Technology, Control and Management

This paper examines the development of regularized algorithms for synthesizing control devices in control systems for polynomial objects, described by multidimensional Volterra functional series. The synthesis problem is solved using a two-stage procedure. In the first stage, the optimization problem is initially solved for an open-loop system. The second stage involves determining the parameters of the control device, i.e., its impulse response functions, by using the relationship between the characteristics of the open-loop and closed-loop systems. Regular algorithms are presented for finding the impulse response functions of the control device based on methods for regularizing the solution of operator equations …

Rdm Interval Arithmetic Based Weapon System Evaluation, Konul Imran Jabbarova Phd

Chemical Technology, Control and Management

For solving this issue, the paper considers a hierarchical multi-criteria decision-making problem, where the choice of a company that corresponds best to the criteria is required. Data used in this problem are presented in the form of intervals, which makes it possible to cope with uncertainty in the problem solution. Several companies working in missile production industry are chosen as alternatives for analysis. Evaluation of the selected alternatives is made based on five criteria clusters. More than twenty criteria are taken into account during evaluation.

Solving this problem is achieved with the help of the technique based on computation of …

Structural Decomposition-Based Control Synthesis For Multivariable Systems Using Oblique Projection Operators, Abdukaxxarov Inomjon Ilxom Ugli Mr, Oripjon Olimovich Zaripov, Jasur Usmonovich Sevinov

Chemical Technology, Control and Management

This paper proposes a novel approach to control synthesis for multivariable systems with algebraic constraints using oblique projection operators and their structural decomposition. The method transforms a standard control law into a structured form by decomposing the control input into constraint-satisfying and null-space components. A generalized oblique projector is constructed using a dual matrix, ensuring flexibility in shaping system properties. Furthermore, a recursive decomposition algorithm is developed, allowing the global projector to be represented as a sum of local operators corresponding to subsystem structures. The proposed framework enables modular control design, decoupling of interactions, and efficient implementation for large-scale systems. …

Using Ali-4 Z-Implication In Controller Design, Shamil Azer Ahmadov

Chemical Technology, Control and Management

One of the widely used theories in the information processing is Professor Zadeh's fuzzy logic theory. Fuzzy implications form the basis of this theory. When processing information using fuzzy implication, the chosen judgment method and the type of implication affect the result. Referring to the review of the relevant literature on fuzzy implications, it can be noted that there are still unresolved problems and issues. For example, fuzzy implications cannot be used in processing imperfect information or information based on probabilistic and fuzzy uncertainty. Existing fuzzy implications face limitations in practical applications. Fuzzy implications only take into account inaccuracy, but …

Conceptual Model For Protecting Personal Data By Depersonalization In Information Systems: Principles, Components, And Life Cycle, Zarina Ildarovna Azizova

Chemical Technology, Control and Management

This article presents a systematic approach to personal data protection through depersonalization in the context of regulatory pressure and growing cyber threats. It proposes a comprehensive conceptual model that formalizes the de-identification process as a manageable sequence of steps, from attribute classification and method selection to mandatory verification of the result. The article also provides a comparative analysis of existing depersonalization methods in terms of their applicability within the proposed model. The model serves as a basis for the development of specific algorithms, as demonstrated by the example of a data shuffling approach.

Analysis Of Soda Production Processes In Ammonia-Soda Production, Nadirbek Rustambekovich Yusupbekov Professor, Djalolitdin Paxritdinovich Mukhitdinov Professor, Fatima Faxritdinovna Iskhakova

Technical science and innovation

This paper provides a comprehensive analysis of the fundamental principles of the classical Solvay process, a key component in the industrial production of soda ash. It is noted that despite its widespread use and technological maturity, the process has a number of significant technological, energy, and environmental limitations associated with high raw material and energy consumption, the generation of significant industrial waste, and CO₂ emissions. The need to modernize the traditional production process to improve efficiency, resource conservation, and environmental sustainability is substantiated. The review systematically summarizes current approaches to process improvement, including modified versions of the Solvay process, the …

Mathematical Modelling And Optimisation Of The Reactor For The Esterification Process Of Safflower Oil With N-Butyl Alcohol, Sadritdin Makhamatdinovich Turabdjanov Academician, Hasan Sadriddin Ugli Fozilov, Ozoda Bakhronovna Axmedova, Sadriddin Fayzullayevich Fozilov

Technical science and innovation

This study addresses the mathematical modelling and optimisation of a reactor for the esterification of safflower oil with n-butyl alcohol. To improve process controllability and reduce the need for numerous pilot-scale trials, an ideal-mixing continuous stirred-tank reactor (CSTR) model was adopted. Incorporating reaction kinetics, the effect of contact time on the relative viscosity of the product mixture was analysed. The modelling results indicate that achieving an acceptable degree of feedstock conversion is difficult when a single ideal-mixing reactor is used. Therefore, a CSTR cascade was proposed, and the configuration with N = 2 reactors was selected as the most appropriate …

Relationships Between The Parameters Of The Vegetable Oil Refining Process And Energy Consumption, Umidjon Abdimajitovich Ruziev, Marufjon Kobuljonovich Shodiev

Technical science and innovation

Vegetable oil refining is a multi-stage thermochemical process that is closely related to energy consumption, process parameters, product quality, and food safety requirements. Despite the extensive scientific literature on oil quality and pollutant formation, the quantitative relationship between purification parameters and relative energy consumption has not been sufficiently studied. In this work, a systematic analysis and engineering synthesis were carried out based on existing studies. According to the analysis results, the deodorization process accounts for 52–56% of the total thermal energy consumption, with a relative value ranging from 160 to 380 kJ/kg, depending on the enterprise's capacity and heat utilization …

Algorithms Of Stable Adaptive Observation Of A Multidimensional Undefinite Object, Tursunova Sadoqat Abdusalom Qizi

Chemical Technology, Control and Management

This article presents an algorithm for simultaneously estimating the parameters and state coordinates of a multidimensional control object when some of its state variables are not directly measured. The inability to measure all state variables (coordinates) of an object is a well-known drawback of identification schemes. Such conditions require the construction of adaptive state observers. This work demonstrates that when identifying the parameters of a mathematical model for an uncertain multidimensional object, the asymptotic stability of the object and the convergence of its parameters to the model parameters are ensured, provided the input vector is sufficiently informative. The construction of …

Inductive Transducers For Measuring Vibrations, S.F. Amirov, A.Kh. Sulliev, A.A. Shoimkulov

Chemical Technology, Control and Management

A new design of an induction transducer has been developed for measuring linear and torsional vibrations in different directions with high sensitivity by constructing an inertial element consisting of four mutually perpendicular sectors and making the masses of two adjacent sectors different from the masses of the other two adjacent sectors. By constructing an inertial element in the form of a sector with two mutually diametric magnetic cores and different masses, and placing it between the horizontal and vertical axes, a design of an induction transducer has been developed that highly sensitively measures linear and torsional vibrations in different directions, …

Physical And Chemical Study Of Interaction In The Urea–Valine System For The Creation Of Modified Liquid Nitrogen Fertilizers, Suvonkul Erkhanovich Nurmonov, Saydullo Khamidovich Azimov

Chemical Technology, Control and Management

This study reports the results of a comprehensive physicochemical investigation of the urea–L-valine binary system, conducted to validate its potential as a modified base for liquid nitrogen fertilizers.

By utilizing the methods of isomolar series, visual-polythermal analysis, X-ray phase (XRD) and single-crystal X-ray diffraction (SC-XRD), synchronous thermal analysis (TGA/DTA), and FT-IR spectroscopy, it was determined that the interaction between components in both aqueous solutions and the solid phase results in the formation of molecular associates stabilized by hydrogen bonds, without the formation of new stoichiometric compounds.

The concentration and temperature limits of the system's stability were defined, revealing a reduction …