Engineering Commons^™

Development Of A Potassium Permanganate Catalyst-Infused Fuel Grain For Hydrogen Peroxide Hybrid Thruster Ignition Enhancement, Ryan J. Thibaudeau

All Graduate Theses and Dissertations, Fall 2023 to Present

This thesis describes and addresses the need for reliable ignition in small satellite hybrid propulsion systems using hydrogen peroxide. It describes process of creating custom 3D printed ABS plastic fuel grains with small amounts of catalysts. These catalysts lead to a more reliable and energy-efficient ignition of a hybrid rocked propulsion system using catalyst-infused ABS and high-test hydrogen peroxide (HTP). Hydrogen peroxide is a high-density oxidizer and therefore more volumetrically efficient for a small satellite using hybrid rocket technology when compared to gaseous oxygen (GOX). The traditional ignition methods of hybrid rocket propulsion systems using HTP are compared to and …

Characterization Of Interlayer Laser Shock Peening During Fused Filament Fabrication Of Polylactic Acid (Pla), Fabien Denise

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

The field of additive manufacturing (AM) has gained a significant amount of popularity due to the increasing need for more sustainable manufacturing techniques and the adaptive development of complex product geometries. The problem is that AM parts routinely exhibit flaws or weaknesses that affect functionality or performance. Over the years, surface treatments have been developed to compensate certain flaws or weaknesses in manufactured products. Combining surface treatments with the modularity of additive manufacturing could lead to more adaptable and creative improvements of product functions in the future. The current work evaluates the feasibility of pursuing a new research axis in …

Study On Debinding And Sintering Conditions In Extrusion-Based Additive Manufacturing Of 316l And 316l + Cu, Jean-François Silvain, Daniel Lincoln Gifford, Sébastien Fourcade, Laurent Cuzacq, Jean-Luc Grosseau-Poussard, Catherine Debiemme-Chouvy, Nicolas Tessier Doyen, Yongfeng Lu

Department of Electrical and Computer Engineering: Faculty Publications

This study investigates the use of a methylcellulose binder in extrusion additive manufacturing of 316L as an alternative to common wax-based binders. Various quantities of copper (Cu) powder were also added in the paste composition to attempt to reduce the sintering temperature by promoting persistent liquid phase sintering. Debinding experiments were conducted under different temperatures and dwell times using argon (Ar), Ar/5%H₂, and Ar/1%O₂ atmospheres. Debinding reduced carbon (C) content to 0.032 wt.% by using a two-step debinding process of Ar/5%H₂ and Ar/1%O₂ thermal treatments. Using this debinding process, sintering was conducted at 1200 ^{o …}

A Review Of The Mechanical Properties Of 17-4ph Stainless Steel Produced By Bound Powder Extrusion, Jaidyn Jones, Ana Vafadar, Reza Hashemi

Research outputs 2022 to 2026

17-4PH Stainless Steel is a mechanically high-performing alloy that is widely used across chemical and mechanical processing industries. The alloy is conventionally fabricated by cast methods, but emerging additive manufacturing techniques are presently offering an economic, efficient, and environmentally friendly alternative. Bound Powder Extrusion (BPE) is a relatively new additive manufacturing technique that is used to fabricate three-dimensional, free-form components. Investigation into the mechanical properties and behavior of 17-4PH stainless steel fabricated by BPE is vital to understanding whether this technique proposes a competitive substitute to the cast alloy within industry. Published literature has investigated the as-fabricated mechanical properties, microstructure, …

Understanding Melt Pool Characteristics In Laser Powder Bed Fusion: An Overview Of Single- And Multi-Track Melt Pools For Process Optimization, Jincheng Wang, Rui Zhu, Yujing Liu, Laichang Zhang

Research outputs 2022 to 2026

Laser powder bed fusion (LPBF) has made significant progress in producing solid and porous metal parts with complex shapes and geometries. However, LPBF produced parts often have defects (e.g., porosity, residual stress, and incomplete melting) that hinder its large-scale industrial commercialization. The LPBF process involves complex heat transfer and fluid flow, and the melt pool is a critical component of the process. The melt pool stability is a critical factor in determining the microstructure, mechanical properties, and corrosion resistance of LPBF produced metal parts. Furthermore, optimizing process parameters for new materials and designed structures is challenging due to the complexity …

Numerical Study Of Solar Receiver Tube With Modified Surface Roughness For Enhanced And Selective Absorptivity In Concentrated Solar Power Tower, Shawn Hatcher, Mathew Z. Farias, Jianzhi Li, Peiwen Li, Ben Xu

Manufacturing & Industrial Engineering Faculty Publications

Concentrated solar power (CSP) is a reliable renewable energy source that is progressively lowering its cost of energy. However, the heat loss due to reflected and emitted radiation hinders the maximum achievable thermal efficiency for solar receiver tubes on the solar tower. Current solar selective coatings cannot withstand the high temperatures that come with state-of-the-art CSP towers often needing to be recoated soon after initial operation. We intend to use Inconel 718 with different additive manufacturing (AM) practices to construct surfaces that allow for more light-trapping to occur. By adjusting printing parameters, we can tailor a surface to allow for …

Non-Planar 3d Printing Of Thermosetting Prepolymers, Junaid Abid Ali

Master's Theses

Additive manufacturing or three-dimensional (3D) printing is an advanced process of manufacturing that challenges traditional manufacturing methodologies. However, the current 3D printing process does exhibit specific limitations. It generates printing paths that are in a horizontal plane, proving inadequate for printing curved or non-flat structures. This study established a printing procedure capable of simultaneously executing printing in X, Y, and Z directions. The limitations posed by conventional 3D printing lead to the poor surface quality of curved printed objects. In contrast, non-planar 3D printing provides smoother surfaces. This work developed a program capable of producing non-planar print paths for the …

Investigation Of Deformation Behavior Of Additively Manufactured Aisi 316l Stainless Steel With In Situ Micro-Compression Testing, Fei Teng, Ching-Heng Shiau, Cheng Sun, Robert C. O'Brien, Michael D. Mcmurtrey

Materials Science and Engineering Faculty Publications and Presentations

Additive manufacturing techniques are being used more and more to perform the precise fabrication of engineering components with complex geometries. The heterogeneity of additively manufactured microstructures deteriorates the mechanical integrity of products. In this paper, we printed AISI 316L stainless steel using the additive manufacturing technique of laser metal deposition. Both single-phase and dual-phase substructures were formed in the grain interiors. Electron backscatter diffraction and energy-dispersive X-ray spectroscopy indicate that Si, Mo, S, Cr were enriched, while Fe was depleted along the substructure boundaries. In situ micro-compression testing was performed at room temperature along the [001] orientation. The dual-phase substructures …

Ai Methods For Identifying Process Defects In Advanced Manufacturing With Rare Labeled Data, Ayantha Umesh Senanayaka Mudiyanselage

Theses and Dissertations

This dissertation aims to provide efficient process defect identification methods for advanced manufacturing environments using AI tools/algorithms with limited labeled data availability. Asset and equipment quality become highly sensitive in sustaining virtuous performance and safety in various manufacturing domains. Internally generated process imperfections degrade finished products' optimum performance and mechanical attributes. The evolution of big data and intelligent sensing systems leverage data-driven defect identification in advanced manufacturing environments. Widely adopted data-driven process anomaly detection methods assume that the training (source) and testing (target) data follow the same distribution and that labeled data are available in both source and target domains. …

Fatigue And Fracture Of Electron Beam Melting Ti-6al-4v, William A. Grell

Electronic Theses and Dissertations

For applications in the aerospace field, selection of materials for a given design requires an understanding of critical properties, like fatigue and fracture, in addition to static mechanical and physical properties. With the ongoing advancements in metallic additive manufacturing techniques and the interest in applying the process to aerospace applications, there is a clear need to fully characterize properties. Arguably, the most attractive alloy for applications in aerospace is the Ti-6Al-4V alloy. The current dissertation examines the mechanical properties of the alloy, made by the Electron Beam Melting (EBM) Powder Bed Fusion (PBF) method. As illustrated in this work, the …

Enhancing Experiential Learning Through Virtual Reality: A Case Study In System Design And Hazard Analysis, Rafia Rahman Rafa

Industrial, Manufacturing, and Systems Theses - Archive

ABSTRACT: The recent advancement of additive manufacturing (AM) technologies leads to an extensive need for an industrial workforce. Training in AM requires expensive capital investment to install and maintain this technology and proper knowledge about potential safety hazards. Experiential, immersive training platforms like Virtual Reality (VR) can overcome this challenge by providing opportunities for effective learning in a safe and controlled environment. VR can teach students through active participation and immersive, hands-on experiences, which is especially important for manufacturing processes involving high-risk conditions. VR can expose students to manufacturing hazards and allow them to learn through trial and error without …

Towards Sustainable Additive Manufacturing: Assessment Of Cost, Greenhouse Gas Emission, And Recyclability, Lei Di

Industrial, Manufacturing, and Systems Engineering Dissertations - Archive

Additive Manufacturing technologies fabricate 3D objects layer by layer following a predesigned CAD model. Owing to the unique layer-wise production method, additive manufacturing offers competitive advantages in comparison with traditional subtractive manufacturing, such as shortened production time, increased design freedom, improved manufacturing capability and complexity, and reduced manufacturing waste. Numerous research studies have been conducted to design, understand, and improve additive manufacturing technologies in order to facilitate the implementation in the supply chain. On the other hand, with the rapid growth of additive manufacturing, sustainability issues that exist on both process level and supply chain level have started to receive …

A Hybrid Metaheuristic And Computer Vision Approach To Closed-Loop Calibration Of Fused Deposition Modeling 3d Printers, Graig S. Ganitano, Shay V. Wallace, Benji Maruyama, Gilbert L. Peterson

Faculty Publications

Fused deposition modeling (FDM) is one of the most popular additive manufacturing (AM) technologies for reasons including its low cost and versatility. However, like many AM technologies, the FDM process is sensitive to changes in the feedstock material. Utilizing a new feedstock requires a time-consuming trial-and-error process to identify optimal settings for a large number of process parameters. The experience required to efficiently calibrate a printer to a new feedstock acts as a barrier to entry. To enable greater accessibility to non-expert users, this paper presents the first system for autonomous calibration of low-cost FDM 3D printers that demonstrates optimizing …

Creep Resistance And Microstructure In Binary Aluminum Cerium Alloy Produced By Laser Powder Bed Fusion, Jillian Ann Stinehart

Master's Theses (2009 -)

Currently, the only commercially available aluminum alloy for additive manufacturing (AM) is AlSi10Mg, which is not suitable for high temperature applications. Al-Ce based alloys have been shown to be highly printable, cost-efficient alloys. Compared to cast Al-Ce alloys, the eutectic features are refined (<1μm), which give AM Al-10Ce favorable strength and ductility at room temperature. The low diffusivity and solubility of cerium in aluminum improve the retention of mechanical properties at high temperatures. In order to quantify the effect of cerium on the thermal stability of AM aluminum and show its suitability for high-temperature applications, Al-10Ce was creep tested between 60-77% of its absolute melting temperature. The creep performance of AM Al-10Ce was favorable compared to that of cast binary Al-Ce and AM AlSi10Mg and was comparable to that of cast ternary Al-Ce alloys. The stress exponent, n, was approximately 1 in the low stress regime and 5-7 in the high stress regime. The activation energy was 231kJ/mol. In comparison, both cast binary Al-Ce and AM AlSi10Mg have higher stress exponents and lower activation energies, showing AM Al-10Ce to be more creep resistant. After creep testing, slight grain coarsening was observed, while grain orientation remained unchanged. The melt pool boundaries (MPBs) faded in appearance after creep testing, and the number of columnar grains decreased.

Image Segmentation With Human-In-The-Loop In Automated De-Caking Process For Powder Bed Additive Manufacturing, Vincent Opare Addo Asare-Manu

Theses and Dissertations

Additive manufacturing (AM) becomes a critical technology that increases the speed and flexibility of production and reduces the lead time for high-mix, low-volume manufacturing. One of the major bottlenecks in further increasing its productivity lies around its post-processing procedures. This work focuses on tackling a critical and inevitable step in powder-bed additive manufacturing processes, i.e., powder cleaning or de-caking. Pressing concerns can be raised with human involvement when performing this task manually. Therefore, a robot-driven automatic powder cleaning system could be an alternative to reducing time consumption and increasing safety for AM operators. However, since the color and surface texture …

Integration Of Insoluble And Soluble Dopants Into Steel Using Laser Powder Bed Fusion, Mckay Goodman Sperry

Theses and Dissertations

Laser Powder Bed Fusion (LPBF) is an Additive Manufacturing (AM) method whereby complex parts can be built to near net geometry in an automated environment. Parts formed by LPBF have excellent properties and require little post-processing. While LPBF allows for creative designs to reduce weight and part count by integrating sub-components of assemblies, designers are limited to one material within any LPBF print. Although various materials can be used in LPBF, metals are of special interest to many industrial customers due to their high strength and toughness. The metals commonly used for LPBF include iron, aluminum, and titanium alloys. These …

Consumer 3d Printing For Remote Control Aircraft Wings: Development Of Novel Wingbox Structure, Ian Clark

University Honors Theses

Remote control aircraft construction and can be a very expensive and time-consuming hobby. With 3D printer consumer adoption rates skyrocketing, there is a gap between demand for RC aircraft and suitable well-designed models available to creators and hobbyists. By creating and testing two iterations of wingbox geometries, this research aims to help close that gap by producing an easily printable wing structure. While there are improvements that can be made on this work, this research has been effective in generating a novel wingbox structure for FFF 3D printing that has distinct advantages over other designs currently available.

Enhancing Microstructure, Composition Homogeneity, And Mechanical Properties In Laser Powder Bed Fused Metallic Alloys: Design, Fabrication, And Evaluation, Bahzad Farhang

Mechanical and Aerospace Engineering Dissertations - Archive

ABSTRACT: Over the past five decades, Nickel-based and Titanium-based alloys have become increasingly popular materials. As the manufacturing industry for these alloys has advanced, the demand for fabricating complex parts with enhanced mechanical properties at elevated temperatures has grown. Laser Powder Bed Fusion (LPBF), one of the most prevalent additive manufacturing techniques, has been employed successfully to produce these alloys. Nonetheless, there is still considerable effort being made to improve the microstructural, compositional, and mechanical properties of LPBF-processed components. In this study, we focused on adjusting the multi-scale microstructure and composition of LPBF-fabricated Nickel-based and Titanium-based alloys. The first objective …

Fusion Bonding Behavior Of 3d Printed Pa6/Cf Composites Via Post Fabrication Compaction, Gonzalo Fernandez Mediavilla

Mechanical & Aerospace Engineering Theses & Dissertations

Additive manufacturing (AM) is becoming a robust production technology for aerospace, healthcare, and construction industries among others. Fused Deposition Modelling (FDM) is one of the methods most used to 3D print products. FDM has limitation due to interlayer adhesion and restriction imposed by the printing direction. Specially with AM composites, as reinforced nylon PA6 with short fibers, parts show more strength along the direction of the filament due to the alignment of the carbon fibers, but weaker in other directions. The proposed method to solve this issue is to print parts separately and join them together by fusion bonding. PA6/CF …

Point Heat Source Correlation To Microstructural Evolution In Advanced Manufacturing, Mark Anderson

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Although there are different ways that advanced manufacturing can be performed, the use of single-point heat sources has become the standard to control a final product’s properties. It is imperative to understand how the heat source used in the different advanced manufacturing processes affect the microstructure of interest. The intimate relationship between the heat source and microstructure allows for controlling and tailoring a part’s properties. Utilizing different microstructural analysis, the cross-correlation of various point heat sources to developed microstructure was conducted in this dissertation.

Laser powder bed fusion allows for unique print-to-part protocols, but the dynamics of the process makes …

Mechanical And Thermal Performance Of Additively Manufactured Digital Materials, Layth Muayyad Ahmad

Mechanical and Aerospace Engineering Theses - Archive

Over the past decades, additive manufacturing has become a critical material processing tool. All ranges of materials including polymers, composites, metals, and ceramics can be used to fabricate structures with complex geometries that are nearly impossible to build using conventional fabrication process. Recently, additive manufacturing methods to build polymeric structures have been advanced significantly. In particular, the emergence of multi-material printers has made it possible to seamlessly print hybrid and digital materials where materials components and compositions are digitally varied to construct fully tailored material system. In this work, using a commercially available polyjet printer (Stratasys J850 Prime 3D printer), …

Multifunctional Additive Manufacturing And Multiphysics Numerical Investigations Of Carbon Fiber Structural Battery Composite Using A Drop-On-Demand Method With In-Situ Consolidation, Xiangyang Dong, Yuekun Chen

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Lightweight Carbon Fiber Structural Battery Composite Has Great Potential in Increasing Structural Energy Storage Efficiency for Multifunctional Applications. However, It is Still Challenging to Design Carbon Fiber Multifunctional Composite Due to Lack of Proper Manufacturing Methods. in This Study, an Integrated Multifunctional Design and Fabrication Approach is Developed by Combining a Drop-On-Demand Additive Manufacturing Method with a Multiphysics Numerical Model to Guide the Development of the New Multifunctional Composite. through Deposition with In-Situ Consolidation, the Function and Thickness of Each Carbon Fiber Layer as Well as its Fiber Volume Fraction Are Accurately Controlled. Decreasing Layer Thickness Improves Flexural Properties. the …

3d Printing With Photopolymerizable Polyester Resins For Resorbable Medical Device Applications, Mathew Murphy Stanford

All Dissertations

In the past decade, the healthcare industry has seen a significant increase in the use of additive manufacturing (AM or “3D printing”) with subsequent improvement in clinical outcomes.As an exceptional AM technology, vat-photopolymerization (VP), often called stereolithography, can create complex structures and has thus been adopted for a range of biomedical applications including surgical guides, temporary implants, and resorbable tissue scaffolds.However, limitations remain in the availability of photopolymerizable resin materials with appropriate mechanical performance, biodegradability, and biocompatibility for application to resorbable medical devices.

The objective of this work was to employ novel photopolymerizable polyester-based macromers in the development of resorbable …

Experimental And Numerical Studies Of Slurry-Based Coextrusion Deposition Of Continuous Carbon Fiber Micro-Batteries To Additively Manufacture 3d Structural Battery Composites, Aditya R. Thakur, Xiangyang Dong

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Carbon Fiber Structural Battery Composites Have Recently Attracted Growing Interests Due to their Potentials of Simultaneously Carrying Mechanical Loads and Storing Electrical Energy for Lightweight Application. in This Study, We Present a Slurry-Based Coextrusion Deposition Method to Additively Manufacture 3D Structural Battery Composites from Carbon Fiber Micro-Batteries. Cathode Slurry is Coextruded Together with Solid Polymer Electrolyte-Coated Carbon Fibers in a Single Deposition. a Network of Carbon Fiber Micro-Batteries is Achieved within the Fabricated Structural Battery Composites. Electrochemical Tests Show a Stable Charge-Discharge Performance Up to 100 Cycles. the Rheological Behavior of the Cathode Slurry is Found to Govern the Coextrusion …

Predicting Thermoelectric Power Factor Of Bismuth Telluride During Laser Powder Bed Fusion Additive Manufacturing, Ankita Agarwal, Tanvi Banerjee, Joy Gockel, Saniya Leblanc, Joe Walker, John Middendorf

Computer Science and Engineering Faculty Publications

An additive manufacturing (AM) process, like laser powder bed fusion, allows for the fabrication of objects by spreading and melting powder in layers until a freeform part shape is created. In order to improve the properties of the material involved in the AM process, it is important to predict the material characterization property as a function of the processing conditions. In thermoelectric materials, the power factor is a measure of how efficiently the material can convert heat to electricity. While earlier works have predicted the material characterization properties of different thermoelectric materials using various techniques, implementation of machine learning models …

Heterogeneous Sensor Data Fusion For Multiscale, Shape Agnostic Flaw Detection In Laser Powder Bed Fusion Additive Manufacturing, Benjamin Bevans, Christopher Barrett, Thomas Spears, Aniruddha Gaikwad, Alex Riensche, Harold (Scott) Halliday, Prahalada Rao

Department of Mechanical and Materials Engineering: Faculty Publications

We developed and applied a novel approach for shape agnostic detection of multiscale flaws in laser powder bed fusion (LPBF) additive manufacturing using heterogenous in-situ sensor data. Flaws in LPBF range from porosity at the micro-scale (< 100 μm), layer related inconsistencies at the meso-scale (100 μm to 1 mm) and geometry-related flaws at the macroscale (> 1 mm). Existing data-driven models are primarily focused on detecting a specific type of LPBF flaw using signals from one type of sensor. Such approaches, which are trained on data from simple cuboid and cylindrical-shaped coupons, have met limited success when used for detecting multiscale flaws in complex LPBF parts. The objective of this work is to develop a heterogenous sensor data fusion …

Pcl And Dmso2 Composites For Bio-Scaffold Materials, Jae-Won Jang, Kyung-Eun Min, Cheolhee Kim, Chien Wern, Sung Yi

Mechanical and Materials Engineering Faculty Publications and Presentations

Polycaprolactone (PCL) has been one of the most popular biomaterials in tissue engineering due to its relatively low melting temperature, excellent thermal stability, and cost-effectiveness. However, its low cell attraction, low elastic modulus, and long-term degradation time have limited its application in a wide range of scaffold studies. Dimethyl sulfone (DMSO2) is a stable and non-hazardous organosulfur compound with low viscosity and high surface tension. PCL and DMSO2 composites may overcome the limitations of PCL as a biomaterial and tailor the properties of biocomposites. In this study, PCL and DMSO2 composites were investigated as a new bio-scaffold material to increase …

Fast-, Light-Cured Scintillating Plastic For 3d-Printing Applications, Brian G. Frandsen, Michael Febbraro, Thomas Ruland, Theodore W. Stephens, Paul A. Hausladen, Juan J. Manfredi, James E. Bevins

Faculty Publications

Additive manufacturing techniques enable a wide range of possibilities for novel radiation detectors spanning simple to highly complex geometries, multi-material composites, and metamaterials that are either impossible or cost prohibitive to produce using conventional methods. The present work identifies a set of promising formulations of photocurable scintillator resins capable of neutron-gamma pulse shape discrimination (PSD) to support the additive manufacturing of fast neutron detectors. The development of these resins utilizes a step-by-step, trial-and-error approach to identify different monomer and cross-linker combinations that meet the requirements for 3D printing followed by a 2-level factorial parameter study to optimize the radiation detection …

Influence Of Dilute Silicon Carbide Nanoparticle Additions To The Microstructure And Mechanical Properties Of Laser Powder Bed Fusion Molybdenum, Nathan E. Ellsworth

Theses and Dissertations

Consolidation of pure molybdenum through laser powder bed fusion and other additive manufacturing techniques is complicated by a high melting temperature, thermal conductivity, and ductile-to-brittle transition temperatures. Nano-sized silicon carbide particles (0.1 wt%) were homogeneously mixed with molybdenum powder and the printing characteristics, chemical composition, microstructure, and mechanical properties were compared to pure molybdenum for scan speeds of 100, 200, 400, and 800 mm/s. The addition of silicon carbide improved the consolidation and mechanical properties and the oxygen content was reduced. Two mechanisms of oxygen reduction were identified as responsible for the improvements: oxidation of free carbon and the creation …

Automated Additive Layering Of Vat Polymerized Plastic Organic Scintillators, Chandler J. Moore

Theses and Dissertations

The current technology for fast neutron detection imaging is limited in achieving the required high spatial resolution, strong neutron discrimination, and practical time of manufacturing. Traditional fabrication methods require days of thermal polymerization and hundreds of man-hours to produce average resolution pixelated scintillator arrays. The present work helps to eliminate this limitation by developing an additive manufacturing technique to construct such detectors for use in in dual particle imaging applications. In this work, fast-, light-curing resins are used in a prototype automated assembly machine, capable of layering of individual light-cured resin layers and optical segmentation with a self-bonded specular reflector, …