Structures and Materials Commons^™

Multiphysics Transport In Porous Thermal Protection Systems: Experimental Characterization Of Gas Permeability And Radiative Properties, Yejajul Hakim

Theses and Dissertations--Mechanical and Aerospace Engineering

Porous thermal protection systems (TPS) used in hypersonic vehicles exhibit coupled gas and radiative transport across multiple regimes and length scales. Accurate performance prediction requires reliable characterization of permeability, slip-flow behavior, and radiative transport properties, particularly for low-permeability and charred materials where existing data are limited. This dissertation presents experimental methods for characterizing multiphysics transport in porous TPS materials. A modular flow system was developed to measure permeability and slip behavior in both virgin and charred materials under relevant environments. A transient pressure decay method enables accurate permeability estimation in low-permeability regimes and provides insight into effective pore structure. Results …

Investigation Of Subsurface Thermal Radiation Phenomena In Fibrous Thermal Protection Systems, Colby L. Gore

Theses and Dissertations--Science, Technology, Engineering, and Mathematics (STEM) Education

Atmospheric re-entry induces intense thermal stress upon vehicles through a high-enthalpy boundary layer that encompasses the craft. To protect these vehicles, numerous insulative methods, known as thermal protection systems (TPS), are deployed to protect the craft during re-entry. The TPS materials insulate the craft from intense thermal transmission that would terminate a mission. In hypersonic environments, vast temperature gradients exist, enforcing the exponential effect of thermal radiation. However, TPS materials are commonly low-density fibrous materials that allow for the potential to be penetrated by thermal radiation. A series of arc-jet tests was completed to replicate enhanced radiative conditions in a …

The Determination Of Darcy Permeabilities And Slip Parameters In Porous Thermal Protection Media Via Pressure-Driven Steady Flows At Varying Levels Of Thermal Decomposition, John Ryan O'Nan

Theses and Dissertations--Mechanical and Aerospace Engineering

A flow apparatus for determining the Darcy permeability and Klinkenberg molecular slip adjustment parameter in arbitrary porous media was created. Two leak-proof methods were developed to secure samples of porous media in the flow apparatus independent of surface irregularities, structural integrity, or material porosity. The first of these methods uses thermoset resin casting to permit material samples of a highly irregular profile to be studied. The second method utilizes heat-shrink polyolefin tubing to create a wall seal while preserving the exposed faces of a given cylindrical sample, enabling the study of inhomogeneous surface features. These methods were used to characterize …

High-Fidelity Coupling For Studies Of Ablative Materials At Hypersonic Conditions, Aleksander Zibitsker

Theses and Dissertations--Mechanical and Aerospace Engineering

The development of accurate models and robust numerical tools for simulating ablative thermal protection materials (TPMs) in hypersonic flows is crucial for advancing atmospheric entry and hypersonic technologies. Traditional methods for simulating ablative materials often rely on heavy assumptions, such as equal heat and mass transfer coefficients and chemical equilibrium in the boundary layer, leading to conservative thermal protection system (TPS) designs and insufficient accuracy for certain in-flight ablation phenomena.

This work presents a high-fidelity and versatile coupled framework between hypersonic flow and material response solvers. The flow domain is modeled with an innovative overset CHAMPS NBS-Cart solver, which features …

Characterization Of Heterogeneous Material Architectures Through X-Ray Computed Micro-Tomography, Cameron Brewer

Theses and Dissertations--Mechanical and Aerospace Engineering

Low-density carbon-phenolic composites, such as phenolic impregnated carbon ablator (PICA), possess meso-, micro-, and nano-pores making the structure of the resin difficult to characterize. X-ray Computed Tomography (XRCT) is a widely ac- cepted method for characterizing the carbon fiber preform, yet this technique is often insufficient for visualizing the resin because of its minimal attenuation of the incident x-ray beam. Phase Contrast Retrieval (PCR) reconstruction considers not only the linear attenuation coefficient, but also the refractive indices of the constituent materials. This research leverages phase contrast tomography to characterize the meso- and micro-structure of the porous resin phase with a …

Experimental Characterization And Quantification Of Deformation Behavior In A Porous Carbon Fiber Network, Robert N Quammen

Theses and Dissertations--Chemical and Materials Engineering

Due to their wide range of attractive functional properties (such as low thermal conductivity and low density) porous materials are utilized in a variety of applications. In order to characterize these properties and others, the intrinsically heterogeneous microstructures of these materials need to be taken into account. These microstructures result in interactions across multiple length scales spanning several orders of magnitude. This makes the creation of robust computational models and straight-forward predictions of mechanical properties difficult for porous materials. With this in mind, this dissertation aims to provide experimental mechanical and deformation information spanning the length scales of interest for …

Impact Of Spallation And Internal Radiation On Fibrous Ablative Materials, Raghava Sai Chaitanya Davuluri

Theses and Dissertations--Mechanical and Aerospace Engineering

Space vehicles are equipped with Thermal Protection Systems (TPS) that encounter high heat rates and protect the payload while entering a planetary atmosphere. For most missions that interest NASA, ablative materials are used as TPS. These materials undergo several mass and energy transfer mechanisms to absorb intense heat. The size and construction of the TPS are based on the composition of the planetary atmosphere and the impact of various ablative mechanisms on the flow field and the material. Therefore, it is essential to quantify the rates of different ablative phenomena to model TPS accurately. In this work, the impact of …

Application Of Multi-Scale Computational Techniques To Complex Materials Systems, Mujan N. Seif

Theses and Dissertations--Chemical and Materials Engineering

The applications of computational materials science are ever-increasing, connecting fields far beyond traditional subfields in materials science. This dissertation demonstrates the broad scope of multi-scale computational techniques by investigating multiple unrelated complex material systems, namely scandate thermionic cathodes and the metallic foam component of micrometeoroid and orbital debris (MMOD) shielding. Sc-containing "scandate" cathodes have been widely reported to exhibit superior properties compared to previous thermionic cathodes; however, knowledge of their precise operating mechanism remains elusive. Here, quantum mechanical calculations were utilized to map the phase space of stable, highly-faceted and chemically-complex W nanoparticles, accounting for both finite temperature and chemical …

Kentucky Re-Entry Universal Payload System (Krups): Hypersonic Re-Entry Flight, John Daniel Schmidt

Theses and Dissertations--Mechanical and Aerospace Engineering

The Kentucky Re-entry Universal Payload System (KRUPS) is a small capsule designed as a technology testbed for re-entry experiments. For its first incarnation, KRUPS has been designed to test Thermal Protection Systems (TPS) and instruments in re-entry flights. Because of the unique environment a vehicle undergoes during re-entry, there is a high-demand for experimental data from re-entry experiments. KRUPS has been developed at the University of Kentucky (UK) over the past seven years to meet this demand. After completing sub-orbital campaigns, the first KRUPS hypersonic re-entry mission was attempted. The mission involved building three 11-inch diameter capsules each outfitted with …

Numerical Investigation On The Effect Of Spectral Radiative Heat Transfer Within An Ablative Material, Raghava S. C. Davuluri, Rui Fu, Kaveh A. Tagavi, Alexandre Martin

Mechanical Engineering Faculty Publications

The spectral radiative heat flux could impact the material response. In order to evaluate it, a coupling scheme between KATS - MR and P1 approximation model of radiation transfer equation (RTE) is constructed and used. A Band model is developed that divides the spectral domain into small bands of unequal widths. Two verification studies are conducted: one by comparing the simulation computed by the Band model with pure conduction results and the other by comparing with similar models of RTE. The comparative results from the verification studies indicate that the Band model is computationally efficient and can be used to …

Fully Coupled Internal Radiative Heat Transfer For The 3d Material Response Of Heat Shield, Raghava S. C. Davuluri, Rui Fu, Kaveh A. Tagavi, Alexandre Martin

Mechanical Engineering Faculty Publications

The radiative transfer equation (RTE) is strongly coupled to the material response code KATS. A P-1 approximation model of RTE is used to account for radiation heat transfer within the material. First, the verification of the RTE model is performed by comparing the numerical and analytical solutions. Next, the coupling scheme is validated by comparing the temperature profiles of pure conduction and conduction coupled with radiative emission. The validation study is conducted on Marschall et al. cases (radiant heating, arc-jet heating, and space shuttle entry), 3D Block, 2D IsoQ sample, and Stardust Return Capsule. The validation results agree well for …

Numerical Reconstruction Of Spalled Particle Trajectories In An Arc-Jet Environment, Raghava S. C. Davuluri, Sean C. C. Bailey, Kaveh A. Tagavi, Alexandre Martin

Mechanical Engineering Faculty Publications

To evaluate the effects of spallation on ablative material, it is necessary to evaluate the mass loss. To do so, a Lagrangian particle trajectory code is used to reconstruct trajectories that match the experimental data for all kinematic parameters. The results from spallation experiments conducted at the NASA HYMETS facility over a wedge sample were used. A data-driven adaptive methodology was used to adapts the ejection parameters until the numerical trajectory matches the experimental data. The preliminary reconstruction results show that the size of the particles seemed to be correlated with the location of the ejection event. The size of …

The Kentucky Re-Entry Universal Payload System (Krups): Orbital Flight, James Tyler Nichols

Theses and Dissertations--Mechanical and Aerospace Engineering

Due to the uniqueness of atmospheric entry environments, ground facilities cannot accurately replicate re-entry conditions. Consequently, scientists primarily rely on numerical models to predict these conditions and inform Thermal Protection System (TPS) designs. These models often lack flight validation, which is necessary for increasing their fidelity. Thus, there is a substantial need to obtain such data to advance modeling capabilities.

The Kentucky Re-entry Universal Payload System (KRUPS) is an adaptable test-bed for scientific experimentation with initial application to TPS. This vehicle was designed at the University of Kentucky to serve as an inexpensive means of obtaining validation data to enhance …

A Computational Fluid-Structure Interaction Method For Simulating Supersonic Parachute Inflation, Jonathan Boustani

Theses and Dissertations--Mechanical and Aerospace Engineering

Following the successful landing of the Curiosity rover on the Martian surface in 2012, NASA/JPL conducted the low-density supersonic decelerator (LDSD) missions to develop large diameter parachutes to land the increasingly heavier payloads being sent to the Martian surface. Unexpectedly, both of the tested parachutes failed far below their design loads. It became clear that there was an inability to model and predict loads that occur during supersonic parachute inflation. In this dissertation, a new computational method that was developed to provide NASA with the capability to simulate supersonic parachute inflation is presented and validated. The method considers the loose …

Structural Optimization Of Space Transit Vehicle Concept, Hercules, James Philip Rogers

Theses and Dissertations--Mechanical and Aerospace Engineering

STRUCTURAL OPTIMIZATION OF SPACE TRANSIT VEHICLE CONCEPT, HERCULES:

A COMPARATIVE STUDY OF STRUCTURAL OPTIONS

Hercules is a vehicle concept developed by NASA Langley's Vehicle Analysis Branch to satisfy the need for sustainable transit between Earth, the moon, and Mars. Hercules features unprecedented abort capabilities and mission flexibility to aid in NASA's Mars campaign. By utilizing modern software to perform structural analysis and optimization for a large selection of stiffened panel concepts, beam concepts, and materials trends in the structural optimization emerge. These trends will be invaluable for the design of future spacecraft needed to fulfill similar roles.

The structural optimization …

Influence Of Size Effects On Surface Generation During Finish Machining And Surface Integrity In Ti-6al-4v, Ian S. Brown

Theses and Dissertations--Mechanical and Aerospace Engineering

Finish machining is an essential manufacturing process that is used to enhance the mechanical characteristics of critical components. The deformation that occurs at the tool and workpiece interface in finish machining significantly affects a host of component properties, commonly referred to as “surface integrity” properties. Surface roughness is a machining deformation-affected characteristic that is of high relevance in contemporary manufacturing. However, over recent decades it has been made clear that the material properties of the deformed surface layers are relevant to component performance as well. Predicting the overall surface quality of a machined component is of great relevance to the …

Carbon Oxidation At The Atomic Level: A Computational Study On Oxidative Graphene Etching And Pitting Of Graphitic Carbon Surfaces, Simon Schmitt

Theses and Dissertations--Mechanical and Aerospace Engineering

In order to understand the oxidation of solid carbon materials by oxygen-containing gases, carbon oxidation has to be studied on the atomic level where the surface reactions occur. Graphene and graphite are etched by oxygen to form characteristic pits that are scattered across the material surface, and pitting in turn leads to microstructural changes that determine the macroscopic oxidation behavior. While this is a well-documented phenomenon, it is heretofore poorly understood due to the notorious difficulty of experiments and a lack of comprehensive computational studies. The main objective of the present work is the development of a computational framework from …

Enhanced Surface Integrity With Thermally Stable Residual Stress Fields And Nanostructures In Cryogenic Processing Of Titanium Alloy Ti-6al-4v, James R. Caudill

Theses and Dissertations--Mechanical and Aerospace Engineering

Burnishing is a chipless finishing process used to improve surface integrity by severe plastic deformation (SPD) of surface asperities. As surface integrity in large measure defines the functional performance and fatigue life of aerospace alloys, burnishing is thus a means of increasing the fatigue life of critical components, such as turbine and compressor blades in gas turbine engines. Therefore, the primary objective of this dissertation is to characterize the burnishing-induced surface integrity of Ti-6Al-4V alloy in terms of the implemented processing parameters. As the impact of cooling mechanisms on surface integrity from SPD processing is largely unexplored, a particular emphasis …

Fracture Initiation In A Transversely Isotropic Solid: Transient Three Dimensional Analysis, Louis Milton Brock

Mechanical Engineering Faculty Publications

A transversely isotropic solid is at rest, and contains a semi-infinite, plane crack. The axis of rotational material symmetry lies in the crack plane. Application of normal point forces to each face of the crack causes transient 3D growth. The related problem of discontinuities in displacement and traction that exist on regions that exhibit dynamic similarity is first considered. Analytic results are obtained in integral transform space. These lead to equations of the Wiener–Hopf type for the fracture problem. Analytic solutions are again obtained and, upon inversion, subjected to a dynamic energy release rate criterion that includes kinetic energy. A …

Thermo-Mechanical Coupling For Ablation, Rui Fu

Theses and Dissertations--Mechanical and Aerospace Engineering

In order to investigate the thermal stress and expansion as well as the associated strain effect on material properties caused by high temperature and large temperature gradient, a two-way thermo-mechanical coupling solver is developed. This solver integrates a new structural response module to the Kentucky Aerothermodynamics and Thermal response System (KATS) framework. The structural solver uses a finite volume approach to solve either hyperbolic equations for transient solid mechanics, or elliptic equations for static solid mechanics. Then, based on the same framework, a quasi-static approach is used to couple the structural response and thermal response to estimate the thermal expansion …

Transient Analysis Of Fracture Initiation In A Coupled Thermoelastic Solid, Louis Milton Brock

Mechanical Engineering Faculty Publications

An isotropic, thermoelastic solid is initially at rest at uniform (absolute) temperature, and contains a semi-infinite, plane crack. Application of in-plane and normal point forces to each face of the crack causes transient 3D growth. The related problem of discontinuities in temperature and displacement that exist on regions that exhibit dynamic similarity is first considered. Asymptotic expressions, whose inverses are valid near the crack edges for short times, are obtained in integral transform space. These lead to equations of the Wiener–Hopf type for the fracture problem. Analytical solutions are obtained and, upon inversion, subjected to a dynamic energy release rate …

Analytical Strip Method For Thin Cylindrical Shells, John T. Perkins

Theses and Dissertations--Civil Engineering

The Analytical Strip Method (ASM) for the analysis of thin cylindrical shells is presented in this dissertation. The system of three governing differential equations for the cylindrical shell are reduced to a single eighth order partial differential equation (PDE) in terms of a potential function. The PDE is solved as a single series form of the potential function, from which the displacement and force quantities are determined. The solution is applicable to isotropic, generally orthotropic, and laminated shells. Cylinders may have simply supported edges, clamped edges, free edges, or edges supported by isotropic beams. The cylindrical shell can be stiffened …

Large Linear Magnetoresistance In Heavily-Doped Nb:Srtio3 Epitaxial Thin Films, Hyunwoo Jin, Keundong Lee, Seung-Hyub Baek, Jin-Sang Kim, Byung-Ki Cheong, Bae Ho Park, Sungwon Yoon, B. J. Suh, Changyoung Kim, Sung S. Ambrose Seo, Suyoun Lee

Physics and Astronomy Faculty Publications

Interaction between electrons has long been a focused topic in condensed-matter physics since it has led to the discoveries of astonishing phenomena, for example, high-T_c superconductivity and colossal magnetoresistance (CMR) in strongly-correlated materials. In the study of strongly-correlated perovskite oxides, Nb-doped SrTiO₃ (Nb:SrTiO₃) has been a workhorse not only as a conducting substrate, but also as a host possessing high carrier mobility. In this work, we report the observations of large linear magnetoresistance (LMR) and the metal-to-insulator transition (MIT) induced by magnetic field in heavily-doped Nb:STO (SrNb_0.2Ti_0.8O₃) epitaxial thin …

Growth Control Of Oxygen Stoichiometry In Homoepitaxial Srtio3 Films By Pulsed Laser Epitaxy In High Vacuum, Ho Nyung Lee, Sung S. Ambrose Seo, Woo Seok Choi, Christopher M. Rouleau

Physics and Astronomy Faculty Publications

In many transition metal oxides, oxygen stoichiometry is one of the most critical parameters that plays a key role in determining the structural, physical, optical, and electrochemical properties of the material. However, controlling the growth to obtain high quality single crystal films having the right oxygen stoichiometry, especially in a high vacuum environment, has been viewed as a challenge. In this work, we show that, through proper control of the plume kinetic energy, stoichiometric crystalline films can be synthesized without generating oxygen defects even in high vacuum. We use a model homoepitaxial system of SrTiO₃ (STO) thin films on …

Cryogenic Processing Of Al 7050-T7451 Alloy For Improved Surface Integrity, Bo Huang

Theses and Dissertations--Mechanical and Aerospace Engineering

Al 7050-T7451 alloy with good combinations of strength, stress corrosion cracking resistance and toughness, is used broadly in the aerospace/aviation industry for fatigue-critical airframe structural components. However, it is also considered as a highly anisotropic alloy as the crack growth behavior along the short transverse direction is very different from the one in the long transverse direction, due to the inhomogeneous microstructure with the elongated grains distributed in the work material used in the sheet/plate applications. Further processes on these materials are needed to improve its mechanical and material properties and broaden its applications.

The material with ultra-fine or nano …

Shape Memory Behavior Of Single Crystal And Polycrystalline Ni-Rich Nitihf High Temperature Shape Memory Alloys, Sayed M. Saghaian

Theses and Dissertations--Mechanical and Aerospace Engineering

NiTiHf shape memory alloys have been receiving considerable attention for high temperature and high strength applications since they could have transformation temperatures above 100 °C, shape memory effect under high stress (above 500 MPa) and superelasticity at high temperatures. Moreover, their shape memory properties can be tailored by microstructural engineering. However, NiTiHf alloys have some drawbacks such as low ductility and high work hardening in stress induced martensite transformation region. In order to overcome these limitations, studies have been focused on microstructural engineering by aging, alloying and processing.

Shape memory properties and microstructure of four Ni-rich NiTiHf alloys (Ni50.3Ti29.7Hf20, Ni50.7Ti29.3Hf20, …

Precipitation, Orientation And Composition Effects On The Shape Memory Properties Of High Strength Nitihfpd Alloys, Emre Acar

Theses and Dissertations--Mechanical and Aerospace Engineering

NiTiHf high temperature shape memory alloys are attractive due to their high operating temperatures (>100 ^oC) and acceptable transformation strain compared to NiTi. However, NiTiHf has limitations due to their lack of ductility and low strength, resulting in poor shape memory properties. In this study, Pd has been added to NiTiHf alloys in an attempt to improve their shape memory behavior. A combined approach of quaternary alloying and precipitation strengthening was used.

The characterization of a Ni_45.3Ti_29.7Hf₂₀Pd₅ (at. %) polycrystalline alloy was performed in compression after selected aging treatments. Transmission electron …

A Design Pathfinder With Material Correlation Points For Inflatable Systems, Jared T. Fulcher

Theses and Dissertations--Mechanical and Aerospace Engineering

The incorporation of inflatable structures into aerospace systems can produce significant advantages in stowed volume to mechanical effectiveness and overall weight. Many applications of these ultra-lightweight systems are designed to precisely control internal or external surfaces, or both, to achieve desired performance. The modeling of these structures becomes complex due to the material nonlinearities inherent to the majority of construction materials used in inflatable structures. Furthermore, accurately modeling the response and behavior of the interfacing boundaries that are common to many inflatable systems will lead to better understanding of the entire class of structures. The research presented involved using nonlinear …

Multidimensional Modeling Of Pyrolysis Gas Transport Inside Orthotropic Charring Ablators, Haoyue Weng

Theses and Dissertations--Mechanical and Aerospace Engineering

During hypersonic atmospheric entry, spacecraft are exposed to enormous aerodynamic heat. To prevent the payload from overheating, charring ablative materials are favored to be applied as the heat shield at the exposing surface of the vehicle. Accurate modeling not only prevents mission failures, but also helps reduce cost. Existing models were mostly limited to one-dimensional and discrepancies were shown against measured experiments and flight-data. To help improve the models and analyze the charring ablation problems, a multidimensional material response module is developed, based on a finite volume method framework. The developed computer program is verified through a series of test-cases, …

Materials Selection And Processing Techniques For Small Spacecraft Solar Cell Arrays, Naseem M. Torabi

Theses and Dissertations--Electrical and Computer Engineering

Body mounted germanium substrate solar cell arrays form the faces of many small satellite designs to provide the primary power source on orbit. High efficiency solar cells are made affordable for university satellite programs as triangular devices trimmed from wafer scale solar cells. The smaller cells allow array designs to pack tightly around antenna mounts and payload instruments, giving the board design flexibility. One objective of this work is to investigate the reliability of solar cells attached to FR-4 printed circuit boards. FR-4 circuit boards have significantly higher thermal expansion coefficients and lower thermal conductivities than germanium. This thermal expansion …