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- Oxygen evolution reaction (18)
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- Fuel cells (17)
- Electrochemical impedance spectroscopy (16)
- Electrochemical oxidation (16)
- Li-ion battery (15)
- Cathode materials (14)
- Proton exchange membrane fuel cell (14)
- Solid oxide fuel cell (14)
- Methanol (13)
- Modified electrode (13)
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Articles 1171 - 1200 of 1254
Full-Text Articles in Materials Chemistry
External Transducing Measurement Of The Internal Pressure In Sealed Battery By Resistance Strain Gauge, Han-Xi Yang, Rong-Hui Hu, Xin-Ping Ai, Cong-Zhi Yang, Sheng-Xian Li
External Transducing Measurement Of The Internal Pressure In Sealed Battery By Resistance Strain Gauge, Han-Xi Yang, Rong-Hui Hu, Xin-Ping Ai, Cong-Zhi Yang, Sheng-Xian Li
Journal of Electrochemistry
A novel method to monitor dynamically the internal pressure of sealed battery with no damage of the battery by using of resistance strain measurement technique is presented. This technique employs the resistence strain gauges in touch of the battery case and to detect the minimal change in the battery deformation due to the increasing internal pressure, electrode expantion or intrenal temperature rise. Application of the technique for the study of the effects of the battery processing factors on the battery performance is described taking Ni MH battery as example.
Photoelectrochemical Studies On Nanoporous Tio2/Pan Film Electrode, Min-Sheng Liu, Yan-Zhong Hao, Xue-Bin Qiao, Mai-Zhi Yang, Sheng-Min Cai
Photoelectrochemical Studies On Nanoporous Tio2/Pan Film Electrode, Min-Sheng Liu, Yan-Zhong Hao, Xue-Bin Qiao, Mai-Zhi Yang, Sheng-Min Cai
Journal of Electrochemistry
The photon to electricity conversion process of nanoporous TiO2/PAn film electrode was studied in electrolytes with and without redox couple by using the photocurrent action spectra and potential dependence of photocurrent. It is concluded that the nanoporous TiO2/PAn film electrode has a structure of duplex n type semiconductor layers. The band gap of PAn film is 2.88eV.The TiO2 nanoporous film electrode modified by PAn can extend the range of optical absorption into visible and infrared region and effectively increase the photocurrent in the visible and infrared region. The photocurrent threshold shifts to>600nm and conversion …
Studies On The Electrode Kinetics Of Electrooxidation Of Mn2+, Wan-Li Hu, Tong Su, Wei Guo, Ding Zhou
Studies On The Electrode Kinetics Of Electrooxidation Of Mn2+, Wan-Li Hu, Tong Su, Wei Guo, Ding Zhou
Journal of Electrochemistry
The mechanism of electrooxidation of MnSO4 on Pb Sb As alloy anode was investigated by using rotating disc electrode technique. The results shown that the conditional standard potential of Mn(Ⅲ)/Mn(Ⅱ)in 40% H2SO4 is 0.886 4 V.The rate controlling step of electrode process is mixed controlled by charge transfer and diffusion.
Study Of Proton Exchange Membrane Fuel Cells(Pemfc), Shan-Hai Ge, Bao-Lian Yi, Hong-Fen Xu, Ming Han, Zhi-Gang Shao
Study Of Proton Exchange Membrane Fuel Cells(Pemfc), Shan-Hai Ge, Bao-Lian Yi, Hong-Fen Xu, Ming Han, Zhi-Gang Shao
Journal of Electrochemistry
The electrode kinetic parameters for proton exchange membrane fuel cells(PEMFC) were investigated by measuring the relations of cell potential and current density. An experimental stack of PEMFC which can be operated at E cell =0.7V, I =0.55A/cm2 steadily is presented, and the effects of electrode structure and operation conditions such as temperature, pressure, humidification, flow rate on the performance of PEMFC are discussed.
Electrooxidation Of Benzene To Benzoquinone In A Packed Bed Reactor, Xin-Sheng Zhang, Ping Ding, Ying-Chun Dai, Wei-Kang Yuan
Electrooxidation Of Benzene To Benzoquinone In A Packed Bed Reactor, Xin-Sheng Zhang, Ping Ding, Ying-Chun Dai, Wei-Kang Yuan
Journal of Electrochemistry
A packed electrode reactor was used to oxidize to benzoquinone. Anode bed of the reactor has a size of 10～30 mm×450 mm×50 mm(thickness×length×width),and was packed porous lead alloy. A dispersion of benzene in 1 mol/L aqueous sulfuric acid was passed through the reactor. Current efficiency for benzoquinone generation is 62.9% at optimal operating condition: velocity of electrolyte flow, 0.19 ms -1 ;current, 10 A; thickness of anode bed, 10 mm, and percentage of benzene, 24%.
Electrochemical Preparation Of Rare Earth Functional Materials And Application Of Rare Earth To Electrochemistry, Qi-Qin Yang, Tong-Xiang Ye
Electrochemical Preparation Of Rare Earth Functional Materials And Application Of Rare Earth To Electrochemistry, Qi-Qin Yang, Tong-Xiang Ye
Journal of Electrochemistry
The new progress and related mechanism of the electrochemical preparation of rare earth materials (magnets, magnetooptic materials, battery materials, luminescent devices, semiconductors, superconductors) and the application of rare earth to the electrochemical areas (e.g. electroplating, corrosion, electrosynthses) have introduced.
In-Situ Raman Spectroscopic Study Of The Oxidation And Reduction Of Ag Electrode In Na2So4, Yan-Xia Chen, Kai-Qi Huang, Zhong-Qun Tian
In-Situ Raman Spectroscopic Study Of The Oxidation And Reduction Of Ag Electrode In Na2So4, Yan-Xia Chen, Kai-Qi Huang, Zhong-Qun Tian
Journal of Electrochemistry
In-situ Raman spectroscopy combined with cyclic voltammogram measurements was used to investigate formation of oxygen species at Ag electrode surfaces during the oxidation and reduction process in 0.1 mol/L Na2SO4 solution. The time dependent Raman spectra show that at potentials positive of 0.2 V, adsorption of oxygen atom occurs, while at the potentials positive of 0.4 V, some oxygen atoms migrate into subsurface of the Ag electrode and the other form strongly bound oxygen on the surface through chemical bond. At the same potentials, part of the silver atoms are oxidized and form Ag2SO4 …
Studies Of Surface Alloy As High Efficient Electrocatalyst For Glyoxylic Acid Synthesis, Sheng-Pei Chen, Sheng-Qing Xia, Shi-Gang Sun
Studies Of Surface Alloy As High Efficient Electrocatalyst For Glyoxylic Acid Synthesis, Sheng-Pei Chen, Sheng-Qing Xia, Shi-Gang Sun
Journal of Electrochemistry
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Studies On The Transport Properties Of Zn2+ In The Zn/V2O5 Secondary Battery With Aqueous Medium, Jia-Hong Zhou, Kuan-Hong Xue, Gu-Ping Pan
Studies On The Transport Properties Of Zn2+ In The Zn/V2O5 Secondary Battery With Aqueous Medium, Jia-Hong Zhou, Kuan-Hong Xue, Gu-Ping Pan
Journal of Electrochemistry
The transport properties and the reaction mechanism of Zn2+ in the cathode material of Zn/V2O5 secondary battery with aqueous medium were studied by use of intermittent titration experiments and X-Ray diffraction analysis. The relations of some kinetic parameters to the discharge depth were discussed. The results of the experiments show that the cathodic discharge reaction is an intercalation process.
Electrode Process Of Lithium Ions On Aluminum Electrode In Molten Licl-Kcl, Shu-Zhen Duan, Cong-Sheng Guan, Qing-Rong Shi, Xin-Dong Wang
Electrode Process Of Lithium Ions On Aluminum Electrode In Molten Licl-Kcl, Shu-Zhen Duan, Cong-Sheng Guan, Qing-Rong Shi, Xin-Dong Wang
Journal of Electrochemistry
The Deposition mechanism of Lithium on aluminium electrode was studied by using linear sweep voltammetry and potential step method. The formation of α-solid solution was controlled by the diffusion of lithium within the aluminium substance. The formation of β-LiAl alloy was limited by the rate of forming the alloy at the legining, and by diffiusion of lithium through the β- LiAl alloy layer was limited by the rate of forming the alloy at the begining, and by the diffusion of lithium through the β-LiAl alloy later. Neucleation polarization for the formation of β-LiAl alloy was observed. This polarization is an …
Studies Of Surface Electrochemistry And Electrocatalysis At Atomic And Molecule Level, Shigang Sun
Studies Of Surface Electrochemistry And Electrocatalysis At Atomic And Molecule Level, Shigang Sun
Journal of Electrochemistry
The main progresses achieved during last few years in our research group concerning studies of surface electrochemistry and electrocatalysis were reviewed in this present paper. Four topics were described: 1) the surface electrochemistry and model electrocatalysis of metal single crystal planes, 2) the electrocatalytic reaction mechanism and the control of reaction pathways at molecule level, 3) the reaction kinetics of electrooxidation of small organic molecules, and 4) the relationship between the properties and the surface chemical states of electrocatalyst. This review lays in emphasis on the demonstration of the results as well as the research direction of surface electrochemistry and …
A Preliminary Study On Thin Film Plasticizing Lithium Ion Battery, Quanfeng Dong, Hanxi Yang, Xinping Ai, Xiaohong Hu, Shengxian Li
A Preliminary Study On Thin Film Plasticizing Lithium Ion Battery, Quanfeng Dong, Hanxi Yang, Xinping Ai, Xiaohong Hu, Shengxian Li
Journal of Electrochemistry
A dry polymer electrolyte was made by plasticizing a copolymer matrix and further filling with liquid electrolyte. A thin-film lithium ion battery based on the dry polymer electrolyte was manufactured and its electrochemical properties were measured. It is found that the thin film lithium ion battery exhibits similar discharge properties to liquid electrolyte battery, and shows strong high rate capability.
Study On The Synthesis And Electrochemical Behavior Of Poly (Quinonoid-Disulfide), Xiaohui Tang, Xiuwu Sun, Yongfang Li, Shibi Fang
Study On The Synthesis And Electrochemical Behavior Of Poly (Quinonoid-Disulfide), Xiaohui Tang, Xiuwu Sun, Yongfang Li, Shibi Fang
Journal of Electrochemistry
Organic polydisulfide containing quinonoid structure was synthesized by chloromethylation, oxidation by nitric acid, and condensation polymerization with sodium disulfide. The effect of quinonoid structure on the electrochemical behavior of organic polydisulfide was investigated with cyclic voltammetry and chargedischarge measurement. The result shows that quinonoid struture mainly affects the positions of redox peaks of organic polydisulfide, open circuit voltage and discharge platform voltage of cell with the organic polydisulfide as cathode.
The Investigations Of Surface Treatment Methods And Characterization Of Oxide Films On Ab5 Based Metal Hydride Electrodes Ⅰ. New NiRich Treatment Methods And Photoelectrochemical Characterization Of Oxide Films, Junmin Nan, Yong Yang, Jun Li, Zugeng Lin
The Investigations Of Surface Treatment Methods And Characterization Of Oxide Films On Ab5 Based Metal Hydride Electrodes Ⅰ. New NiRich Treatment Methods And Photoelectrochemical Characterization Of Oxide Films, Junmin Nan, Yong Yang, Jun Li, Zugeng Lin
Journal of Electrochemistry
Two simple and efficient surface treatment methods for AB5 type hydrogen storage alloys were developed. The results of X-ray photoelectron spectroscopy (XPS) and cyclic voltammetric (CV) experiments showed that the hydrogen storage alloys treated by two different methods had Ni rich surface layer so that the performances of the electrodes were improved after treatment. The characterization of the oxide films which formed on the surface of electrodes through potentiodynamic oxidation with the help of photoelectrochemical microscopy (PEM) were done. The anodic photocurrent and the cathodic photocurrent related to the oxidation of hydrogen and the reduction of oxygen on the …
A Study On Heterogeneous Indirect Electrosynthesis Of Benzaldehyde, Daobao Chu, Changjian Lin, Huashui Lin, Jianguang Tan
A Study On Heterogeneous Indirect Electrosynthesis Of Benzaldehyde, Daobao Chu, Changjian Lin, Huashui Lin, Jianguang Tan
Journal of Electrochemistry
Heterogeneous indirect electrosynthesis process of benzaldehyde has been investigated using cyclic voltammetry and polarization curves. An optimum condition for preparation of benzaldehyde by indirect electrooxidation of toluenc with redox Mn3+/Mn2+ is given in this paper. Electrolytic regeneration Mn3+ are made at Pt/Ti anode in “slurry” MnSO4/H2SO4 medium. Current efficiency for electrolytic regeneration Mn3+ was maintained over 88% by “double cyclic way”.
Investigation Of Methanol Anode Electrooxidation Catalysts, Gangyao Wen, Ying Zhang, Zhenglong Yang, Changzhi Li
Investigation Of Methanol Anode Electrooxidation Catalysts, Gangyao Wen, Ying Zhang, Zhenglong Yang, Changzhi Li
Journal of Electrochemistry
A series of catalysts, Pt-WO3/C, Pt/Ru/C and Pt-Ru-WO3/C were prepared by chemical reduction deposition. Electrocatalytic oxidation of methanolon different catalyst/Nafion membrane electrodes was studies by voltammetry and current-potential polarization. The results indicated that the catalytic activity order of different catalysts is as follows: Pt-Ru-WO3/C > Pt-Ru/C > Pt-WO3/C. At the same time, influences of methanol concentrations and catalyst proportion on performances of anodes were also studies.
Progresses In Surface Electrochemistry And Electrocatalysis ——A Review On The 1997 Joint International Meeting Of Electrochemistry And 97' International Meeting Of Surface Electrochemistry, Shigang Sun
Journal of Electrochemistry
The progresses in surface electrochemistry and electrocatalsis reported in the 1997 joint international meeting of electrochemistry and in the 97′ international meeting of surface electrochemistry were reviewed. The main trends described in this paper consisted of 7 aspects: 1) the studies employing single crystal electrodes, 2) the development of in situ methods of diverse spectroscpoy, 3) the innovation of new research techniques, 4) the preparaton of electrocatalyst of high performances, 5) the quantitative studies on kinetics of electrocatalytic reactions, 6) the investigation on the dynamic processes of surface by timeresolved methods, and 7) the theoretical modeling and simulation of surface …
Anchor Effect Of Iron And Cobalt To Platinum On Carbon Substrates, Zidong Wei, Hetong Guo, Zhiyuan Tan
Anchor Effect Of Iron And Cobalt To Platinum On Carbon Substrates, Zidong Wei, Hetong Guo, Zhiyuan Tan
Journal of Electrochemistry
The cathodic reduction of oxygen is studied on porous carbonbased electrodes carrying platinumiron and/or cobalt alloy catalysts. Electrodes using such electrocatalysts, particularly when used as cathodes in acidic electrolytes, remain stable for longer periods. The cathodic polarization of oxygen reduction on such electrodes is 20 mV to 40 mV lower than that on the conventional electrode on which only platinum alone is used as an electrocatalysts. An accelerated aging test (AAT) is used to evaluate the corrosion resistance and sintering resistance of each catalyst. The dissolution of the catalyst in the AAT filtrate is analysed and provides a measure of …
Study On Nano Electrode Material Of Lithium Ion Batteries, Jinkua You, Yong Yang, Dong Shu, Shenghui Wu, Yingchun Zhang, Zugeng Lin
Study On Nano Electrode Material Of Lithium Ion Batteries, Jinkua You, Yong Yang, Dong Shu, Shenghui Wu, Yingchun Zhang, Zugeng Lin
Journal of Electrochemistry
In this paper, the structure and morphology of the nano phase electrode materials have been characterized with XRD and TEM. The performances of electrochemical intercalation and deintercalation of lithium ions have been studied by using cyclic voltammograms and galvanostatic charge discharge techniques. The results show that the nano materials posses advantage of micro structure and Li+ ions intercalation performances. The observed high capacity and large charge discharge current density of the nano phase materials seem to have resulted from three kinds of effects: 1) an increase in the space for Li+ ions intercalation; 2) a decrease in the …
Preparation Of High Rate Discharge Foamed Ni-Cd Battery, Yuming Wang, Jinsheng Chen
Preparation Of High Rate Discharge Foamed Ni-Cd Battery, Yuming Wang, Jinsheng Chen
Journal of Electrochemistry
A novel device of SC type foamed NiCd battery is presented, in which, the innerresistance of battery is appeared to be reduced, and the electrode performance is gained to very improved, and so, this battery can be suited to using of the powerdrive pistol drill.
Molten Carbonate Fuel Cell Materials And Technology, Naichao Li, Baolian Yi
Molten Carbonate Fuel Cell Materials And Technology, Naichao Li, Baolian Yi
Journal of Electrochemistry
Molten Carbonate Fuel Cell materials are reviewed, and the technology of Molten Carbonate Fuel Cell are discussed.
The Activity Of Alloy Cu-Ni Electrode In Electroreduction Of Aromatic Nitro-Compounds, Chunan Ma, Shaoping Tong, Xiaojun Cheng, Hui Wang
The Activity Of Alloy Cu-Ni Electrode In Electroreduction Of Aromatic Nitro-Compounds, Chunan Ma, Shaoping Tong, Xiaojun Cheng, Hui Wang
Journal of Electrochemistry
Cu-Ni alloy on the basis of copper at different ratio Cu/Ni are prepared by codepostion. The cathode activtiy of film are studied by steady-state polarization for electroreduction nitro-benzene (NB) and 1,5-dinitroanthraquinone (1,5-DNA) to p-aminophenol and 1,5-diamino-4,8-dihydroanthraquinone respectly. The results show that the alloy cathodes at different ratio Cu/Ni have different exchange current density (io) and apparent activition energy (EA). The alloy (CN-30) has maximal io and minimal EA by codeposition at the following conditions: electrolyte: 0.05 mol/L CuSO4·5H2O+0.6 mol/L NiSO4·6H2O+0.25 mol/L Na3Cit·2H2O; …
Study On The Oxygen Electrodes Of Alkaline Fuel Cells Effect Of Dopant On The Activity Of Ag/C Catalyst, Jiawei Teng, Linhua Jin, Luncheng Tang
Study On The Oxygen Electrodes Of Alkaline Fuel Cells Effect Of Dopant On The Activity Of Ag/C Catalyst, Jiawei Teng, Linhua Jin, Luncheng Tang
Journal of Electrochemistry
A new kind of nonnoble catalyst for the oxygen electrodes of Alkaline Fuel Cells was investigated. The AgNiBiHg/C catalyst, which was prepared by chemical reduction, was active for the cathodic reduction of oxygen in alkaline fuel cells. It was found that the catalytic activity was improved by adding Ni, Bi, Hg to Ag/C catalyst, and the maximum activity was observed at Ag50%-Ni2%-Bi3%-Hg3%-C42%(wt%). XRD inconjunction with SEM indicated that the crystalline silver turned into amorphous in the presence of doping agents and the grain size of silver was reduced. No dramatic deactivation of the catalyst occured after 5200 hours of service.
Study On Perchlorate Produced By Electrolysis With Oxygen Cathode, Zhigang Shao, Baolian Yi, Naichao Li, Ming Han
Study On Perchlorate Produced By Electrolysis With Oxygen Cathode, Zhigang Shao, Baolian Yi, Naichao Li, Ming Han
Journal of Electrochemistry
A new method of measuring the flow capacity of cell gas in the perchlorate cell process equipped with an oxygen cathode is applided to investigate the influence of changes in the concentration of solution (chloride, chlorate, perchlorate and metal ion) and changes in the operation parameters (current density, temperature and pH) on perchlorate current efficiency. The main abstacle that the oxygen cathode is used in the perchlorate cell process is put forward and a method is provided to resolve it.
Photoluminescence Of Photoelectrochemically Etched N+-Si, Guozheng Li, Chengqian Zhang, Xiumei Yang
Photoluminescence Of Photoelectrochemically Etched N+-Si, Guozheng Li, Chengqian Zhang, Xiumei Yang
Journal of Electrochemistry
PS layer on n+-Si with (111) orientation prepered by means of photoelectrochemically etched has photo-luminescent (PL) ability like PS layer on usual n-Si. The data of PL spectra and quenching are given.
Surface Modifications Of Carbon Materials Used As Anode Of Lithium Ion Battery Ⅲ. Improvement Of Artificially Imposed Solid Electrolyte Film On Cell Performance, Shuhua Ma, Xiabin Jing, Fosong Wang
Surface Modifications Of Carbon Materials Used As Anode Of Lithium Ion Battery Ⅲ. Improvement Of Artificially Imposed Solid Electrolyte Film On Cell Performance, Shuhua Ma, Xiabin Jing, Fosong Wang
Journal of Electrochemistry
The improving effect of solid electrolyte film artificially imposed on carbon electrode was investigated. The result showed that both the charge/discharge capacity and first charge/discharge efficiency, to a certain extent, were enhanced, and the result also suggested the effectiveness of the substitution of the artificially imposed solid electrolyte film for the inherent passivating film which was formed on the surface of the carbon electrode while inserted in the electrolyte during charging or discharging. The Scanning Electron Microscope result displayed the compact and well-defined morphology of the artificially imposed crystalline film.
Preparation And Examination Of Planar Type Solid Oxide Fuel Cells, Yi Jiang, Jingwang Yan, Shizhong Wang, Chunying Yu, Wenzhao Li
Preparation And Examination Of Planar Type Solid Oxide Fuel Cells, Yi Jiang, Jingwang Yan, Shizhong Wang, Chunying Yu, Wenzhao Li
Journal of Electrochemistry
The solid oxide fuel cells of planar type (SOFC) have been developed after successfully preparing La0.8Sr0.2MnO3 cathodes and Ni-YSZ ceramic anodes on YSZ plates and solving the high temperature sealing technical problem. Examination of the single cells fabricated showed that the maximum power output at 950 ℃ for H2 as fuel and air as oxidant reached 0.12 W/cm2. It was found that the large polarization overpotential of the Ni-YSZ anode and the Ohmic losses of the cells were two main factors responsible for the relative low output power density.
Electrocatalytic Oxidation Of Methanol On The Stearate Nickel L-B Film, Benzeng Hua, Wenyan Hu, Yanzhen Chen, Yanhong Zhang
Electrocatalytic Oxidation Of Methanol On The Stearate Nickel L-B Film, Benzeng Hua, Wenyan Hu, Yanzhen Chen, Yanhong Zhang
Journal of Electrochemistry
The stearate nickel L-B films is good electroacatlyst for the oxidation of methanol MeOH in alkaline. The electrochemical behaviors of stearate nickel L-B films is affected by the concentration of KOH. The rate of quantity of mickel ion and stearic acid in L-B films is 1∶1, which means that the nickel ion may exist in -COONi(OH) form. The electrocatalytic process is influenced by the concentration of OH-, it involves the penetration of MeOH into the films. The oxidative currents of MeOH are linearly dependent on the bulk concentration.
Investigation On Electro Reduction Behaviour Of Copper Anodic Products In Concentrated Naoh Solutions Ⅱ. Electro Reduction Of Cu(Ⅱ) Products, Jianbo He, Hanhe Chen, Jianxin Lin
Investigation On Electro Reduction Behaviour Of Copper Anodic Products In Concentrated Naoh Solutions Ⅱ. Electro Reduction Of Cu(Ⅱ) Products, Jianbo He, Hanhe Chen, Jianxin Lin
Journal of Electrochemistry
Potentiostatic oxidation potentiodynamic or galvanostatic reduction methods have been used to study the cathodic reduction behaviour of various products anodically formed on the second stage of copper oxidation in concentrated NaOH solutions. Seven cathodic current peaks and the corresponding cathodic potential plateaus are observed on the potentiodynamic E/i curves and the galvanostatic E/t curves, respectively. In the negative potential scan, there are three couples of voltammetric peaks which have been attributed to the formation and reduction of CuO, Cu(OH)2 and Cu(Ⅱ) ion, respectively. The complicated mechanism for the electro formation of the three Cu(Ⅱ) species are discussed.
Studies On The Failure Modes Of Stationary Vrla Batteries, Yibo Tong, Xiangming Qiu
Studies On The Failure Modes Of Stationary Vrla Batteries, Yibo Tong, Xiangming Qiu
Journal of Electrochemistry
In order to improve the reliability and the quality of stationary valve-regulated lead-acid (VRLA) batteries, the failure modes of the stationary VRLA batteries which caused by the water loss and the thermal runaway are studied. The water loss may be solved by increasing the Oxygen-recombination efficiency, choosing the suitable grid material and the additives of megative paste, decreasing the corrosion of the positive plates. The thermal runaway may be solved by decreasing the inner ohmic resistance of VRLA batteries, improving the outside condition of batteries such as putting into the absorbing-heat material between the abtteries etc..