Mechanical Engineering Commons^™

Fabrication, Microstructure And Mechanical Characterization Of Crvnbtaw High Entropy Alloy Coatings Using Magnetron Sputtering, Jorge Quezada

Open Access Theses & Dissertations

In this project a CrVNbTaW high entropy alloy was evaluated. The samples were made using radio frequency magnetron sputtering and were made under similar conditions. The deposition parameters were explored to find the ideal deposition process. The process included a pressure from 0.1-2mTorr, 600C, 1 hour duration, at 100W power to guns, and constant argon flow. The samples were fabricated under similar parameters using silicon steel and sapphire substrates. The samples were analyzed and characterized using X-ray diffraction, scanning electron microscopy, atomic force microscopy, nanoindentation and corrosion testing. Based on these results we were able to get a better understanding …

Fabrication And Characterization Of Iron-Based Catalysts For The Dehydrogenation Of Fossil Fuels, Victoria Isabel Reyes

Open Access Theses & Dissertations

For a prosperous and sustainable future, hydrogen is an encouraging solution due to its simple transition for industrial decarbonization and synergy for economic development. Paradoxically, current hydrogen production pathways release substantial amount of greenhouse gases into the atmosphere contributing to climate change. To keep up with increasing demand, hydrogen could be produced through microwave-assisted thermocatalytic dehydrogenation of fossil fuels without emitting carbon dioxide. This requires specified catalysts to meet the requirements of hydrogen yield and selectivity. The objective of the present research is to fabricate, characterize, and compare iron-based alumina (FeAl_x O_y) catalysts produced via solution combustion synthesis and iron-based …

Evaluation And Implementation Of Lean Engineering Principles For Improving A University Rocket Team, Alan Garcia

Open Access Theses & Dissertations

In the present day, lean is a tool applied to manufacturing industries trying to reduce wasteand non-value-added work to every process during the supply chain. While implementing lean thinking in the industry has been highly effective, it is less common for academic purposes. However, it can also improve performance if the concept is correctly applied. The purpose of this thesis is to show and analyze the application of Lean Engineering thinking and its six principles to the Sun City Summit Rocket Team from the University of Texas at El Paso which competed in the Intercollegiate Rocket Engineering Competition (IREC) Spaceport …

Multi-Sensor Signatures From Ultrasonic Wire Embedding Used In Hybrid Additive Manufacturing, Patrick Steven Gutierrez

Open Access Theses & Dissertations

Additive Manufacturing (AM) has matured such that its products are used in applications ranging from prototypes to end-use parts; however, to expand the adoption of AM, the inclusion of multiple manufacturing technologies has become a focus area especially when the result is a 3D printed part with an embedded electrical system. The W.M. Keck Center for 3D Innovation has developed the Foundry Multi3D system consisting of two material extrusion AM machines, a robotic arm, and a CNC machine equipped with a laser soldering tool, solder micro-dispensing tool and an ultrasonic wire embedding (USWE) tool. The focus of this paper is …

Thin Film Evaporation Through Engineered Copper Micropillar Arrays, Alejandro Amador

Open Access Theses & Dissertations

This work explored and characterized the evaporator section of a fully engineered heat pipe, a proposed semi-passive cooling solution for the thermal management at high heat fluxes, with the use of thin film evaporation. High heat loads present a problem in electronics, circuitry, space, and defense applications which are the main target areas for this cooling solution. Conventionally manufactured flat samples made of copper micropillar arrays were tested to determine their heat removal capabilities for high heat flux applications. The samples were manufactured with 400 μm micropillar hydraulic diameter, various micropillar spacings ranging from 500-1100 μm, with 500 μm and …

Characterization Of A Flex-Fuel Oxy-Combustion System Through Experimental Investigation And Computational Modeling, Md Mohieminul I. Khan

Open Access Theses & Dissertations

Oxy-fuel combustion has the potential to offer high thermal efficiency and lower pollutants emission compared to other existing combustion technologies. More than 63% of the worldâ??s electricity is produced by fossil fuel combustion which also is the major reason for greenhouse gas emissions. Oxy combustion offers a solution to it. Oxy combustion uses pure oxygen as an oxidizer instead of air which eliminates the NOx and SOx products from the exhaust. In oxy-combustion flue gas mainly consists of CO2 and water vapor. Furthermore, combustion in presence of pure oxygen results in higher flame temperature and hence promises higher thermal efficiency. …

Optimization Of Lattice Structure Using Machine Learning Approach, Tanzila Bint Minhaj

Open Access Theses & Dissertations

The goal line of designing any structure is to get maximum performance at minimum cost. Therefore, optimization is the only method to achieve that objective. Engineers have been practicing different formats of optimization. Topological optimization is one of the well-known long-practiced methods. But it is always desired to find the most helpful design method that considers every relevant parameter associated with the structure. In the continuation of this search to enhance the efficacy of design through optimization, a new approach was explored in the following work. The motivation was to enable a model to be capable of finding out the …

Characterization Of 3d Printed Parts Containing Integrated Functionality Via Ultrasonically Embedded Wires, David Abraham Sepulveda

Open Access Theses & Dissertations

Material extrusion additive manufacturing has been widely adopted because it offers freedom of design, which allows complex geometry fabrication, and rapid prototyping. Interest in producing components with integrated functionality allowed forms of hybrid manufacturing to be developed such as the Multi3D system. This system produces parts with embedded components by combining additive, subtractive, soldering, dispensing, and embedding techniques. However, this involves pausing the printing process (which takes place in a controlled environment) and exposing it to ambient temperature where embedding takes places. In this research, the effect of embedding parts with 24 AWG copper for improved functionality was quantified mechanically. …

Multi-Material/Fiber/Particulate Selective Laser Sintering System Capable Of Local Composition Control And Material Gradients, Jonathan James Slager

Open Access Theses & Dissertations

Multi-material (M2) manufacturing with functional gradients and local composition control (LCC) is an emerging technology with high demand in numerous industries. This research investigated multi-material technology that has potential impact to joint implants, synthetic joints, and damage resistant parts. Novel manufacturing subsystems within established selective laser sintering (SLS) additive manufacturing processes were pioneered to enable printing M2 parts with LCC and functionally graded materials. Powder bed fusion (PBF) material blends consisting of low temperature thermoplastics, low temperature thermoplastic elastomers (TPE), carbon fibers (CF), and hydroxyapatite (HA) particulates were explored to match the designed and tested M2 SLS prototype. M2 sintering, …

A Central Compact Hybrid-Variable Method With Spectral-Like Resolution, Md Mahmudul Hasan

Open Access Theses & Dissertations

Numerical methods for hyperbolic conservation laws have been a driving force for theresearch in scientific computing and simulation science in the past decades, as many physical, biological, and engineering systems are governed by these equations, such as fluid mechanics, tumor growth, and virtual wind tunnel simulations. Despite the existence of many schemes in the literature, people have never stopped searching for more accurate and efficient methods for these problems. Indeed, the increasing complexity of systems in emerging applications demands better resolution of sub-grid scale phenomenon whereas classical methods usually fail to deliver high-fidelity simulation results of such systems within realistic …

Suitability Of Low-Cost Additive Manufacturing For Polymer Electrolyte Fuel Cells, David Alexander

Open Access Theses & Dissertations

The purpose of this dissertation is to study the feasibility of low-cost additive manufacturing to fabricate polymer electrolyte fuel cell bipolar plate materials. Traditional manufacturing techniques include molding, milling, hollow embossing, hydro-forming, rolling, and electromagnetic forming. These processes are employed when a design has been selected due to higher costs at low volumes. The combination of high initial costs and bipolar plates being the most expensive component of the polymer electrolyte fuel cell creates incentive to mitigate this obstacle. The feasibility of low-cost additive manufactured bipolar plates will be proven by fabrication, post-processing, and characterization of printed test specimen. The …

Material Synthesis And Additive Manufacturing Of Ceramics, Elsa Bramasco-Rivera

Open Access Theses & Dissertations

This research is divided into two main topics: vitrimer polymers and alumina ceramics. Additive manufacturing is an emerging technology. In this research, two main methods of additive manufacturing are used: material extrusion and vat photopolymerization. The hypothesis of self-healing and mechanochromism functionalities was tested through the synthesis of vitrimers, a novel material combining properties of both thermosets and thermoplastics. These vitrimers were 3D printed using material extrusion. Casted vitrimers showed stiffening effects after submergence in water. Lithography based ceramics have gained attention in recent years due to their wide range of applications. Alumina ceramics were additively manufactured using digital light …

Application Of The Continuum Damage Mechanics Wilshire-Cano-Stewart (Wcs) Model, Jaime Aaron Cano

Open Access Theses & Dissertations

In this study, the applications of the continuum damage mechanics-based Wilshire-Cano-Stewart (WCS) model are explored to predict rupture time, minimum-creep-strain-rate (MCSR), damage, damage evolution, and creep deformation. Increase knowledge in manufacturing methods has pushed the limit of material science and the development of new materials. Conventional testing is required to qualify materials against creep which according to the ASME B&PV III code, 10,000+ hours of experiments are necessary for each heat before materials are put into service. This process is costly and not feasible for new materials. As an alternative, models have been employed to predict creep behaviors and reduce …

Femtosecond Laser Machining Of Drilled Holes In Silicon Nitride, Stephani Nevarez

Open Access Theses & Dissertations

In this study, the laser drilling parameters of a Nd:YAG ultrashort pulsed laser are evaluated to produce zero taper through holes on silicon nitride ceramics. Manufacturing of ceramics is expensive and difficult because of the mechanical and thermal properties of ceramics, limiting applications. Additionally, the high level hardness of the ceramic can affect the ceramic and the manufacturing tool. There is a need to explore non-contact machining such as laser machining to expand the uses of ceramics in industry applications.In order to accomplish this goal, understanding of the physical mechanisms that occurs while laser ablation is needed. Furthermore, the minimum …

All-In-One Multi3d System: Exploring Potential Of 5-Axis Material Extrusion Additive Manufacturing, Angel Vega

Open Access Theses & Dissertations

Additive Manufacturing (AM) has experienced consistent growth since its inception across its seven process categories, especially Material Extrusion (MEX) with systems that can be seen in commercial and industrial settings. As MEX evolves, innovation can be traced in the growing variety of available process materials and new system capabilities leading to greater interest in the technology across various industries including automotive, aerospace and even nuclear weapons. This has created an increasing demand for end-use parts from MEX systems leading to more complex machines with additional Degrees of Freedom (DoF), specialized workflows, and expanded post processing that address the drawbacks of …

Material Synthesis And Machine Learning For Additive Manufacturing, Jaime Eduardo Regis

Open Access Theses & Dissertations

The goal of this research was to address three key challenges in additive manufacturing (AM), the need for feedstock material, minimal end-use fabrication from lack of functionality in commercially available materials, and the need for qualification and property prediction in printed structures. The near ultraviolet-light assisted green reduction of graphene oxide through L-ascorbic acid was studied with to address the issue of low part strength in additively manufactured parts by providing a functional filler that can strengthen the polymer matrix. The synthesis of self-healing epoxy vitrimers was done to adapt high strength materials with recyclable properties for compatibility with AM …

Supercritical Co2 Recompression Closed Brayton Cycle Analysis, Andres Eduardo Gutierrez Hernandez

Open Access Theses & Dissertations

On this research, the results of an analysis made of a Supercritical Carbon Dioxide (sCO2) Recuperated Closed Brayton Cycle (RCBC) done by performing theorical calculations and comparing it to the results obtained with the use of the software ASPEN Plus will be presented. To demonstrate and determine that this software is a useful tool for modeling the proposed type of cycle, a preliminary comparison was made to verify with previous studies found in literature. A comparison and analysis between the possible working fluids and thermal energy sources was also performed to emphasize the decision of using CO2 as the cycle …

Fabrication Of Alloy 625 Through Electron Beam Powder Bed Fusion Additive Manufacturing, Characterization And Mechanical Performance, Aldo Rubio Hidalgo

Open Access Theses & Dissertations

Electron Beam Powder Bed Fusion (EB-PBF) is an additive manufacturing process that allows for the fabrication of nearly fully dense Alloy 625 parts. In this study EB-PBF Alloy 625 samples were fabricated in an Arcam A2X, heat-treated, then machined and tensile tested. Preliminary process tests varying focus offset, and speed function were conducted to establish baseline process parameter conditions to fabricate Alloy 625 parts based on surface finish and structural defects. The microstructure observed in EB-PBF Alloy 625 parts along the build direction in the as-built state consists of irregularly sized columnar grains averaging 105 μm in width that have …

Electron Beam Melted Parameter Development Of Pure Tungsten & Post-Processing Hip And Heat Treatment Of Gamma Titanium Aluminide, Kurtis Isami Watanabe

Open Access Theses & Dissertations

Pure tungsten is a refractory metal and has been gaining interest for the use in nuclear fusion reactors as a plasma facing material. Titanium Aluminide (TiAl) has been growing in popularity as a possibly to phase out Nickel based superalloys due to its high specific strength at elevated temperatures. These two materials suffer from poor machinability due to being brittle at room temperature. Additive manufacturing (AM) is a recently developed manufacturing method that is fundamentally different than formative or subtractive. AM is a layer-by-layer process that has the potential to manufacture metals to a near net shape. Since the AM …

Phase Transformation And Strain Hardening Mechanisms In Advanced Engineering Steels, Hangyu Dong

Open Access Theses & Dissertations

Strain hardening and associated deformation mechanisms play a determining role in the performance of metallic materials. The objective of the doctoral research was to explore and fundamentally understand the strain hardening mechanisms in the next generation of advanced engineering steels. Two main work hardening mechanisms, notably, twinning-induced plasticity (TWIP) and transformation-induced plasticity (TRIP)) were identified that governed strength and ductility. In the nanograined austenitic steel with high strength-high ductility combination, processed by the novel phase reversion concept, twinning-induced plasticity (TWIP) was the governing deformation mechanism and contributed to good ductility. In striking contrast, transformation-induced plasticity (TRIP) was the deformation mechanism …

Synthesis And Characterization Of Tin (Sn) Incorporated Ga2o3, Guillermo Nicolas Gutierrez

Open Access Theses & Dissertations

In this work, we report on the synthesis, characterization of tin (Sn) incorporated gallium oxide Ga2O3 compounds, also included in this work is the effect of tin concentration related to the optical and electrochemical properties. The Sn incorporation into Ga2O3 creates a significant reduction in the bandgap and causes a nonlinear optical activity as the concentration varies. Substantial investigation performed to the structure, phase, and morphology of the mixed compounds governed by the stoichiometry equation Ga2−2xSnxO3-ɗ indicates that the Sn incorporation from 0.00 ≤ x ≤ 0.30 has a significant effect on these properties. To synthesize the Ga-Sn-O compounds a …

Rarified Water Vapor Deposition From Icy Lunar Regolith On An Engineered Cold Plate, Nathaniel Ian Jurado

Open Access Theses & Dissertations

This work presents the fundamental ice collection experiments conducted under rarefied flow regime to develop a high-capacity cryogenic heat pipe for ice recollection on the Moon’s surface. Preliminary ice collection experiments are conducted under cryogenic vacuum environment of 1.5 × 10-2 Torr and -60 °C. The characterization of water vapor sublimation rates from icy lunar regolith (JSC-1A) at various heating powers is established by utilizing a cryogenic thermal vacuum chamber (T-VAC). A custom-built engineered cold plate is designed, manufactured and tested at various degrees of subcooling and vapor sublimation rates. A thin film heater is embedded within the cold plate …

Mechanical Properties And Microstructure Evolution Of Thermally Treated Laser Powder Bed Fusion Alsi10mg, Jorge Merino-Gomez

Open Access Theses & Dissertations

The optimization of mechanical properties with thermal postprocessing treatments was investigated in this study across a wide variety of variants. The relationship between heat treatments and the impacts on the mechanical properties and microstructure of printed materials is a crucial part of additive manufacturing. As a result, the current paper provides a comprehensive overview of postprocess heat treatments for Laser Powder Bed Fusion fabricated AlSi10Mg alloy, including stress relief anneals at 190 and 285 degrees Celsius for 2 hours, hot isostatic pressing at 515 degrees Celsius for 3 hours, hot isostatic pressing + T6 treatment for 6 hours, and final …

Combustion Of Hydroxylammonium Nitrate Based Monopropellants, Robert Edwin Ferguson

Open Access Theses & Dissertations

"Green" monopropellants based on hydroxylammonium nitrate (HAN) are of interest for replacing highly toxic hydrazine in space propulsion systems and for other applications. Further, gelling such propellants may offer additional advantages such as the long-term stability of compositions with added energetic and catalytic particles in suspension. However, the combustion mechanisms of HAN-based monopropellants and the effect of gelling on their combustion characteristics are poorly understood. In the present work, combustion of an aqueous HAN/methanol solution (70.1 wt% HAN and 14.9 wt% methanol) was studied in a strand burner at nitrogen pressures up to 30 MPa. A version gelled with 1 …

Development Of A Laser Solder Process For Use With Material Extrusion Additive Manufacturing And Rapid Electronics Prototyping In Embedded Sensing Applications, Emerson Roland Armendariz

Open Access Theses & Dissertations

Industrial and rapid prototyping (RP) trends toward miniaturization of electronic devices containing temperature sensitive electronics and surrounding materials are calling for highly controllable, selective laser soldering technologies. Laser soldering is a non-contact technique that eliminates the risk of marring or damaging sensitive components by precisely focusing a laser beam on a solder filler alloy, leading to a fast and non-destructive electrical joint. Using the benefits of accurate and controlled heat delivery via inexpensive low power laser diodes (LPDL's) in conjunction with ever-increasing additive manufacturing capability in producing complex internal features and geometries, development and testing of a laser application system …

Synthesis And Characterization Of Functiona Materials For 3d Printed Composites, Elizabeth Irene Reza

Open Access Theses & Dissertations

The following body of work encompasses the synThesis, upscaling, additive manufacturing, and characterization of microspheres as functional fillers incorporated into polymer syntactic foams. Synthesizing microspheres permits control over morphology, dispersion of particles, and size while the use of direct write manufacturing allowed for the controllability of filler orientation. Two different syntactic foams were developed from similar methodologies: (1) a silicone syntactic foam (2) epoxy syntactic foam. The silicone epoxy foam showed an increasing in damping and elastic modulus. The epoxy syntactic foams showed an enhanced thermal and electrical properties.

Multiscale And Multimaterial 3d Printing: Impact Of Feedstock Properties And Processing Parameters On Printed Parts, Kazi Md Masum Billah

Open Access Theses & Dissertations

Material extrusion additive manufacturing (AM) technology is one of the most commonly used technology to fabricate functional prototypes and end-use application parts with custom design. The evolution of the extrusion technology led this particular AM process to grow in many aspects such as new materials development, new design thinking, fabrication of parts in multiscale length, and manufacturing of monolithic parts with multiple functionalities. The research presented in this Dissertation results in the creation of knowledge in material extrusion AM technology with the length scale of production-grade to large-scale 3D printing machine those were used to enable the fabrication of multimaterial …

Fabrication And Testing Of Advanced Composites For Extreme Environments, Victoria Centeno

Open Access Theses & Dissertations

The following research focuses on the additive manufacturing and characterization of epoxy syntactic foams that utilize hollow carbon microspheres (CMS) and graphene-coated hollow carbon microspheres (GCMS) as fillers. The matrix that is utilized in this study is a thermoset epoxy resin, chosen for its high strength, low shrinkage, excellent adhesion to various substrates, effective electrical properties, chemical and solvent resistance, low cost, and low toxicity.1 CMS and GCMS were used as fillers for the properties they contribute to the overall epoxy syntactic foam, and can be seen in Fig.1.1. CMS consist of outer stiff carbon and inner gas, giving the …

Microstructural Evolution And Mechanical Properties Of L-Pbf Aerospace Alloys: Hydride- Dehydride Ti-6al-4v And Experimentally Heat-Treated Inconel 718, Jaime Varela

Open Access Theses & Dissertations

Experimental HIP and heat treatment cycles were applied to Laser Powder Bed Fusion fabricated Inconel 718 parts. Recent advances allow for rapid cooling in the HIPing chamber allowing one unit to perform HIP along with other heat treatment cycles such as solution annealing and ageing. Different cycles yield various effects on the porosity reduction as well as the growth of grain in the microstructure, consequently presented different mechanical properties. Specimens were therefore analyzed for density, microstructure, and tensile properties.

In addition, the mechanical and microstructural analysis of HDH Ti-6Al-4V was performed. The high cost of GA Ti64 material is a …

Effect Of Dopants On The Properties And Performance Of Gallium Oxide: Bulk Ceramics And Nanomaterials, Vishal Bhimrao Zade

Open Access Theses & Dissertations

A comprehensive investigation performed in order to understand the fundamental aspects of transition metal (TM) incorporation into Ga2O3, a wide band gap semiconductor with a huge potential for application in electronics, optics, micromechanics and optoelectronics. An approach is presented to tailor the structural, optical, electrical, mechanical properties of Ga2O3 ceramics and thin films. The tungsten (W) mixed Ga2O3 with variable W at% (Ga2-2xWxO3 ; 0.00 ≤ x ≤ 0.30) were synthesized by the high temperature solid state route involving a 2-step calcination process. The solubility limits and phase stability of the compounds are established. While solubility and phase stability occur …