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Articles 4741 - 4770 of 5042
Full-Text Articles in Food Processing
Study On Extraction Of Flavonoids From Poacynum Hendersonii By Suporcritical Co2, Shi Junyou, Jing Nianhua, Li Caixia
Study On Extraction Of Flavonoids From Poacynum Hendersonii By Suporcritical Co2, Shi Junyou, Jing Nianhua, Li Caixia
Food and Machinery
The supercritical CO2 extraction processing of flavonoids was optimized with Poacynum hendersonii leave as raw material. Firstly, the influences of the type and pH value for cosolvent were explored by single factor experiments. And the 70% ethanol with pH value of 10 was fixed as cosolvent. Then, the effects of extracting factors such as extracting pressure, temperature, time and cosolvent dosage, were investigated with orthogonal experiments. According to the researching report, the optimal process conditions were as follows: 150 g raw material, extraction temperature 45 ℃, extraction pressure 20 MPa, extraction time of 2 h, 70% ethanol with pH value …
Optimization Of Ultrasonic-Assisted Ethanol Extraction For Total Flavonoids From Buckwheat Hust, Yang Fang, Yang Wanlin, Chen Jinyu, Shao Jinliang, Lan Shanshan
Optimization Of Ultrasonic-Assisted Ethanol Extraction For Total Flavonoids From Buckwheat Hust, Yang Fang, Yang Wanlin, Chen Jinyu, Shao Jinliang, Lan Shanshan
Food and Machinery
The extraction of total flavonoids from buckwheat hust was optimized by ultrasound-assisted ethanol extraction method. Through the optimization by single factor, with extraction efficiency of total flavonoids, the effects of ultrasonic extraction time, ultrasonic extraction temperature, ethanol concentration and material-to-liquid ratio of total flavonoids from buckwheat hust were investigated. Through the optimization by response surface method, the optimal extraction conditions were found. The experimental results showed that the best conditions were ethanol concentration 69%, material-to-liquid ratio 1∶51(m∶V), extraction time 30 minute and ultrasonic extraction temperature 59 ℃, the yield rate of total flavonoids was 3.542%.
Improvement On Quality Of Rice Noodles By Screw Extrusion Technology, Tang Hanjun, Li Linjing, Zhu Wei
Improvement On Quality Of Rice Noodles By Screw Extrusion Technology, Tang Hanjun, Li Linjing, Zhu Wei
Food and Machinery
The treatments of screw extrusion technology on rice noodle (TDM, and XMM) and Fensi (TFS), and traditional craft rice noodles (WFM) were compared in the characteristics of quality, and the microstructure was observed after cooked. Physicochemical properties of TDM and XMM were between TFS and WFM before cook, and TDM was almost close to the best strength of TFS. Physicochemical properties after cook were the similarities between TDM and XMM, and close to TFS, further away from the WFM. Their microstructure characterized by irregular, polygonal honeycomb cellular structure, micro-Chamber diameter approximately 0.5~2.0 μm. The results showed that the screw extrusion …
Preparation Of Reconstitute Germination Sorghum Flake, Li Yan, Yi Cuiping, Li Mengting, Yang Yang
Preparation Of Reconstitute Germination Sorghum Flake, Li Yan, Yi Cuiping, Li Mengting, Yang Yang
Food and Machinery
In order to improve the eating quality and nutrition quality of sorghum, reconstitute germination sorghum flakes were prepared by mixing germination sorghum with grain amaranth and non-waxy rice through screw extrusion and roller press. The protein and dietary fiber contents were used as the nutrition index and the processing formula was designed by software. The results indicated that the protein and dietary fiber contents got to 8.8% and 7.3%, respectively, when the products was prepared by mixing 17.3% of germination red sorghum, 18.1% of amaranth and 64.6% of non-waxy rice. And the contents of protein and dietary fiber were 9.5% …
Optimization Of Spray Drying Technology And Analysis Of Dissolution Characteristics On Fruit Powder From Akebia Trifoliate, Xiaoyan Da, Li Jiaxing, Xiao Xiufeng, Wu Yue, Ma Lang, Zhou Yanhui
Optimization Of Spray Drying Technology And Analysis Of Dissolution Characteristics On Fruit Powder From Akebia Trifoliate, Xiaoyan Da, Li Jiaxing, Xiao Xiufeng, Wu Yue, Ma Lang, Zhou Yanhui
Food and Machinery
Research on optimizing the spray dry preparation technology of Akebia trifoliate fruit powder and analyze its dissolution characteristics. First of all, the effects of dry agent dosage, pulp solids content, inlet air temperature, outlet air temperature on fruit powder yield were discussed by single factor tests. And then the spray drying process conditions were optimized by orthogonal test, and the dissolution characteristics was analyzed by detection of powder fluidity, solubility, dissolution time. The results showed that the optimal preparation conditions of Akebia trifoliate were as followed: malt dextrin dosage 16%, pulp solids content 20%, the inlet air temperature 150 ℃, …
Comparative Study On Germination Characteristics For Different Varieties Of Unpolished Coix Seed And Optimization Of Germinated Technological Conditions, Dang Juan, Qin Likang, Yang Xianlong, Jin Yi
Comparative Study On Germination Characteristics For Different Varieties Of Unpolished Coix Seed And Optimization Of Germinated Technological Conditions, Dang Juan, Qin Likang, Yang Xianlong, Jin Yi
Food and Machinery
This comparative study to analyze the changes in physiological and biochemical in the same condition by unpolished coix seed of 5 varieties that have been produced in Guizhou or Laos, selecting out optimal germination of varieties, then optimizing the germination rate and germination by using γ-amino butyric acid(GABA) as evaluation index, using single factor experiment and orthogonal design methods, tracing its main nutrients and functional components dynamically. The results showed that the sprouts of GZ-1 from Guizhou had the highest germination rate, free amino acids and γ-amino butyric acid (GABA) levels among the five varieties. Based on the sprouting rate …
Optimization Of L-Lysine Medium By Response Surface Methodology, Teng Guosheng, Liu Yong, Wu Lida, Fan Chunyan, Wang Jinzhi, Guan Bing, Shi Shuhui, Tong Yi
Optimization Of L-Lysine Medium By Response Surface Methodology, Teng Guosheng, Liu Yong, Wu Lida, Fan Chunyan, Wang Jinzhi, Guan Bing, Shi Shuhui, Tong Yi
Food and Machinery
Plackett-Burman design, steepest ascent design and response surface methodology were used to optimize fermentation mediumof L-lysine. Plackett-Burman designmethod was applied to evaluate the main significant factors, and the result had shown that sodium chloride、magnesium sulfate and corn steep liquor were the major factors. Then, the Box-Behnken design and response surface methodology we used to confirm the optimum parameters with NaCl 2.72%, MgSO4·7H2O 0.05%, and corn steep liquor (CSL) 21.13 g/L, which were proceeded based on thegreatest response area of NaCl, MgSO4·7H2O and corn steep liquor. Under the optimal conditions, the theoretical yield …
Research Progress On Gas Storage And Transport Packaging Of Chinese Bayberry Fruit, Jiang Qiaojun, Zheng Yonghua, Xu Jing, Jiang Peishan
Research Progress On Gas Storage And Transport Packaging Of Chinese Bayberry Fruit, Jiang Qiaojun, Zheng Yonghua, Xu Jing, Jiang Peishan
Food and Machinery
Reviewed the research progress in Chinese bayberry gas storage and transport packaging in recent years. Now the Chinese bayberry gas storage methods were mainly as followed: modified atmosphere, controlled atmosphere storage with N2, high CO2, superatmospheric oxygen and fixed gas proportion and so on. Chinese bayberry packaging transportation methods were mainly included: Foam Box + Ice, Plastic Box Packaging and Functional Fresh-keeping Packaging and so on. From the view of practical application, systematically elaborated the problem of this technology system，and points out such as the fast precooling, appropriate proportion of gases and dynamic monitoring, the solution of the mold problem …
Current Situation Of Food Safety Crime And The Criminal Law Perfection, Gong Tingting
Current Situation Of Food Safety Crime And The Criminal Law Perfection, Gong Tingting
Food and Machinery
The prevention and control of China's current food safety crimes has two problems: one is the awe force shortage on food safety crime punishment for criminal suspects; the other is serious lack of food safety regulatory system. In order to effectively solving the increasingly severe food safety crime problem, combined with Chinese national conditions, and based on the inspection experience on the basis of the prevention and control of foreign food safety crime, to strengthen the prevention and control of food safety crime criminal legislation work, should increase the intensity of punishment, set up the defects of food recall system …
Application Of Information Technology In Chinese Food Safety Management, Xiao Yumei, Xiao Fuqiang
Application Of Information Technology In Chinese Food Safety Management, Xiao Yumei, Xiao Fuqiang
Food and Machinery
The management of Chinese food safety is not optimistic right now. The mainly cause of this problem is the degree of food information in low procurement, production, circulation, and other aspects. Whether the government supervision departments or social forces are difficult to comprehensively collect and master the information related to food security. It can not form a timely and effective regulation. In the contrast, information technology is applied to the important link of the food safety management in the United States, the European Union and other developed countries or regions. The experiences of the developed countries should be taken as …
Real Dilemma And Improvement Of Food Industry Tourism Development, Lin Wenchao
Real Dilemma And Improvement Of Food Industry Tourism Development, Lin Wenchao
Food and Machinery
Food industry tourism meets the needs of tourists seeking novelty, expands the brand influence and improves the trust of consumers on food safety, enable consumers to participate in food business management and promote the development of local economy. However, there are many problems in Chinese food industry tourism, for example the tourism project design is single, the degree of participation of visitors is not high, the food companies themselves do not pay enough attention, and lack of specialized hardware support, which cause a dilemma of development. In order to ensure the smooth development of food industrial tourism, some actions should …
Study On Food Nutrition Of Left-Behind Children By Latent Class Model, Zhang Zhenxia
Study On Food Nutrition Of Left-Behind Children By Latent Class Model, Zhang Zhenxia
Food and Machinery
The latent class model was used to study the special group of children who lacked food nutrition, the left behind children, and the effects were also studied, including the food nutritional status and the individuals genetic and the food and nutrition intake, mothers care, and basic medical and health services. Through research and analysis, two groups of children who were left behind were identified, the food nutrition malnutrition and the food nutrition condition good, and the proportion of malnourished children was higher with 69.4%. In the Two groups of left behind children, the main difference lies in the mother care, …
Design And Research Of Fruit Detection And Grading Machine By Clamping Fruit Stems, Wang Yunxiang, Ma Benxue, Jia Yanting, Yang Jie
Design And Research Of Fruit Detection And Grading Machine By Clamping Fruit Stems, Wang Yunxiang, Ma Benxue, Jia Yanting, Yang Jie
Food and Machinery
No abstract provided.
Design Of Starter-Making Process Control System Using Bidirectional Variable Frequency Vibration Pressing, Li Hong, Wang Wenle, Hua Yong
Design Of Starter-Making Process Control System Using Bidirectional Variable Frequency Vibration Pressing, Li Hong, Wang Wenle, Hua Yong
Food and Machinery
Based on the condition of lower mud extracting ability of starter making, developed a starter making method of rotary bidirectional variable frequency vibration pressing which is designed on Programmable Logic Controller(PLC), and the hardware and software design of PLC field controlling as well as host control system was achieved. The results showed that starter produced by this method had the advantage of density uniformity, good porosity, modest hardness, easy demoulding, smooth surface, exterior condition and full degree surface, and it also has an ideal effect on mud extracting.
Reseach On Quality Changes During Fruit Development Of Chayote, Li Yu, Qin Wen, Du Xiaoqin, Liu Ji
Reseach On Quality Changes During Fruit Development Of Chayote, Li Yu, Qin Wen, Du Xiaoqin, Liu Ji
Food and Machinery
The changes of growth phase and quality indicators during different growth stages of chayote were measured and analyzed. The results indicated that the growth curve of chayote showed single sigmoid pattern and the trends of quality indicators were different with fruit development dynamics. Respiration rate decreased rapidly with fruit development and respiration peak appeared at maturity; the contents of Vc, chlorophyll and hydrolysis amino acids were higher during the young fruit development, then decreased to a low level; while cellulose content and hardness showed the opposite trends. The fruit had fully grown with higher content of amino acids, lower respiratory …
Research Progress In Starch Modification By Heat Moisture Treatment, Liao Luyan, Wu Weiguo
Research Progress In Starch Modification By Heat Moisture Treatment, Liao Luyan, Wu Weiguo
Food and Machinery
The heat moisture treatment refers to the relative lower humidity and temperature in a certain time, and it is a physical modification method of starch properties change. This method costs lower and avoid the pollution by chemical modification, and achieve the purpose of improving starch specific features, which has been showing a good application prospect in modified starch. This paper introduces the effects on the starch structure and properties by heat moisture treatment in detail, and finally expounds the mechanism of the heat moisture treatment starch and the research progress in food applications.
Preparation Of Immobilized Lipoxygenase Onto Magnetic Fe3O4 Nanometer Particles, Ding Wenwu, Cao Ruyi, Sun Mingzhen, Xia Yunkong
Preparation Of Immobilized Lipoxygenase Onto Magnetic Fe3O4 Nanometer Particles, Ding Wenwu, Cao Ruyi, Sun Mingzhen, Xia Yunkong
Food and Machinery
Lipoxygenase which is a kind of peroxidase could be used in many facets of industry. The stability and using times of the enzyme would be increased after the enzyme was immobilized by appropriate methods and materials. In this study, nanometer Fe3O4 was prepared by hydrothermal method and modified with SiO2 and KH550 to obtained composite carriers. Lipoxygenase was immobilized on the composite carriers by glutaraldehyde. The influence factors on enzyme activity for free and immobilized enzyme were studied. The TEM results showed that the black nanoparticles were rod shaped. The mass of enzyme immobilized on the …
Component Analysis Of Rhizomes Of Chinese Atractylodes Medicinal Plants, Han Bangxing, Peng Huasheng, Zhang Ling
Component Analysis Of Rhizomes Of Chinese Atractylodes Medicinal Plants, Han Bangxing, Peng Huasheng, Zhang Ling
Food and Machinery
To explore the relationship between the essential oils from the rhizomes of Chinese Atractylodes medicinal plants in Dabie Mountains and its eastern hilly regions and the medicinal products. The medicinal plants of Atractylodes regions were investigated successively, GC—MS analysis was performed for 14 samples of different areas, and cluster analysis and principal component analysis were carried out by SPSS. Result: The colour of the essential oils of A. macrocephala, its transition types and A. chinensis was lighter, while of A. lancea in low altitude areas it was deeper.Clustering results showed that three categorizations were clustered. A. macrocephala was in a …
Analysis Of Chemical And Volatile Components Of Cyclocarya Paliurus Tea, Li Tingting, Shi Yerong, Wu Caie, Fangshengzuo, Pan Haixia, Zhu Zhenji
Analysis Of Chemical And Volatile Components Of Cyclocarya Paliurus Tea, Li Tingting, Shi Yerong, Wu Caie, Fangshengzuo, Pan Haixia, Zhu Zhenji
Food and Machinery
To evaluate the quality of Cyclocarya paliurus (Batal) Ijinskaja tea, main chemical compounds, agricultural chemicals residues, and aroma compounds of Cyclocarya paliurus tea were analyzed. The aroma compounds of Cyclocarya paliurus tea were extracted by headspace solid-phase microextraction (HS—SPME), and analyzed by gas chromatography-mass spectrometry (GC—MS). The results showed that the contents of total flavonoids, polysaccharide, triterpene saponinsin of Cyclocarya paliurus tea were 0.73%, 2.53% and 0.88%, respectively. As for pesticide residues in Cyclocarya paliurus tea, 23 kinds of pesticide residues are below the limit of detection. The content of lead, arsenic, and mercury in Cyclocarya paliurus tea were 2.27, …
Study On Moisture Adsorption Mechanism By Lf—Nmr And Esem, Han Dan, Tian Zhaofu, Wang Hongsheng, Zhang Xiaoming
Study On Moisture Adsorption Mechanism By Lf—Nmr And Esem, Han Dan, Tian Zhaofu, Wang Hongsheng, Zhang Xiaoming
Food and Machinery
Tobacco is hygroscopic products, and the moisture content has a significant impact on its quality. The relaxation time of different cigarette samples were measured by low-field NMR techniques to study the moisture adsorption mechanism and the microstructure difference between different tobacco samples which in different water content and were observed by ESEM. T21 values are the most sensitive indicators reflected the bonding strength of water. The dominated way of tobacco absorption is through the capillary sorption while after adding a polar group such as a hydroxyl the absorption mechanism steering chemisorptions. Spongy tissue and palisade tissue is an important organizational …
Performance Evaluation And Application Of Novel Two-Way Water-Blocking Additive In Tobacco, Zhang Xuqian, Tian Zhaofu, Wang Hongsheng, Zhang Xiaoming
Performance Evaluation And Application Of Novel Two-Way Water-Blocking Additive In Tobacco, Zhang Xuqian, Tian Zhaofu, Wang Hongsheng, Zhang Xiaoming
Food and Machinery
The water content of mainstream smoke components is closely associated with the sensory comfort of smoking, and it was also susceptible to the environment. In order to improve the stability of the water content in cigarette tobacco, the effective two-way water-blocking additive was developed of aliphatic hydrocarbons and compound sugars, the synergy of both additives made the water content of tobacco under a good control. The function of the additive was proved by testing in the simulation environment (RH=32% and RH=84%) in 35 ℃. Finally, proved that when added 1.0% aliphatic hydrocarbon (GY) and 0.1% polysaccharose (B), a good two-way …
Effect Of Ozone Treatment On Quality Of Steamed Breads, Li Bo, Gao Xin
Effect Of Ozone Treatment On Quality Of Steamed Breads, Li Bo, Gao Xin
Food and Machinery
The wheat was treated by ozone fumigation method at concentration of 5 mg/L for 0, 0.5, 1.0, 1.5 and 2.0 h, respectively. Then the wheat flour was used to make steamed bread. The ozone treatment effect on steamed bread quality was evaluated by the specific volume, texture profile analysis, and sensory evaluation. The aspect ratio increased with the increased ozone treatment time, however, the specific volume increased first and then decreased. For the texture profile analysis, 1.0 h ozone treatment could reduce the α-amylase activity and increase the gluten content, which increased the hardness and elasticity of the steamed bread. …
Purification And Identification Of Endogenous Allergy Protein Ara H 2 In Peanut, Zhu Qingqing, Zhang Wenju, Cai Qin, Chen Qin
Purification And Identification Of Endogenous Allergy Protein Ara H 2 In Peanut, Zhu Qingqing, Zhang Wenju, Cai Qin, Chen Qin
Food and Machinery
Ara h 2 is one of the major allergen in peanut. Raw peanut was subjected to a series of sequential treatments, such as protein extraction, DEAE-Sepharose Fast Flow anion-exchange chromatography and sodium dodecyl sulfate polyacrylamide gel electrophoresis (SDS—PAGE) recovery. The purified protein was identified by matrix-assisted laser desorption/ionization time of flight mass spectrometry (MALDI—TOF/MS). The results showed that the highly purified protein could be obtained by this method and was identified as Ara h 2 by MALDI—TOF/MS. The molecular weights of two constituents were 18.5 kD (Ara h 2.01) and 20.1 kD (Ara h 2.02). Recovery rate of column chromatography …
Effect Of Stabilized Rice Bran Addition On Retrogradation Kinetics Of Restructured Rice, Wang Peng, Yang Liu, Xiao Zhigang, Xie Tiemin, Li Zhe, Xie Bing
Effect Of Stabilized Rice Bran Addition On Retrogradation Kinetics Of Restructured Rice, Wang Peng, Yang Liu, Xiao Zhigang, Xie Tiemin, Li Zhe, Xie Bing
Food and Machinery
The retrogradation and crystallization characteristics of restructured rice were studied by DSC and XRD, and the effect of stabilized rice bran on Avrami equation and retrogradation behavior of restructured rice were analyzed. The results indicated that stabilized rice bran has a significant inhibition on retrogradation of restructured rice. The rate constant k of restructured rice with stabilized rice bran was the lowest in the test samples, and the development of crystal showed instantaneous nucleation; the V-type diffraction pattern and less B-type diffraction pattern were found in the restructured rice with stabilized rice bran after 7 days storage, which indicated that …
Study On Enzymolysis Of Pleurotus Nebrodensis Cooking Juices Based On Principal Component Analysis, Wang Xiaoli, Xue Shujing, Zhou Ming, Li Lu, Cheng Wei, Guan Jian, Yang De
Study On Enzymolysis Of Pleurotus Nebrodensis Cooking Juices Based On Principal Component Analysis, Wang Xiaoli, Xue Shujing, Zhou Ming, Li Lu, Cheng Wei, Guan Jian, Yang De
Food and Machinery
The effect of six enzymes was studied, as edible fungus hydrolase A01, Edible fungus hydrolase A02, cellulose, neutral protease, papain and flavourzyme on the content of free amino acid, resolvable sugar and L*, a*, b* value in Pleurotus nebrodensis cooking juices. The results indicated that the influence on the content of free amino acid and resolvable sugar was the most significant. The amount of free amino acid was increased by 55.0% after the neutral protease treatment; and the amount of resolvable sugar increased by 41.28% after cellulase treatment. The L* value both increased apparent …
Study On Quantum Dot Immune Chromatography Test Strip For Escherichia Coli O157:H7, Yuan Liejiang, Li Mengli, Wang Shuyuan, Yang Mengxin, Li Zhonghai
Study On Quantum Dot Immune Chromatography Test Strip For Escherichia Coli O157:H7, Yuan Liejiang, Li Mengli, Wang Shuyuan, Yang Mengxin, Li Zhonghai
Food and Machinery
To develop a quantum dotsb(QDs) immune chromatographic strip test for rapid and sensitive detection of Escherichia coli O157:H7. Water soluble QDs was electrostatic coupled with mouse anti- Escherichia coli O157:H7 monoclonal antibody and mouse anti- Escherichia coli O157:H7 and rabbit anti-mouse IgG were marking on the NC membrane as test line and control line, respectively. The rapid detection of immune chromatographic strip test paper was based on double antibody sandwich. With the immune chromatographic strip test, only 5 min was needed for detection. The limit of detection was 1×104 CFU/mL. No cross-reactivity was found with 8 kinds of common …
The Feasibility Of Rapid Determination Of The Cadmium Content In Rice Based On Near Infrared Spectroscopy And Synergy Interval Partial Least Squares, Zhu Xiangrong, Li Gaoyang, Su Donglin, Liu Wei, Shan Yang
The Feasibility Of Rapid Determination Of The Cadmium Content In Rice Based On Near Infrared Spectroscopy And Synergy Interval Partial Least Squares, Zhu Xiangrong, Li Gaoyang, Su Donglin, Liu Wei, Shan Yang
Food and Machinery
Near infrared spectroscopy (NIRS) combined with synergy interval partial least squares (siPLS) were used to establish the rapid method for the determination of cadmium content in rice. The NIR spectra of 72 rice samples were collected and analyzed. After optimization, an approach (SG smoothing combined with MSC and mean-centering) was adopted as a pre-treatment method for raw spectrum. SiPLS method was used as extraction methods of characteristic variables, and the NIRS quantitative model was built and predicted. The RMSECV and RMSEP of the siPLS model were 0.247 and 0.261, respectively. The Rc and Rp were 0.919 and 0.895, respectively. The …
Risk Assessment On Exposure Of Lead And Cadmium Of Rice In Guangdong Residents From 2012 To 2014, Cai Wenhua, Hu Shuguang, Xu Xiumin
Risk Assessment On Exposure Of Lead And Cadmium Of Rice In Guangdong Residents From 2012 To 2014, Cai Wenhua, Hu Shuguang, Xu Xiumin
Food and Machinery
According to monitoring data of rice of Guangdong from 2012 to 2014, assessment on exposure of lead, cadmium in Guangdong residents was made by the method of China Total Diet Study. The contents of lead, cadmium in the rice of Guangdong were measured through the food safety risk monitoring from 2012 to 2014. The margin of exposure (MOE) of lead, estimated monthly intake (EMI) of cadmium were worked out as evaluation criteria. The over limit rate of lead, cadmiumin in Guangdong Province rice were 0.11%, 622% respectively. In addition to parts of cadmium in rice exceed the standard rate is …
Simultaneous Determination Of 16 Kinds Of Phthalate Esters In White Spirit By Gas Chromatography-Mass Spectrometry With Internal Standard, Liu Miaofen, Liu Jia, Qiu Peili
Simultaneous Determination Of 16 Kinds Of Phthalate Esters In White Spirit By Gas Chromatography-Mass Spectrometry With Internal Standard, Liu Miaofen, Liu Jia, Qiu Peili
Food and Machinery
Introduced a way to measure 16 kinds of phthalate esters from wine by using internal standard on GC—MS. Diethyl terephthalate as the internal standards were added in wine, after reduced the alcohol concentration by adding distilled water. The hexane extraction efficiency of 16 kinds of PAEs was improved significantly. The results revealed that the quantitative detection of the linear was in a range of 0.25～6.00 mg/L, which the correlation coefficient was more than 0.997. Through the measurement of real samples, the method recovery was in 31.2%～109.0%, and the RSD was lower than 10%. To summarize, this approach was easy to …
Determination Of Α-Solanine And Α-Chaconine In Potato By Hplc—Elsd, Shang Tingting, Kuang Mengting, Hu Xingxi, Xiong Xingyao, Lu Ying
Determination Of Α-Solanine And Α-Chaconine In Potato By Hplc—Elsd, Shang Tingting, Kuang Mengting, Hu Xingxi, Xiong Xingyao, Lu Ying
Food and Machinery
A method of reversed-phase high performance liquid chromatography (HPLC) coupled with evaporative light scattering detection (ELSD) was developed for the determination of α-solanine and α-chaconine in potato，and determine the contents in different samples. The results showed α- solanine and α- chaconine can be obtained good separation and high efficiency peaks when took 0.1% trifluoroacetic acid water and acetonitrile as mobile phase with gradient elution, and the drift tube of ELSD detector was 98 ℃, the pressure of nebulizing gas was 6.90 kPa. α-solanine and α-chaconine could be extracted with 100 times the mass 1% formic acid in methanol at 70 …