Mechanics of Materials Commons^™

Powder Degradation Analysis In Reused Pure Tungsten For Electron Beam Melting (Ebm), Hernan Valenzuela

Open Access Theses & Dissertations

Additive manufacturing (AM) enables unparalleled design freedom and geometric complexity, driving its adoption in aerospace and medical fields. A major advantage of metal powder AM technologies, such as Electron Beam Melting (EBM), is its ability to reuse unused metal powder, reducing material waste and costs. However, reusing powder repeatedly alters its properties, affecting the final product. Despite its significance, research on powder degradation remains limited, primarily focusing on alloys like Ti-6Al-4V. This thesis investigates the degradation of pure tungsten powder reused over multiple Electron Beam Melting (EBM) cycles. A literature review revealed general powder-reuse mechanisms across additive manufacturing (AM) technologies …

Coupling Material Formulation Strategies To Tailor Piezoelectric Properties Of Ceramic Lattices, Amanda Lauren Borgaro

Open Access Theses & Dissertations

This thesis examines the material formulation and infiltration processes required to create interpenetrating ceramic composites with a particular focus on developing piezoelectric ceramic-epoxy lattice structures (PCELS). Following this, a high–solid loading barium titanite photopolymer resin (BT40) was developed to produce BTO scaffolds with controlled porosity suitable for metal infusion. The resin’s shear-thinning behavior and scattering-dominated curing response enabled the formation of stable, uniform ceramic structures whose pore networks directly influence infiltration behavior. Building on this foundation, a low-temperature Field’s Metal (FM) infiltration method was established using controlled thermal equilibration and the melting of pre-formed alloy rods. By maintaining the ceramic …

Development Of Oxide And Oxynitride Thin Films For Advanced Optical Applications, Nathan Christopher Episcopo

Open Access Theses & Dissertations

To develop Ga2O3 and TiOₓNᵧ thin films for optical applications, the process–structure–properties relationship was investigated using a comprehensive set of characterization techniques to establish the atomic structure and composition of the films in relation to the deposition conditions. The results provide critical insights into how deposition parameters influence the atomic structure and composition during magnetron sputtering. Furthermore, the correlation between atomic structure and composition with the optical and electrical properties of the films was examined to determine how variations in these factors affect functional performance. Collectively, these findings offer the necessary information to target desirable optical properties for Ga2O3 and …

Microstructure Evolution During Annealing Of Cryogenically Processed Cantor High Entropy Alloy, Mynel Gomez

Open Access Theses & Dissertations

This work focuses on the annealing behavior of a cryogenically processed Cantor high entropy alloy over a wide temperature range of 500–800°C. Scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), X-ray diffraction (XRD), and transmission electron microscopy (TEM) were employed to analyze the microstructural evolution, with particular emphasis on twinning. Hardness and grain size were measured to correlate these microstructural changes with mechanical properties. The cryogenically processed alloy exhibited a high density of twin bundles, resulting in an initial hardness of 338 HV. Upon annealing at 500 °C, 550 °C, and 600 °C, the material showed only a limited degree …

Decoupling Piezoelectric And Pyroelectric Effects In Anisotropic Polymer-Ceramic Lattices Produced Via Fused Filament Fabrication, Sofia Alexandra Perez

Open Access Theses & Dissertations

This thesis investigates how multi-material fused filament fabrication (FFF) can be used to engineer lattice structures that decouple piezoelectric and pyroelectric responses within a single polymer–ceramic composite. A hybrid ABS–BaTiO3/PLA lattice—referred to as the Hybrid PIZCAL—was designed to direct mechanical strain along the Z-axis while suppressing deformation in the transverse directions. After thermal poling, the lattice exhibited a 293% increase in Z-axis voltage sensitivity compared to a monolithic ABS–BaTiO3 cube and significantly reduced off-axis electromechanical output. Finite element simulations and directional compression testing confirmed that geometric anisotropy and material zoning produce strong, axis-selective piezoelectric behavior. The second part of this …

Characterization Of The Fatigue Threshold Behavior Of Uhmwpe, Bethany B. Smith, Anurag Roy, Robert O. Ritchie, Lisa A. Pruitt

Faculty Journal Articles

Ultra-high-molecular-weight-polyethylene (UHMWPE) has been the material of choice for bearings in total joint replacements (TJRs) for decades as a result of its excellent wear resistance, chemical inertness, energetic toughness, low friction, and biocompatibility. Utilization of this polymer in orthopedic devices requires oxidation, wear, and fatigue resistance. Balancing these important properties by tailoring processing techniques and modulating microstructural features has been an ongoing endeavor in the field. Research into the clinical applications of UHMWPE has primarily focused on the challenges of wear and oxidation while studies into the realm of fatigue have been more limited. Literature gaps exist in fully understanding …

Investigations On The Fatigue Strength Of Threads Produced By Different Fabrication Techniques, Philippe Du Maire, Jürgen Hoffmeister, Andreas Öchsner, Michael Johlitz

15th International Conference on Shot Peening

The increasing importance of sustainability in engineering demands the development of long-lasting, high-performance components that reduce material and energy consumption over time. This study investigates how different thread manufacturing processes, i.e., cutting, rolling, and deep rolling, affect the fatigue strength of bolts made from 42CrMo4+QT steel. Cylindrical specimens with M12 threads were subjected to cyclic tensile loading with constant mean stress. Fatigue strength was evaluated using the staircase method, and supporting analyses included X-ray diffraction for residual stress, and full width half maximum examination and Vickers microhardness measurements. Results show that thread rolling significantly improves fatigue strength, achieving 113.8 MPa …

Enhancing The Fatigue Strength Of Am Materials Via Mechanical Surface Treatment, Fabian Keil, Jan Schubnell, Sascha Fliegener, Alexander Heiss

15th International Conference on Shot Peening

Additive manufacturing (AM) processes, while enabling the production of intricate geometries, frequently result in suboptimal surface quality, which can significantly restrict the fatigue strength of components when compared to those manufactured using traditional methods. This study explores the effectiveness of mechanical surface treatment (MST) techniques, specifically shot peening and deep rolling, in enhancing the fatigue performance of additively manufactured AlSi10Mg and 316L alloys. A combination of experimental investigations and finite element simulations was employed to evaluate the influence of these treatments on surface integrity, microstructure, and fatigue life. The results reveal that both MST approaches lead to substantial improvements in …

Expansion Of Laser Peening Application With A High-Power Microchip Laser On A Robotic Arm, Yuji Sano, Yoshio Mizuta, Satoshi Tamaki, Tomonao Hosokai, Tomoharu Kato, Yoshihiro Sakino, Volker Schneidau, Sebastian Holz, Jörg Behler

15th International Conference on Shot Peening

Laser peening (LP) introduces compressive residual stress (RS) onto the surface of metallic materials using nanosecond laser pulses irradiated through a water layer, thereby effectively suppressing fatigue crack initiation. However, conventional LP systems require large, stationary setups, restricting their use to indoor environments. To overcome this limitation, a portable LP device featuring a finger-sized microchip laser mounted on a collaborative robot arm has been developed. Equipped with a compact power supply and a water circulation/recovery system, the device can operate on-site with minimal setup. Successful processing across various materials has confirmed both compressive RS induction and fatigue life extension. Notably, …

Effects Of Laser Peening On Fatigue Properties Of Welded Aluminum Thin Plates, Kiyotaka Masaki, Yoshio Mizuta, Satoshi Tamaki, Yuji Sano

15th International Conference on Shot Peening

To improve the fatigue properties of welded aluminum alloy thin plates used in transportation machinery, handheld laser peening (HH-LP) was applied to 2 mm-thick A5083-O specimens prepared by bead-on TIG welding. Conventional laser peening often causes warping in thin plates, but the HH-LP treatment using low-energy laser pulses avoids this problem. The HH-LP treatment introduced compressive residual stresses of over 200 MPa on the heat-affected zone (HAZ) of the welded specimens. Fatigue tests under plane bending conditions revealed that the HH-LP treatment significantly improved the fatigue strength of the welded specimens, achieving a level comparable to that of the base …

Experimental And Numerical Investigation On The Effect Of Projectile Mass And Apex Angle On Penetration Depth Into Sandy Soils, Abdul-Rahman K. Osman, Ahmed Elshesheny Dr, Mohamed S. Zahran Dr, Nabil M. Nagy Prof.

Journal of Engineering Research

Projectile penetration in granular soils remains a critical concern in defense engineering and ballistics research. This study presents an experimental and numerical investigation of rigid cone-tip projectile penetration into very dense sand, examining the influence of apex angle and projectile weight on penetration depth. Laboratory experiments were conducted using metallic projectiles with apex angles of 10°, 30°, 60°, and 90° and weights of 2.445, 3.87, 5.33, and 6.81 kg, dropped from a height of 4.295 m into a 500×500×500 mm wooden tank filled with sand to 400 mm height at 95% relative density. Through systematic testing, two empirical correlation …

Tensile Creep Of A Hybrid Polymer-Matrix/Ceramic-Matrix Composite At Elevated Temperature, Waleed S. Alshehri

Theses and Dissertations

Advanced aerospace systems require structural materials that can perform reliably in high-temperature environments for long durations. The performance of standard polymer matrix composites (PMCs) in these conditions is often limited by their susceptibility to time-dependent deformation, such as creep. The objective of this research is to characterize the high-temperature creep behavior of a novel unitized material system comprising a polymer matrix composite (PMC) and a ceramic matrix composite (CMC) co-cured together. The PMC part consists of the polyimide matrix reinforced with laminated carbon fibers woven in an eight harness satin weave (8HSW). The CMC part consists of a zirconia-based ceramic …

Mechanical Characterization Of M Plane (10-10) And C Plane (0001) Gallium Nitride Semiconductors Via Spherical Nanoindentation, Daniela Alejandra Duarte

Open Access Theses & Dissertations

Gallium nitride's (GaN) mechanical characterization is essential for evaluating its performance and long-term dependability, especially when subjected to mechanical stress and irradiation. The design and optimization of GaN-based devices, which are extensively employed in high-power electronics and optoelectronics, depend on an understanding of these characteristics. Mechanical characterization allows for the evaluation of key characteristics, including stress distributions, representing the spatial variation of internal stresses under applied loading, and pop-in events, which correspond to abrupt displacements associated with the onset of dislocation nucleation and slip. These features are essential for understanding the anisotropic (direction-dependent) response of the material to external forces …

Application Of Distributed Fiber Optic Sensing (Dfos) For Monitoring Asphalt Pavement Strains Under Accelerated Loading Conditions, Sebastian Morales

Open Access Theses & Dissertations

This thesis presents a study on the application of Distributed Fiber Optic Sensing (DFOS) technology for detecting pavement's strain response with high spatial resolution. Using a Rayleigh-based optical frequency domain reflectometry (OFDR) system, DFOS sensors were calibrated and embedded in full-scale asphalt slabs subjected to accelerated loading using a Model Mobile Load Simulator 3 (MMLS3). Calibration of the DFOS sensors was conducted using a three-point bending flexural test with known load conditions and reference strain gauges to validate theoretical and numerical models. The results demonstrate DFOS's capability to detect pavement response under static and dynamic loading, as well as changes …

Laser Scan Path Design For Controlled Microstructure In Additive Manufacturing With Integrated Reduced-Order Phase-Field Modeling And Deep Reinforcement Learning, Augustine Twumasi

Open Access Theses & Dissertations

Laser Powder Bed Fusion (L-PBF) is a well-established additive manufacturing technique for fabricating intricate metal components with exceptional precision. A significant challenge in L-PBF is the formation of complex microstructures that influence final material properties. We propose a physics-guided, machine learning-aided approach to optimize scan paths for desired microstructure outcomes, such as equiaxed grains. We employed a phase-field method (PFM) to model the evolution of the crystalline grain structure. To reduce computational costs, we trained a surrogate machine learning model, a 3D U-Net convolutional neural network, using single-track phase-field simulations with varying laser powers to predict crystalline grain orientations based …

Shape Memory Behavior In Medium To High Entropy Shape Memory Alloys: Design, Prediction, And Experimental Analysis, Hatim Raji

Theses and Dissertations

This dissertation provides a data-driven system integrating synthetic data generation and machine learning (ML) techniques to create multicomponent SMA compositions with specific transformation temperatures (TTs). Models were trained to represent the nonlinear dependencies influencing martensitic transformation behavior by using elemental, thermodynamic, and process-related aspects. The capacity of the ML models on medium entropy NiTiHfPd and high entropy NiTiHfZrCu systems accuracy was confirmed by experimental validation showing TTs closely matched with model outputs.

Advancing Multi-Physics Modeling For Microwave Heating: Application In Micro-Reactor Design And Optimization, Raghav Adhikari

All Theses

Microreactors are a type of small-scale chemical reactors for achieving reduced volume, improved product selectivity and higher reaction rate. It allows precise temperature control, which is crucial for sensitive chemical processes. Microreactors can be employed as key components of conducting small-scale reactions with improved reactor configuration and process efficiency. It is important to identify a localized and precise heating mechanism to trigger and control the corresponding chemical reactions.

In fact, microwave heating has gathered significant attention in recent years due to its ability to deliver efficient, rapid, and localized heating, which can accelerate reaction rates and enhances the reaction selectivity. …

Mno2 Nanoscale Interface Modification, Alexander C. Skoppe

Doctoral Dissertations and Master's Theses

Interface modification of carbon fibers has been shown to improve the mechanical performance of composites. In addition, interface modification of carbon fiber composites can impart multifunctionality into the resulting composite. This work will explore ZnO and MnO2 as interface modifications for use on carbon fibers. When exposed to high temperatures, carbon fibers undergo fiber degradation, leading to the need for low-temperature hydrothermal processes. This work will develop and characterize a nanoscale ZnO and MnO2 interface modification for use on carbon fibers. These nanomodifications will be developed with low-temperature processes, minimizing the fiber degradation that the fibers undergo. Fourier transform infrared …

Advanced Study Of Nickel-Titanium Alloy: Effects Of Point Defects On Mechanical And Thermodynamic Properties, Diego Armando Juarez Rosales

Open Access Theses & Dissertations

High-throughput first-principles calculations of point defects are emerging as a powerful tool to accelerate materials discovery in applications [1]. Substitutional, antisite, and vacancy defects can play an important role in the mechanical and thermal properties of intermetallic alloys [2]. In this present work I compute the thermal and mechanical properties of shape-memory alloy nickel-titaniun (NiTi) in the B19â?? martensitic and B2 austenitic phases from molecular dynamics (MD), using a second nearest neighbor (2NN) modified embedded atom method (MEAM) [3] classical potential in the temperature range from 200K to 600K and composition range from 45 atomic percent to 55 atomic percent …

Comparative Study Of Experimental And Fea Strain Data For Cnt-Coated Fiberglass Sensors, Extensometers, And Metal Foil Strain Gauges, Omar Dwidar

Master's Theses

Material testing is essential across industries such as aerospace, automotive, and construction, playing a critical role in verifying material selection, diagnosing failures, and understanding the development of flaws in structures. These insights are key to designing successful, reliable systems. Conventional metal foil strain gauges are low cost and reliable but provide limited sensitivity with a typical gauge factor around 2. Extensometers provide highly sensitive strain measurements with the disadvantage of a bulky form factor. With advanced materials such as carbon nanotubes, it is possible to manufacture a sensor with the sensitivity closer to that of an extensometer with the small …