Structures and Materials Commons^™

Fused Filament Fabrication Additive Manufacturing Of 17-4 Ph Stainless Steel: Process–Structure–Property Relationships In Magnetic Materials, Maanav Patel

Theses and Dissertations

Additive manufacturing (AM) enables the fabrication of complex metallic components through layer-by-layer processing directly from digital models. Among AM techniques, material extrusion–based processes such as fused filament fabrication (FFF) provide an accessible method for producing metal parts using filament feedstocks composed of metal powders and polymer binders. When applied to precipitation-hardening stainless steels such as 17-4 PH, the processing route and heat treatments can influence the resulting microstructure and functional properties. This work investigates the magnetic behavior of 17-4 PH stainless steel fabricated using FFF and evaluates how heat treatment conditions influence measured magnetic properties. Samples were produced and analyzed …

Tensile Creep Of A Hybrid Polymer-Matrix/Ceramic-Matrix Composite At Elevated Temperature, Waleed S. Alshehri

Theses and Dissertations

Advanced aerospace systems require structural materials that can perform reliably in high-temperature environments for long durations. The performance of standard polymer matrix composites (PMCs) in these conditions is often limited by their susceptibility to time-dependent deformation, such as creep. The objective of this research is to characterize the high-temperature creep behavior of a novel unitized material system comprising a polymer matrix composite (PMC) and a ceramic matrix composite (CMC) co-cured together. The PMC part consists of the polyimide matrix reinforced with laminated carbon fibers woven in an eight harness satin weave (8HSW). The CMC part consists of a zirconia-based ceramic …

Experimental And Theoretical Fracture Analysis Of Additively Manufactured Orthotropic V-Notches, Venkata Siva Sainath Bavapuram

Theses and Dissertations

This study presents a comprehensive investigation into the fracture behavior of additively manufactured orthotropic V-notched components made of Acrylonitrile Butadiene Styrene (ABS) material. The research integrates both theoretical and finite element approaches to evaluate stress intensity factors (SIFs) in Modes-I and II, which are fundamental in characterizing stress field distributions around notches under applied loading conditions. Unlike isotropic materials, where stress fields depend only on geometry of the component, the anisotropic nature of 3D-printed ABS introduces a dependency on material properties that necessitate different approaches to include anisotropy of the material.

Tensile specimens are 3D-printed with specific material orientations to …

Experimental And Theoretical Fracture Analysis Of Rift Manufactured Carbon Fiber-Vinyl Ester Lamina, Daniel Joseph Longo

Theses and Dissertations

This thesis investigates the fracture behavior of unidirectional carbon fiber-vinyl ester (CFVE) laminates manufactured using the Resin Infusion with Flexible Tooling (RIFT) process, a cost-effective alternative to autoclave-based fabrication methods. Composite materials like CFVE are increasingly adopted in high-performance applications due to their high strength-to-weight ratio and corrosion resistance; however, their anisotropic nature presents challenges in predicting crack initiation and propagation. To address this, a comprehensive approach combining experimental testing, finite element modeling (FEM), and classical fracture mechanics was employed. Orthotropic mechanical properties were first determined through tensile and shear tests, providing critical properties for FEM simulations. A series of …

Mixed-Mode Fracture Analysis Of Additively Manufactured Periodic Orthotropic Functionally Graded Microcellular Materials, Behnam Shahbazian

Theses and Dissertations

The quest for safety, efficiency, and innovation in aerospace engineering demands a relentless focus on understanding how materials and structures behave under extreme and complicated loading conditions. Among the many challenges faced by engineers in this field, predicting and preventing structural failure stands out as both a fundamental necessity and a complex problem. Fracture mechanics, the science of how materials fail under stress, is a cornerstone of this effort. Whether it is the fuselage of an aircraft enduring cyclic loading or the lightweight components of a spacecraft resisting impact, the ability to accurately predict fracture behavior directly influences the reliability …

Mechanical Response Of Triply Periodic Minimal Surface Gyroid Structures Under Combined Loading, Jay B. Patel

Theses and Dissertations

This work explored combined tensile and torsional loads applied to additively manufactured Inconel 718 specimens employing Triply Periodic Minimal Surface (TPMS) structures. The gyroid TPMS unit cell was selected with two variations of cylindrical cell maps, a rectangular cell map, and a spherical cell map. All four variants were tested in an axial-torsion test frame at room temperature using equal parts of vertical and angular displacement control until failure. The combined loading in these tests utilized tension and torsion. The data from the tests were compared to finite element analysis (FEA) models to visualize when yielding was predicted. Finally, the …

Computational Modeling Of Single Shear Bolted Joints In Hybrid Composite Laminates With And Without Film Adhesive, Cameron S. Mcmahan

Theses and Dissertations

This research explores the effectiveness of predicting composite failure subject to quasi-static loading conditions using computational methods. FEA models were created using Abaqus and were employed to predict composite yield and initial failure behavior. Boundary conditions are generated to replicate the loading scenario seen in the experimental tests. Computationally predicted structural response of the composite range in accuracy from a 2% difference compared to experimental values to a maximum of 63%.

Influence Of Environmental Barrier Coatings On The Overall Effectiveness Of A Film Cooled Ceramic Matrix Composite Plate, Shane P. Lindsay

Theses and Dissertations

Silicon carbide ceramic matrix composites, a promising new potential upgrade over the conventional metals currently used for jet engine turbine blades, have a propensity to oxidize in a combustion environment. Engine manufacturers often apply environmental barrier coatings to prevent the composites from oxidizing. What is unclear, however, is how environmental barrier coatings effect underlying composite temperatures. This research examined the coatings’ effects by first characterizing the influence of environmental barrier coatings on the underlying temperature of a protected ceramic, then evaluating the significance of lateral conduction for cooling a coated ceramic, and finally comparing cooling results for coated and uncoated …

Influence Of Periodic Stitching On The In-Plane And Out-Of-Plane Mechanical Properties Of Polymer Composites, Radwa Alaziz

Theses and Dissertations

The purpose of this research is to investigate the influence of stitching architectures by using different stitching periodic patterns on the in-plane and out-of-plane mechanical properties. By using the inherent periodic architecture of these composites, their mechanical properties may be tailored for specific applications. Composite structures are extensively used in several industries such as aerospace, automotive, sports, and construction due to their many advantages, which include tailorable mechanical properties, high strength-to-weight ratios, and high specific stiffness. However, due to their low interlaminar tensile strength, composites are prone to delaminations, which can degrade the overall mechanical performance of the structure. Through-thickness …

Gas Permeability Of 3d Stitched Composites For Cryogenic Applications, Shuvam Saha

Theses and Dissertations

This research aims to investigate the influence of 3D through-thickness stitching on the gas permeability and transverse microcracking of cryogenically cycled carbon/epoxy composites. 3D through-thickness stitching can be used to improve the interlaminar properties of polymer matrix composites (PMCs) and produce lightweight, unitized structures for cryogenic storage tanks. To fully utilize stitched composite structures for these applications, their inherent gas permeability challenges must be understood. Therefore, in this study, the stitched composites' damage evolution and gas permeability was experimentally characterized under a) pure thermal stress, b) thermal and uniaxial mechanical stress, and c) thermal and biaxial mechanical stress. Helium gas …

Effects Of Alternative Jet Fuels On Aerospace-Grade Composites: Experimental And Modeling Studies, Naoufal Harich

Theses and Dissertations

The aviation industry aims to reduce its environmental impact through innovation and research. The usage of composite materials for multiple primary structures represents one such measure. Several alternative fuels were approved and used along with the Federal Aviation Administration (FAA). These alternative fuels are produced from wastes and biomasses. Some alternative fuels were initially only approved as drop-in fuels, meaning they must be blended with conventional fuels to operate. Fuel tanks are usually embedded into the wing structure, which is mainly made of composite materials. These composites tend to absorb fluids it encounters through their matrix phase. The absorption behavior …

Towards An Understanding Of The Thermodynamic Properties Of Crtao4: A Computational Perspective, Tanner B. Gordon

Theses and Dissertations

Materials that can withstand higher temperatures are paramount for next-generation aircraft design. Hypersonic capabilities and jet-turbine engines operate in extreme environments. Choosing materials that have high thermal stability and oxidation resistance for these applications can increase engine efficiency, reduce size, weight and power (SWaP), and increase the maneuverability of the aircraft. The mixed oxide CrTaO₄ has been experimentally observed to significantly contribute to oxidation resistance at high temperatures. However, and despite its significance, its properties remain largely unknown. This work explores the thermal properties of this material from a multi-scale approach, by obtaining an accurate description of the thermodynamics …

Experimental And Computational Bearing Strength Of Fiber Metal Laminate With And Without Film Adhesive, Christopher L. Bellanova Jr.

Theses and Dissertations

This research characterized the performance of a fiber metal laminate composed of carbon fiber and stainless steel without film adhesive and compared it to a similar, previously tested, fiber metal laminate including film adhesive. Removal of the adhesive layers reduced the localized thickness, simplified manufacturing, and allowed for a 20% increase in foil thickness. Quasi-static testing was conducted in double shear, single shear protruding, and single shear countersunk configurations. The results were compared to adhesive hybrid and control samples. To study the affects of bolt tension, samples at low torque in double shear were also tested. Progressive failure samples revealed …

Mechanical Properties And Performance Of A Novel Nano-Engineered Unitized Composite With Quasi-Isotropic Layup, Brian Matthew Pudlo

Theses and Dissertations

Carbon nanotubes (CNTs) exhibit outstanding mechanical, electrical, and thermal properties, but are a challenge to effectively implement into macroscopic composites for aerospace applications. This research investigates the mechanical properties and performance of a newly developed hybrid NanoStitch composite, alongside a control polymer matrix composite, at room temperature. Both composite material systems investigated in this work have quasi-isotropic layup. Monotonic tension-tofailure, tension-tension fatigue, and creep tests were performed to characterize the performance of the composites under cyclic and sustained loading. Experimental results obtained for the quasi-isotropic NanoStitch composite were compared to those obtained for the quasi-isotropic control composite. The properties and …

Additively Manufactured Lenses For Modulating Guided Waves In Laminated Composites, Hajar Righi

Theses and Dissertations

Composite materials have increasingly been used as an alternative to metals and other isotropic materials for primary structural components in aerospace industries. Unlike traditional isotropic materials, composite materials are known to have complex internal microstructures. Therefore, it is essential to develop methods for the inspection, evaluation, and monitoring of composite materials. Ultrasonic-guided waves and, more precisely, Lamb waves have proven to be an efficient and accurate technique for the non-destructive testing. Since guided waves are dispersive and multimodal, it is important to develop a practical method to manipulate Lamb waves to achieve better structural health monitoring and non-destructive inspection results. …

Structural Sizing Of Post-Buckled Thermally Stressed Stiffened Panels, Walid Arsalane

Theses and Dissertations

Design of thermoelastic structures can be highly counterintuitive due to design-dependent loading and impact of geometric nonlinearity on the structural response. Thermal loading generates in-plane stresses in a restrained panel, but the presence of geometric nonlinearity creates an extension-bending coupling that results in considerable transverse displacement and variation in stiffness characteristics, and these affects are enhanced in post-bucking regimes. Herein a methodology for structural sizing of thermally stressed post-buckled stiffened panels is proposed and applied for optimization of the blade and hat stiffeners using a gradient-based optimizer. The stiffened panels are subjected to uniform thermal loading and optimized for minimum …

Effects Of A Nitrogen And Hydrogen Build Atmosphere On The Properties Of Additively Manufactured Tungsten, Dana C. Madsen

Theses and Dissertations

Additively manufactured tungsten was printed in pure nitrogen, nitrogen-2.5% hydrogen, and nitrogen-5% hydrogen atmospheres as part of a 2^3 full factorial designed experiment and subjected to room temperature and high-temperature three-point-bend testing, chemical analysis, hardness testing, and microstructural imaging techniques. The pure nitrogen specimens exhibited the highest strength and ductility at both high temperature and room temperature. Chemical analysis showed a 2-8x reduction in compositional oxygen relative to unprocessed powder. Hardness values for all samples was between 306.8 and 361.5 HV1. It is proposed that adding hydrogen into the build atmosphere reduced the available energy density for tungsten melting by …

Investigation Of Additively Manufactured Molybdenum-Tungsten-Rhenium Alloys, Randolph T. Abaya

Theses and Dissertations

The process of creating metal components through additive manufacturing is changing the way different industries can avoid the shortcomings of traditional metal production. Metals such as tungsten, molybdenum, and rhenium have many advantages for different applications, especially when alloyed together. In this study, an additively manufactured alloy containing 70% molybdenum, 25% tungsten, and 5% rhenium (70Mo-25W-5Re) is tested for its strength, ductility, hardness, and porosity. The 70Mo-25W-5Re alloy is printed through Laser Powder Bed Fusion (LPBF) under different conditions such as printing speed and printing atmosphere. Additionally, the effects of post printing heat treatment are conducted to understand the advantages …

Thermal Relaxation Of Shot Peen Induced Residual Stresses In A Nickel-Base Superalloy, Bryce E. Van Velson

Theses and Dissertations

Shot peening induces compressive residual stresses in components that positively influence fatigue life. Thermal and mechanical loading causes those residual stresses to relax. The hole drilling method and xray diffraction is used to measure the thermal relaxation of residual stresses in the nickel-base superalloy ME3.

Creep Behavior And Deformation Mechanisms Of Spark Plasma Sintered Oxide Ceramics For Aerospace Systems At 1300˚C - 1400˚C, David D. Swanson

Theses and Dissertations

The mechanical behavior of YAG and LuAG was investigated at elevated temperatures. The specific materials investigated in this work include high-purity, polycrystalline YAG, high-purity, polycrystalline LuAG, and two doped variants of YAG: 2at% Yb-doped, polycrystalline YAG and 2at% Er-doped, polycrystalline YAG. Several billets of each material were prepared and processed by means of spark plasma sintering (SPS). Many different sintering parameters were utilized in order to obtain materials with various physical properties and to identify the effects of sintering parameters on the average grain size of the resulting materials. The compressive creep behavior of these materials was investigated at 1300°C …

Evaluation Of Additively Manufactured Lattices Under High Strain Rate Impact, Derek G. Spear

Theses and Dissertations

Several additively manufactured lattice designs and configurations were evaluated under compression loads under various strain rates from quasi-static to highly dynamic. These experiments examined how the mechanical behavior of the lattice changed based on the lattice design properties and the applied strain rates. The modulus of elasticity, yield strength, plateau stress, and toughness were observed to decrease with an increase in strain rate, revealing that the lattice designs exhibit a negative strain rate sensitivity. A new lattice flow stress model was developed to account for the mechanical response of the lattice and was incorporated into a computational model for simulation. …

Fluid-Structure Interaction Of Nrel 5-Mw Wind Turbine, Mohamed Sayed Elkady Abd-Elhay

Theses and Dissertations

Wind energy is considered one of the major sources of renewable energy. Nowadays, wind turbine blades could exceed 100 m to maximize the generated power and minimize produced energy cost. Due to the enormous size of the wind turbines, the blades are subjected to failure by aerodynamics loads or instability issues. Also, the gravitational and centrifugal loads affect the wind turbine design because of the huge mass of the blades. Accordingly, wind turbine simulation became efficient in blade design to reduce the cost of its manufacturing. The fluid-structure interaction (FSI) is considered an effective way to study the turbine's behavior …

Design And Analysis Of Air-Stiffened Vacuum Lighter-Than-Air Structures, Ruben Adorno-Rodriguez

Theses and Dissertations

Lighter-than-air (LTA) systems have been developed for numerous applications and have taken several forms. Airships, aerostats, blimps, and balloons are all part of this family of systems, which uses Archimedes principle to achieve neutral and positive buoyancy in air by replacing an air volume with LTA gases. These lifting gases stiffen the otherwise compliant envelope structures, allowing them to sustain the pressure difference brought by the displaced air. The compliance of these structures is a byproduct of the weight requirement, materials and geometrical arrangement of which these structures are built from, typically resulting in dimensionalities that exhibit low or virtually …

Static Fatigue Of Hi-Nicalon™ S Ceramic Fiber Tows At 600°C In Air And Silicic Acid-Saturated Steam, Caleigh M. Nelson

Theses and Dissertations

Ceramic matrix composites (CMCs) have the potential to be utilized in applications such as hypersonic vehicles, aircraft leading edges, hot sections of engines, and rocket nozzles. Of particular interest are advanced SiC/SiC composites that can withstand the elevated temperatures and harsh oxidizing environments while maintaining their properties and structural integrity under an applied load. Steam, a major component of combustion environment, is one such aggressive oxidizing environment. As steam passes through the SiC/SiC composite, entering the composite interior through the cracks in the SiC matrix, it becomes saturated with silicic acid, Si(OH)₄. Before incorporating SiC/SiC composites in the …

Fatigue Of Two Oxide/Oxide Ceramic Matrix Composites At 1200°C In Air And In Steam. Effect Of Diamond Drilled Effusion Holes, Anthony R. Cabri

Theses and Dissertations

The tension-tension fatigue behavior of two oxide-oxide ceramic matrix composites (CMCs) was investigated at 1200°C in laboratory air and steam. Both composites consist of a porous oxide matrix reinforced with laminated, woven mullite/alumina (NextelTM720) fibers. The first composite had an alumina matrix, while the second had an alumina-mullite matrix. First, we assessed the effects of incorporating mullite into the matrix material on fatigue performance by studying the tension-tension fatigue behavior of alumina-mullite matrix CMC. Second, we evaluated the effects of effusion holes on the alumina matrix CMC's fatigue performance. Specimens containing an array of 17 effusion holes of 0.5-mm diameter …

Structural Dynamic And Inherent Damping Characterization Of Additively Manufactured Airfoil Components, Andrew W. Goldin

Theses and Dissertations

The push for low cost and higher performance/efficient turbine engines have introduced a new demand for novel technologies to improve robustness to vibrations resulting in High Cycle Fatigue (HCF). There have been many proposed solutions to this, some passive and some active. With the advent of Additive Manufacturing (AM), new damping techniques can now be incorporated directly into the design and manufacture process to suppress the vibrations that create HCF. In this study, this novel unfused pocket damping technology is applied to a blade structure and the resulting damping effectiveness is quantified. The application of this technology to complex geometries …

Laser Shock Peening Pressure Impulse Determination Via Empirical Data-Matching With Optimization Software, Colin C. Engebretsen

Theses and Dissertations

Laser shock peening (LSP) is a form of work hardening by means of laser induced pressure impulse. LSP imparts compressive residual stresses which can improve fatigue life of metallic alloys for structural use. The finite element modeling (FEM) of LSP is typically done by applying an assumed pressure impulse, as useful experimental measurement of this pressure impulse has not been adequately accomplished. This shortfall in the field is a current limitation to the accuracy of FE modeling, and was addressed in the current work. A novel method was tested to determine the pressure impulse shape in time and space by …

Evaluating The Effectiveness Of Aerospace Materials, Vehicle Shape And Astronaut Position At Lowering The Whole Body Effective Dose Equivalent In Deep Space, Daniel K. Bond

Theses and Dissertations

As future crewed, deep space missions are being planned, it is important to assess how spacecraft design can be used to minimize radiation exposure. Collectively with shielding material, vehicle shape and astronaut position must be used to protect astronauts from the two primary sources of space radiation: Galactic Cosmic Rays (GCR) and Solar Particle Events (SPE). GCRs, which are composed of low intensity, highly energetic, and fully ionized stable and meta-stable isotopes, are considered a chronic source of radiation risk to the astronauts. SPEs, which originate from solar coronal mass ejections, are composed mostly of high intensity protons that can …

Peridynamic Approaches For Damage Prediction In Carbon Fiber And Carbon Nanotube Yarn Reinforced Polymer Composites, Forrest E. Baber

Theses and Dissertations

Aerospace structures are increasingly utilizing advanced composites because of their high specific modulus and specific strength. While the introduction of these material systems can dramatically decrease weight, they pose unique certification challenges, often requiring extensive experimental testing in each stage of the design cycle. The expensive and time-consuming nature of experimental testing necessitates the advancement of simulation methodologies to both aid in the certification process and assist in the exploration of the microstructure design space.

Peridynamic (PD) theory, originating from Sandia National Lab’s in the early 2000’s, is a nonlocal continuum-based method that reformulates the equation of motion into an …

Piezoelectric Sensor Crack Detection On Airframe Systems, Kevin J. Lin

Theses and Dissertations

In 2008, the Department of Defense published a guidebook for a methodology named Condition-Based Maintenance Plus (CBM+) which capabilities include improving productivity, shortening maintenance cycles, lowering costs, and increasing availability and reliability. This push replaces existing inspection criteria, often conducted as non-destructive testing (NDT), with structural health monitoring (SHM) systems. The SHM system addressed utilizes guided Lamb waves generated by piezoelectric wafer active sensors (PWAS) to detect the existence, size, and location of damage from through-thickness cracks around a rivet hole. The SHM field lacks an experiment testing how small changes in receiver sensor distances affect damage detection. In addition, …