Engineering Physics Commons^™

Optical Cell For Combinatorial In Situ Raman Spectroscopic Measurements Of Hydrogen Storage Materials At High Pressures And Temperatures, Jason R. Hattrick-Simpers, Wilbur S. Hurst, Sesha S. Srinivasan, James E. Maslar

Faculty Publications

An optical cell is described for high-throughput backscattering Raman spectroscopic measurements of hydrogen storagematerials at pressures up to 10 MPa and temperatures up to 823 K. High throughput is obtained by employing a 60 mm diameter × 9 mm thick sapphire window, with a corresponding 50 mm diameter unobstructed optical aperture. To reproducibly seal this relatively large window to the cell body at elevated temperatures and pressures, a gold o-ring is employed. The sample holder-to-window distance is adjustable, making this cell design compatible with optical measurement systems incorporating lenses of significantly different focal lengths, e.g., microscope objectives and single element …

Strain Energy And Lateral Friction Force Distributions Of Carbon Nanotubes Manipulated Into Shapes By Atomic Force Microscopy, Mark C. Strus, Roya R. Lahiji, Pablo Ares, Vincente Lopez, Arvind Raman, Ron R. Reifenberger

Other Nanotechnology Publications

The interplay between local mechanical strain energy and lateral frictional forces determines the shape of carbon nanotubes on substrates. In turn, because of its nanometer-size diameter, the shape of a carbon nanotube strongly influences its local electronic, chemical, and mechanical properties. Few, if any, methods exist for resolving the strain energy and static frictional forces along the length of a deformed nanotube supported on a substrate. We present a method using nonlinear elastic rod theory in which we compute the flexural strain energy and static frictional forces along the length of single walled carbon nanotubes (SWCNTs) manipulated into various shapes …

Pressure-Driven Transport Of Particles Through A Converging-Diverging Microchannel, Ye Ai, Sang W. Joo, Yingtao Jiang, Xiangchun Xuan, Shizhi Qian

Mechanical Engineering Faculty Research

Pressure-driven transport of particles through a symmetric converging-diverging microchannel is studied by solving a coupled nonlinear system, which is composed of the Navier–Stokes and continuity equations using the arbitrary Lagrangian–Eulerian finite-element technique. The predicted particle translation is in good agreement with existing experimental observations. The effects of pressure gradient, particle size, channel geometry, and a particle’s initial location on the particle transport are investigated. The pressure gradient has no effect on the ratio of the translational velocity of particles through a converging-diverging channel to that in the upstream straight channel. Particles are generally accelerated in the converging region and then …

Predicting The Hydrogen Pressure To Achieve Ultralow Friction And Diamondlike Carbon Surfaces From First Principles, Haibo Guo, Yue Qi, Xiaodong Li

Faculty Publications

Hydrogen atmosphere can significantly change the tribological behavior at diamond and diamondlike carbon (DLC) surfaces and the friction-reducing effect depends on the partial pressure of hydrogen. We combined density functional theory modeling and thermodynamic quantities to predict the equilibrium partial pressures of hydrogen at temperature T, P_H2 (T), for a fully atomic hydrogen passivated diamondsurface. Above the equilibrium P_H2 (T), ultralow friction can be achieved at diamond and DLC surfaces. The calculation agrees well with friction tests at various testing conditions. We also show that P_H2 (T) …

Performance Comparison Of Pb(Zr0.52Ti0.48)O3-Only And Pb(Zr0.52Ti0.48)O3-On-Silicon Resonators, Hengky Chandrahalim, Sunil A. Bhave, Ronald G. Polcawich, Jeff Pulskamp, Dan Judy, Roger Kaul, Madan Dubey

Faculty Publications

This paper provides a quantitative comparison and explores the design space of lead zirconium titanate (PZT)–only and PZT-on-silicon length-extensional mode resonators for incorporation into radio frequency microelectromechanical system filters and oscillators. We experimentally measured the correlation of motional impedance (R_X) and quality factor (Q) with the resonators’ silicon layer thickness (t_Si). For identical lateral dimensions and PZT-layer thicknesses (t_PZT), the PZT-on-silicon resonator has higher resonant frequency (f_C), higher Q (5100 versus 140), lower R_X (51 Ω versus 205 Ω), and better linearity [third-order input intercept …

). Size Dependency Of The Elastic Modulus Of Zno Nanowires: Surface Stress Effect, Guofeng Wang, Xiaodong Li

Faculty Publications

Relation between the elastic modulus and the diameter (D) of ZnOnanowires was elucidated using a model with the calculated ZnOsurface stresses as input. We predict for ZnOnanowires due to surface stress effect: (1) when D>20nm, the elastic modulus would be lower than the bulk modulus and decrease with the decreasing diameter, (2) when 20nm>D>2nm, the nanowires with a longer length and a wurtzite crystal structure could be mechanically unstable, and (3) when D<2nm, the elastic modulus would be higher than that of the bulk value and increase with a decrease in nanowire diameter.

Nanoindentation Of The A And C Domains In A Tetragonal Batio3 Single Crystal, Young-Bae Park, Matthew J. Dicken, Zhi-Hui Xu, Xiaodong Li

Faculty Publications

Nanoindentation in conjunction with piezoresponse force microscopy was used to study domain switching and to measure the mechanical properties of individual ferroelectric domains in a tetragonal BaTiO₃ single crystal. It was found that nanoindentation has induced local domain switching; the a and c domains of BaTiO₃ have different elastic moduli but similar hardness.Nanoindentationmodulus mapping on the a and c domains further confirmed such difference in elasticity. Finite element modeling was used to simulate the von Mises stress and plastic strain profiles of the indentations on both a and c domains, which introduces a much higher stress level than …

Self-Assembled Composite Nano-/Micronecklaces With Sio2 Beads In Boron Strings, Hai Ni, Xiaodong Li

Faculty Publications

Nano-/micronecklaces with SiO₂ beads in boron strings were synthesized by simply sublimating the desired powders in a sealed quartz tube at high temperature. The boron strings have a rectangular cross section with width varying from 80to1000nm while the SiO₂ beads bear either spindle or spherical shape with a size ranging from 100nmto5μm. The spacing between the SiO₂ beads is uniform in each boron string. Both the boron strings and the SiO₂ beads are amorphous and free of defects. The supersaturated vapors of silicon and oxygen induced the SiO₂ bead formation.

Design And Fabrication Of A Prototype Fabry-Perot Cavity For The Compton Polarimeter Upgrade At Jefferson Lab, Deepa Deepa

Mechanical & Aerospace Engineering Theses & Dissertations

Upcoming experiments at Hall A at Jefferson lab require 1 % absolute accuracy of the electron beam polarization measurement at 0.85 Ge V energy. The Compton polarimeter at Hall A is capable of measuring beam polarization with 3 - 4 % accuracies at this beam energy. Hence it was proposed to upgrade the present Compton by doubling the laser frequency [2]. The present Compton polarimeter operates with a 1064 nm, continuous wave laser at 200 mW. This power is enhanced to 1.5 kW using a 0.85 m long Fabry-Perot Cavity. Changing to 532 nm laser with the same power would …

Material Evaluation By Pulsed Diode Laser Optoacoustics, Xiaodong Xu

Electrical & Computer Engineering Theses & Dissertations

Pulsed diode laser optoacoustic diagnostics were carried out to characterize solid sample materials. The apparatus developed is compact, portable, cost-effective and therefore very promising for both industrial as well as laboratory applications. To our knowledge, this is the first time that optoacoustic characterization and measurement have been performed with a diode laser. The method was successfully applied to measure the thickness of a multilayer structure non-intrusively. Internal cracks of the material were detected by this technique.

A theory for optoacoustic signal generation, propagation and detection is given. A numerical analysis technique is developed to solve for the expected signal. In …

Optimal Active And Passive Control Design For A Slewing Piezoelectric Laminate Beam, Travis V. Dubois

Mechanical & Aerospace Engineering Theses & Dissertations

This thesis presents the development and experimental verification of a distributed parameter model for a slewing beam system with piezoelectric actuators and sensors. Also presented is the development of an optimal active control synergism which employs IMSC, (Independent Modal Space Control) and an optimally designed, viscoelastic damping treatment. The beam is pinned at the proximal end and patches of thin piezoelectric laminates are attached to its surface. Formulation is general enough to allow the patches to be located anywhere on the beam's surface. A viscoelastic material with a constraining layer covers the rest of the beam. The differential equation of …

A Magnetic Suspension System With A Large Angular Range, Colin P. Britcher, Mehran Ghofrani

Mechanical & Aerospace Engineering Faculty Publications

In order to explore and develop technology required for the magnetic suspension of objects over large ranges of orientation, a small-scale laboratory system, the large-angle magnetic suspension test fixture (LAMSTF) has been constructed at NASA Langley Research Center. This apparatus falls into the category of large-gap, actively stabilized magnetic levitation systems. The hardware comprises five conventional electromagnets in a circular arrangement, each driven from a separate bipolar power amplifier. Electromagnet currents are commanded by a digital control system, implemented on a microcomputer, which in turn derives the position and attitude of the suspended element from an infrared optical system. The …

An Apparatus For Measuring The Thermal Conductivity Of Cast Insulation Materials, Christine A. Wilkins, Robert L. Ash

Mechanical & Aerospace Engineering Faculty Publications

A steady-state apparatus has been developed for measuring the thermal conductivity of cast materials. The design has employed a novel thermal symmetry arrangement which can permit total electrical isolation of the test material from its surroundings. © 1980 American Institute of Physics

Static Temperature Measurements In Supersonic Flow Using Lasar Raman Spectroscopy, Paul A. Nystrom

Mechanical & Aerospace Engineering Theses & Dissertations

Laser Raman spectroscopy is a nonintrusive technique which can generate mean static temperature (MST) data within flow fields. By ratioing two simultaneously gathered portions of the Raman scattered spectrum, absolute intensity measurements were not needed. This method was applied to a supersonic cold air jet, where the NST ranged from 160'K to 300'K. Accurate measurements were not realized due to the presence of flow contaminates, especially water vapor.