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Grinding And Super-Finishing Test Machine Project, Michael Simon Jan 2022

Grinding And Super-Finishing Test Machine Project, Michael Simon

Williams Honors College, Honors Research Projects

A research project in The University of Akron to study grinding and super-finishing of silicon nitride ceramic was initiated by Dr. Siamak Farhad and sponsored by the Timken Company, with the assistance of undergraduate students Michael Simon, Ryan Hosso and Mathew Rozmajzl. The study required analysis of forces and scratches generated during grinding processes of silicon nitride samples. A testing assembly was designed and constructed to record the forces generated during grinding and super-finishing of silicon nitride samples in a computer-numerical-control machine. Silicon nitride samples were subjected to desired grinding and super-finishing operations and all forces generated during the process …


First-Principles Studies Of Anion Engineering In Functional Ceramics, Steven Timothy Hartman May 2020

First-Principles Studies Of Anion Engineering In Functional Ceramics, Steven Timothy Hartman

McKelvey School of Engineering Theses & Dissertations

Ceramic materials display a wide variety of valuable properties, such as ferroelectricity, superconductivity, and magnetic ordering, due to the partially covalent bonds which connect the cations and anions. While many breakthroughs have been made by mixing multiple cations on a sublattice, the equivalent mixed-anion ceramics have not received nearly as much attention, despite the key role the anion plays in the materials’ properties. There is great potential for functional ceramics design using anion engineering, which aims to tune the materials properties by adding and removing different types of anions in existing classes of ceramic materials. In this dissertation, I present …


Microstructure And Mechanical Properties Of Nanofiller Reinforced Tantalum-Niobium Carbide Formed By Spark Plasma Sintering, Christopher Charles Rudolf May 2016

Microstructure And Mechanical Properties Of Nanofiller Reinforced Tantalum-Niobium Carbide Formed By Spark Plasma Sintering, Christopher Charles Rudolf

FIU Electronic Theses and Dissertations

Ultra high temperature ceramics (UHTC) are candidate materials for high temperature applications such as leading edges for hypersonic flight vehicles, thermal protection systems for spacecraft, and rocket nozzle throat inserts due to their extremely high melting points. Tantalum and Niobium Carbide (TaC and NbC), with melting points of 3950°C and 3600°C, respectively, have high resistivity to chemical attack, making them ideal candidates for the harsh environments UHTCs are to be used in. The major setbacks to the implementation of UHTC materials for these applications are the difficulty in consolidating to full density as well as their low fracture toughness. In …


Fabricating Complex-Shaped Components By Room-Temperature Injection Molding Of Aqueous Ceramic Suspension Gels, Valerie Lynn Wiesner Oct 2013

Fabricating Complex-Shaped Components By Room-Temperature Injection Molding Of Aqueous Ceramic Suspension Gels, Valerie Lynn Wiesner

Open Access Dissertations

Water-based ceramic suspension gels (CeraSGels) effectively produced dense, near-net shape ceramic parts by room-temperature injection molding, a novel processing method based on traditional ceramic injection molding. This alternative method eliminated the need for heating and cooling feedstocks to process, as is required in conventional injection molding, through control of the rheological response of the CeraSGels by simply varying polymer content without the use of any harsh crosslinking or curing agents or further chemical processes. The development of room-temperature injection molding initially focused on forming CeraSGels based on alumina, a readily available model material, in order to optimize suspension preparation and …


Oxidation Of Borides And Carbides With Y2o3 And Ta Additions, Salvador Manuel Rodriguez Jan 2012

Oxidation Of Borides And Carbides With Y2o3 And Ta Additions, Salvador Manuel Rodriguez

Open Access Theses & Dissertations

The study presented here describes an investigation of an oxidation scale of a fully-sintered Y2O3-ZrB2-TiC composite exposed in air at 1173K. Upon oxidation of the boride/carbide, a ZrO2-TiO2 was expected to form similar to the ZrO2-SiO2 dual scale of an oxidized ZrB2-SiC. The 47wt% Y2O3-38wt%ZrB2-16wt%TiC composite formed a dual scale consisting primarily of an Y2O3-ZrO2-TiC inner scale with an outer scale of ZrO2-TiO2-Y2O3.

The samples oxidized with a parabolic layer growth allowing the calculation of the effective diffusion coefficient indicating that the oxidation was controlled by oxygen ingress through primarily the ZrO2-Y2O3 phase. The oxygen potential between the inner layer …