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Articles 31 - 60 of 1219
Full-Text Articles in Engineering
Implementation Of A Three-Port Solar Converter With A Battery Energy Storage System, Maison Christopher Phipps
Implementation Of A Three-Port Solar Converter With A Battery Energy Storage System, Maison Christopher Phipps
Graduate Theses and Dissertations
The increasing deployment of distributed solar and energy storage systems has created the need for integrated power converters that can efficiently manage photovoltaic (PV) generation, battery energy storage, and grid-tied AC output. This thesis presents the implementation and validation of a 5kW non-isolated Three-Port Converter (TPC) adapted for residential solar applications. The converter consolidates three power stage into a high-frequency, compact architecture: a unidirectional boost converter for PV input, a bidirectional interleaved buck-boost converter for battery energy storage, and a configurable DC/AC inverter for 120Vac single-phase output. The system is controlled using a central controller implemented on a TI C2000™ …
Design And Optimization Of High-Frequency Medium-Voltage Dual Active Bridge Dc/Dc Converter Using Sic Device, Hui Cao
Graduate Theses and Dissertations
High frequency Dual Active Bridge (DAB) converters have become a key enabling technology in medium- and high-power applications such as renewable energy integration, electric vehicle fast charging, and emerging DC power distribution systems. However, when operating at high power and high frequency, DAB converters face critical challenges including limited soft-switching range, uneven semiconductor loss distribution, deadtime-induced resonance, switching-frequency constraints of wide-bandgap (WBG) devices, and transformer DC bias during dynamic transitions. This dissertation addresses these challenges through advancements in modulation strategies and converter architecture. First, an enhanced triple-phase-shift (E-TPS) modulation scheme is proposed to achieve balanced switching and conduction losses across …
Optical Characterization Of Ge And Gesn Grown In Aspect Ratio Trapping Structures For Enhanced Emitter Performance, Abdulla Said Ali
Optical Characterization Of Ge And Gesn Grown In Aspect Ratio Trapping Structures For Enhanced Emitter Performance, Abdulla Said Ali
Graduate Theses and Dissertations
Silicon (Si) began dominating the electronics industry since 1960s, the dominance came due to its affordability and well developed fabrication processes. But when it comes to light emitting devices and photonics devices in general, the indirect bandgap of Si has caused many scientists to search for alternative semiconductor materials that can deliver better light emission, materials that can also improve wavelengths detection which is also very limited when it comes to Si, reduce losses and greater light amplification, all this while still being affordable. Despite these limitations, Si has been widely used in Complementary Metal Oxide Semiconductor (CMOS) manufacturing and …
Design And Development Of A Multi-Port Solid State Circuit Breaker Based On Half Bridge Sic Mosfets, Yannal Nawafleh
Design And Development Of A Multi-Port Solid State Circuit Breaker Based On Half Bridge Sic Mosfets, Yannal Nawafleh
Graduate Theses and Dissertations
This thesis investigates multi-port solid-state circuit breaker (M-SSCB) architectures that reduce steady-state conduction losses while preserving microsecond-class DC fault interruption and per-port selectivity. The proposed M-SSCB consolidates protection for several node interfaces into a single assembly with shared sensing, control, and a common energy-absorption branch. In normal operation, two electrically symmetric parallel semiconductor paths are established so each port’s current divides approximately in half; because conduction loss scales with current squared, the M-SSCB achieves ≈75% reduction in on-state loss relative to a conventional anti-series SiC path without increasing device count. During fault handling, the coordinated controller detects the local over-current, …
Advanced Membrane Methods For Treatment Of Toxic Contaminants And Education Of Early-Career Researchers, Thomas Mckean Iii
Advanced Membrane Methods For Treatment Of Toxic Contaminants And Education Of Early-Career Researchers, Thomas Mckean Iii
Graduate Theses and Dissertations
Membrane technologies are attractive as they are linearly scalable and often require lower operating costs compared to other technologies. One area where they are particularly effective is the treatment of water contaminated with toxic substances. The simplicity of this removal mechanism provides reliable performance capable of meeting stringent removal requirements. However, membrane fouling is a major challenge that often limits their commercial viability. This research sought to investigate novel approaches to pretreatment and membrane modification to overcome fouling and high operating pressures. In addition, membrane separation processes can often be developed into simple yet educational experiments that are ideal for …
Series Resonant Converters With Medium Voltage Sic Mosfets For Electric Aircraft Applications, Xinyuan Du
Series Resonant Converters With Medium Voltage Sic Mosfets For Electric Aircraft Applications, Xinyuan Du
Graduate Theses and Dissertations
To develop high-performance high- power-density MV power converters, the emerging silicon carbide (SiC) devices are more attractive than their silicon (Si) counterparts, since the fast switch frequency brought by the SiC can effectively reduce the volume and weight of the filter components and thus increase the converter power density. From the converter topology perspective, with the MV dc distribution, the single stage isolated dc/dc converter are suitable for next-generation electric aircraft system due to soft switching and high power density. In this work, comprehensive static and dynamic characterizations were conducted for the latest 6.5 kV silicon carbide (SiC) MOSFETs from …
Design Of Phase Shifter And True Time Delay Gan Mmics For High-Temperature Ku-Band Applications, Michael Lee Thompson
Design Of Phase Shifter And True Time Delay Gan Mmics For High-Temperature Ku-Band Applications, Michael Lee Thompson
Graduate Theses and Dissertations
This thesis presents the design, implementation, and high-temperature characterization of Gallium Nitride (GaN) monolithic microwave integrated circuits (MMICs) developed for beamforming and phased-array systems operating in the Ku-band (12-14 GHz). Two integrated circuits were designed: a 3-bit digital phase shifter and a 3-bit true time delay (TTD), both optimized for high linearity, low insertion loss, low phase error, and stable operation at elevated temperatures up to 300°C. Developing both a phase shifter and a TTD enabled a direct comparison of their beamforming performance and the evaluation of beam squint effects over frequency, a critical factor in wideband array design. The …
Solar Powered Conservation: The Effects Of Solar Photovoltaic Facilities On Avian Community Composition, Michael Christopher Ferrara
Solar Powered Conservation: The Effects Of Solar Photovoltaic Facilities On Avian Community Composition, Michael Christopher Ferrara
Graduate Theses and Dissertations
The expansion of solar photovoltaic energy infrastructure is transforming landscapes worldwide. Increasingly, facilities are planted with native vegetation, yet how vegetation characteristics and landscape variables shape wildlife communities in solar facilities remains poorly understood. Because avian populations have been in decline and are sensitive to habitat changes, understanding how solar facilities influence avian communities is important. In Chapter 1, we used autonomous recording units, local vegetation measurements, and land use and land cover data to quantify how avian community occupancy is influenced by solar cover in solar facilities and comparable reference sites. We used a Bayesian multi-species occupancy model to …
Volume Status Detection With Integral Pulse Frequency Modulation Model Of Peripheral Venous Pressure, Jeremiah Rhys Wimer
Volume Status Detection With Integral Pulse Frequency Modulation Model Of Peripheral Venous Pressure, Jeremiah Rhys Wimer
Graduate Theses and Dissertations
This thesis studies the effectiveness of utilizing a modified integral pulse frequency modulation (IPFM) algorithm to synthesize peripheral venous pressure (PVP) waveforms for the detection of several physiological conditions using logistic regression. PVP waveforms are collected from 18 human patients and 4 porcine subjects. Human data are used to train models for determining the hypovolemic status of the patient, while the porcine data are used to train models for determining level of anesthesia and detecting internal hemorrhaging. In the human dataset, the waveforms collected from the 18 patients are classified into two groups according to serum chloride levels: resuscitated (≥100 …
Unraveling Nucleation Mechanisms In Membrane Distillation: A Molecular Dynamics And Enhanced Sampling Approach, Nazanin Abbasi
Unraveling Nucleation Mechanisms In Membrane Distillation: A Molecular Dynamics And Enhanced Sampling Approach, Nazanin Abbasi
Graduate Theses and Dissertations
Membrane distillation offers a promising route for desalination but remains limited by salt scaling, where mineral crystals nucleate and grow in concentrated brines. To inform strategies that mitigate scaling, this thesis investigates homogeneous nucleation in supersaturated aqueous NaCl solutions using molecular dynamics and enhanced sampling techniques. Several collective variables (CVs) are tested to capture the early stages of ion aggregation and crystal formation, including ion–ion coordination number, dehydration, and bond orientational order parameters Q₄ and Q₆. Enhanced sampling techniques, such as metadynamics and umbrella sampling, are employed to overcome the high free energy barriers associated with the formation of critical …
Extending Touch: Investigating Sensorimotor Integration, Cognitive Workload, And Presence With Neuro-Haptic Feedback In Virtual Reality, Aliyah Khadijah Shell
Extending Touch: Investigating Sensorimotor Integration, Cognitive Workload, And Presence With Neuro-Haptic Feedback In Virtual Reality, Aliyah Khadijah Shell
Graduate Theses and Dissertations
Sensory feedback from the hand is fundamental for the coordination of fine motor skills and overall sensorimotor function. Impaired somatosensation during task execution has been associated with the development of inaccurate motor plans, which can hinder motor learning. Virtual Reality (VR) has emerged as a promising tool for motor rehabilitation; however, most VR-based interventions overlook the critical role of tactile feedback in motor control. The absence of touch feedback, which is integral to conventional rehabilitation and training, may limit the full therapeutic potential of VR. Integrating functionally relevant neurostimulation based haptic feedback (neuro-haptic feedback) into VR-based interventions may enhance functional …
Design And Testing Of A Gallium Nitride Power Amplifier For High-Temperature Radar Applications, Walker Landry Harbison
Design And Testing Of A Gallium Nitride Power Amplifier For High-Temperature Radar Applications, Walker Landry Harbison
Graduate Theses and Dissertations
This thesis offers the design, fabrication, and evaluation of a gallium nitride (GaN) power amplifier integrated circuit (IC) intended for high-temperature radar applications. Radar systems are used in many different applications, such as defense, aerospace, and weather. For their function, these systems require high power, efficiency, and reliability under a wide range of operating conditions. Taking advantage of the material properties of GaN, including its high breakdown voltage, wide bandgap, and thermal conductivity bolstered by the use of silicon carbide in the substrate, this work focuses on examining amplifier performance in both ambient and elevated temperature conditions. The PA was …
Automation And Upgrading Of Custom Cold Wall Uhv-Cvd Reactor For Group Iv Material Development, Alexander Golden
Automation And Upgrading Of Custom Cold Wall Uhv-Cvd Reactor For Group Iv Material Development, Alexander Golden
Graduate Theses and Dissertations
Group IV alloys have shown promising results for infrared optoelectronic applications where III-V materials are currently dominant. The III-V material system has vacancies that Group IV materials can fill, most importantly complementary metal oxide semiconductor (CMOS) process compatibility making quality devices much cheaper and widely available compared to the current state of the art. Silicon, being an indirect band gap Group IV material, has poor performance in optoelectronic applications but is the dominant material for most of the electronic industry. However, when silicon is alloyed or substituted with other group IV materials, these optoelectronic properties can be enhanced and, in …
The Fate Of Intra- And Extracellular Antibiotic Resistance Genes Through Advanced Wastewater Treatment Process, Celestene Adrianne Sebag
The Fate Of Intra- And Extracellular Antibiotic Resistance Genes Through Advanced Wastewater Treatment Process, Celestene Adrianne Sebag
Graduate Theses and Dissertations
More areas across the globe are becoming affected by water stress or water scarcity. The decrease in available freshwater due to overconsumption reveals the direct need to consider other sources for necessities such as drinking water or food production. Agricultural irrigation uses 70% of the world’s freshwater, making the focus on safe and reliable reclaimed water for agricultural reuse imperative. However, contaminants of emerging concern (CECs), such as antibiotics and their resulting antibiotic resistance genes (ARGs), can spread and affect human health if reclaimed water is not treated to the proper level. Antibiotics are widely used in human medicine and …
Switching Performance Optimization Of Sic Mosfets With Digital Active Gate Drivers, Liyang Du
Switching Performance Optimization Of Sic Mosfets With Digital Active Gate Drivers, Liyang Du
Graduate Theses and Dissertations
Silicon carbide (SiC) metal-oxide-semiconductor field-effect transistors (MOSFETs) have extensive applications in high-power density devices, but they exhibit quick switching transients that are problematic, including electromagnetic interference (EMI), voltage overshoot, and current imbalance between paralleled devices. The purpose of this dissertation is to maximize the switching performance of SiC MOSFETs using digital active gate drivers (AGDs). A three-level gate driving approach is presented to improve current sharing in paralleled SiC MOSFETs through turn-on voltage and gate signal delay adjustment. Closed-loop control with real-time feedback ensures high-reliability operation. For better practicability, a compact AGD structure of a single-path Class-B amplifier-based topology is …
Fpga-Based Overlay Accelerators With Massive Parallel Processing Units To Accelerate Deep Neural Networks, Ehsan Kabir
Fpga-Based Overlay Accelerators With Massive Parallel Processing Units To Accelerate Deep Neural Networks, Ehsan Kabir
Graduate Theses and Dissertations
Deep neural networks (DNNs) are widely used in applications such as classification, prediction, and regression. Various DNN architectures, such as convolutional neural networks (CNN), multilayer perceptrons (MLP), long short-term memory (LSTM), recurrent neural networks (RNN), and transformers, have become leading machine learning techniques in these applications. They require significant computational resources and have substantial memory demands due to intensive matrix-matrix multiplications and complex data flows. Hence, efficient utilization of on-chip computational and memory resources is essential to maximize parallelism and minimize latency. Designing an optimal tiling scheme that aligns effectively with the architecture is also necessary. Modern FPGAs are equipped …
Comparative Study On The Long-Term Performance Of Bmd Mixtures Prepared Using Different Sample Preparation Techniques And Superpave Mixtures Under Varying Pavement Structures, Amarjeet Tiwari
Graduate Theses and Dissertations
Asphalt mix design has advanced significantly since the 1930s, with Balanced Mix Design (BMD) emerging to address durability concerns found in the Superpave method by optimizing binder content based on performance criteria. The performance of bituminous mixtures can be assessed through laboratory testing. These tests require proper sample preparation, and various techniques are employed for this purpose. Understanding the differences between these techniques is essential for the successful application of bituminous mixtures in the field. The objective of this study is to assess the differences in the predicted long-term performance of two sample preparation techniques, Lab Mix Lab Compacted (LMLC) …
Analysis And Predictive Modeling Of Stall And Spin Accidents In General Aviation Fixed-Wing Aircraft, Mehedi Hasan
Analysis And Predictive Modeling Of Stall And Spin Accidents In General Aviation Fixed-Wing Aircraft, Mehedi Hasan
Graduate Theses and Dissertations
Stall and spin accidents represent a persistent safety concern in General Aviation, with approximately 41% resulting in fatalities despite their relatively low occurrence. This study analyzes 1,079 General Aviation stall and spin accidents from 2008 to 2023 using the National Transportation Safety Board accident database. Our analysis identified the top phases of flight, injury outcomes, and causal factors in stall/spin accidents. Findings indicate that over 93% of stall/spin events involved General Aviation aircraft, with most accidents occurring during initial climb, takeoff, or low-altitude maneuvering. Pilot-related control errors, especially poor airspeed and angle-of-attack management, were the most common causes. To assess …
Engineered Interfaces For Enhanced Transient Liquid Phase Bonding In Electronics Assembly, John Russell Harris
Engineered Interfaces For Enhanced Transient Liquid Phase Bonding In Electronics Assembly, John Russell Harris
Graduate Theses and Dissertations
Growing applications in transportation make power density a key optimization target in the power electronics industry. More power in a shrinking environment leads to high heat flux and junction temperatures that damage silicon-based switching devices. Temperatures approaching 175℃ can result in false triggering of the device’s activated state, resulting in short circuits. Developing wide bandgap semi-conductors, such as gallium nitride and silicon carbide, are less susceptible to this complication as the energy from elevated temperature is a smaller fraction of what would be required to trigger the device. These devices are projected to function reliably in environments of up to …
Photochemical Fabrication And Tribological Evaluation Of Hexagonal Grooves With Corner Dimples On Cast Iron Surfaces, Steven Sonntag
Photochemical Fabrication And Tribological Evaluation Of Hexagonal Grooves With Corner Dimples On Cast Iron Surfaces, Steven Sonntag
Graduate Theses and Dissertations
The traditional honing process used to texture cylinder liners in internal combustion engines has long been recognized as suboptimal, as evidenced by the need for a break-in period before achieving peak performance. Although laser-based methods can produce micro-scale features with high precision, they are often cost-prohibitive and difficult to scale for large or complex components. This study explores photochemical machining (PCM) as a low-cost, scalable alternative for fabricating high-resolution surface textures—specifically, hexagonal grooves with corner dimples—on gray cast iron. The resulting textures exhibit uniform groove widths (~13 μm) and varied depths, demonstrating PCM’s capability to create high-resolution patterns with sub-micron …
High-Resolution Energy Efficient Selective Laser Sintering Of Copper Nanoparticles, Bo Shen
High-Resolution Energy Efficient Selective Laser Sintering Of Copper Nanoparticles, Bo Shen
Graduate Theses and Dissertations
Copper (Cu) is widely utilized in electronics and photonics applications due to its outstanding electrical and thermal conductivity. With increasing demand for miniaturization and higher precision in modern manufacturing, traditional selective laser sintering (SLS) techniques designed primarily for high-throughput production are becoming insufficient. These conventional methods struggle to deliver the resolution required for micro-scale fabrication and often cause thermal damage to sensitive substrates. Therefore, there is a growing necessity to develop compact and high-resolution laser sintering systems capable of precise microfabrication with minimal thermal influence. This study addresses this challenge by investigating nanosecond pulsed laser sintering as a method to …
Design, Modeling, Control, And Analysis Of A Modular Two-Wheeled Self-Balancing Robotic System, Mishek Jair Musa
Design, Modeling, Control, And Analysis Of A Modular Two-Wheeled Self-Balancing Robotic System, Mishek Jair Musa
Graduate Theses and Dissertations
Two-wheeled self-balancing robots have garnered substantial attention within the realms of research and innovation in academia and industrial settings. In particular, advances in control algorithms, machine learning, reinforcement learning, and sensor technologies have played a pivotal role in their development. Although primarily recognized for their utility in personal transportation in the commercial sector, these robots possess potential applications across various domains, including search and rescue, healthcare, material handling, logistics, etc., due to their active stabilization and exceptional maneuvering capabilities. A particular area of interest lies in the creation of modular self-balancing robots designed for seamless reconfiguration and enhanced human interaction. …
Controlling Electroless Deposition On Polymer Interfaces Towards Discrete Functional Particle Synthesis, Grecia Pierina Alvarado Munoz
Controlling Electroless Deposition On Polymer Interfaces Towards Discrete Functional Particle Synthesis, Grecia Pierina Alvarado Munoz
Graduate Theses and Dissertations
Electroless deposition is a process that facilitates the formation of metal layers on surfaces through the reduction of metal ions onto a surface in the presence of a sacrificial reducing agent. This process can be applied to synthesize conductive metal layers on insulators such as glass or polymers. The kinetics of heterogeneous deposition depend on the interfacial surface chemistry, including the presence of added catalyst materials, as well as the bulk chemical environment, such as the concentration of metal ions and sacrificial reductants. Furthermore, the homogeneous formation of metal nanoparticles may compete with the deposition reaction, adversely affecting the control …
Growth And Characterization Of Thin Film Gase On Si(111) And Sio2/Si(001) Substrates By Molecular Beam Epitaxy, Christopher John Hocevar
Growth And Characterization Of Thin Film Gase On Si(111) And Sio2/Si(001) Substrates By Molecular Beam Epitaxy, Christopher John Hocevar
Graduate Theses and Dissertations
Gallium selenide (GaSe) is a thin-film semiconducting material with promising optoelectronic properties, including a tunable bandgap, high photosensitivity, and atomic-layer scalability. These characteristics make it suitable for devices such as photodiodes, FETs, MOSFETs, Hall effect sensors, and p–n diodes. In this study, GaSe thin films were grown on SiO2 and Si(111)-7×7 substrates using molecular beam epitaxy (MBE) to compare growth behavior across different substrates. The films were characterized using Raman spectroscopy, X-ray diffraction (XRD), atomic force microscopy (AFM), photoluminescence (PL) spectroscopy, and reflection high-energy electron diffraction (RHEED). RHEED confirmed the 7×7 reconstruction of the Si(111) surface and the amorphous nature …
Design And Validation Of A High-Frequency Multi-Output Dc-Dc Converter For Radar Power Applications, Tory Sutton
Design And Validation Of A High-Frequency Multi-Output Dc-Dc Converter For Radar Power Applications, Tory Sutton
Graduate Theses and Dissertations
Modern radar systems and advanced electronics demand compact, efficient, and reliable power solutions capable of delivering multiple tightly regulated voltage rails under strict size, weight, power, and reliability (SWaP-R) constraints. This thesis presents the design, implementation, and validation of a high-frequency (460 kHz – 1 MHz), multi-output DC-DC converter for a mission?critical radar platform, addressing both integration and performance requirements. The first implementation, an isolated modular converter (IMC), utilizes isolated silicon?based DC-DC modules to deliver twelve isolated voltage outputs from a single input. This approach provided robust electrical isolation, simplified system integration, and minimized design risk, making it well-suited for …
Polymer-Enhanced Nanopore Sensing, Eugene Gyasi Agyemang
Polymer-Enhanced Nanopore Sensing, Eugene Gyasi Agyemang
Graduate Theses and Dissertations
The resistive pulse technique characterizes single analytes by detecting fluctuations in the ion current as they pass through a narrow orifice connecting two electrolyte-filled chambers, each containing a single electrode. The amplitude, shape, frequency, and duration of these fluctuations primarily provide information about the analyte’s size, shape, concentration, and net surface charge, respectively. One configuration for resistive pulse measurements is of an electrolyte-filled nanopipette immersed in a bath, where the nanopipette tip acts as the nanoscale orifice. It was previously shown that incorporating the large quantities polymer polyethylene glycol (PEG 8K, 50% w/v) into the external electrolyte bath dramatically enhanced …
Synthesis, Structural Characterization And Optical Studies Of Silver-Indium-(Zinc)-Chalcogenide Fluorescent Quantum Dots, Sujal Acharya
Synthesis, Structural Characterization And Optical Studies Of Silver-Indium-(Zinc)-Chalcogenide Fluorescent Quantum Dots, Sujal Acharya
Graduate Theses and Dissertations
Developing a non-toxic, high-performance fluorescent nanomaterial is crucial for overcoming the environmental and health restrictions of current cadmium, and lead based quantum dots (QDs), which limit the application of quantum dots in optoelectronics and bioimaging. In this thesis, we synthesized environmentally friendly AgInS2 QDs by a colloidal method, systematically altering the In/Ag precursor ratio from 2 to 6 to study the impact on their optical and photophysical properties. Our goals were to find the optimal stoichiometry for maximum quantum efficiency and stability. We also investigated further improving optical and photophysical properties through shelling with ZnS. The emission spectra appeared broad, …
Simulation- And Machine Learning-Based Methods For Inland Waterway Operation And Maintenance Decision-Making, Maryam Aghamohammadghasem
Simulation- And Machine Learning-Based Methods For Inland Waterway Operation And Maintenance Decision-Making, Maryam Aghamohammadghasem
Graduate Theses and Dissertations
The U.S. inland waterway transportation system (IWTS) is an essential part of the country's multimodal freight transportation network. In addition to seasonal droughts and floods, the operations of the IWTS may be disrupted by random malfunctions and scheduled maintenance of its critical components. Among these critical components, locks play a key role in the operation of navigable inland waterways, and lock-induced disruptions to the supply chains of related industries, such as agriculture and manufacturing, often result in significant economic losses. To assess the performance of the U.S. IWTS, we develop a PyNetLogo simulation tool to capture the movements and delays …
Effect Of Beam Bracing On The Seismic Performance Of Laterally Skewed Reduced Beam Section Moment Connections With Composite Concrete Slabs, Pratik Ghimire
Effect Of Beam Bracing On The Seismic Performance Of Laterally Skewed Reduced Beam Section Moment Connections With Composite Concrete Slabs, Pratik Ghimire
Graduate Theses and Dissertations
Existing experimental reduced beam section (RBS) moment frame investigations, particularly those used for prequalification in AISC-358, consider orthogonally oriented beam-to-column connections. While the design commentary provided in AISC-358 references recent skewed SMF numerical studies and potential performance effects when a lateral beam skew is introduced, limited experimental studies have been performed to verify the numerical findings. This study presents an experimental investigation into the cyclic behavior of RBS special moment frames that have lateral skew at the beam-to-column connection and composite concrete slabs. In this study, a skewed composite double-sided RBS connection is tested, having beam bracing outside the RBS …
Novel Atomic Layer Deposition Processes Of Silver For Battery Applications, Darlington Ehijie Imhanzuaria
Novel Atomic Layer Deposition Processes Of Silver For Battery Applications, Darlington Ehijie Imhanzuaria
Graduate Theses and Dissertations
This thesis presents a novel approach to enhance the performance and stability of anode-free lithium-ion batteries (AFLBs) by employing atomic layer deposition (ALD) to coat copper (Cu) current collectors with a silver-aluminum oxide (AgAlOx) layer. Leveraging the unique capabilities of ALD for precise and conformal deposition, the AgAlOx coating was achieved using triethyl phosphine-(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato)-silver(I) (Ag(fod)(PEt3)), trimethylaluminum (TMA), and de-ionized water (H2O) as precursors. This innovative coating method significantly enhanced the cycling stability and Coulombic efficiency (CE) of both Li||Cu and Cu||NMC811 cells, as evidenced by improved electrochemical performance metrics. The AgAlOx layer …