A Nanoindentation Study Of The Fatigue Properties Of Al/A-Si Core-Shell Nanostructures, Jason Steck

Mechanical Engineering Undergraduate Honors Theses

Nanostructure-textured surfaces can reduce friction and increase the reliability of micro- and nanoelectromechanical systems (NEMS/MEMS). For MEMS incorporating moving parts, the fatigue properties of nanostructures pose a challenge to their reliability in long-term applications. In this study, the fatigue behavior of hemispherical Al/a-Si core-shell nanostructures (CSNs), bare hemispherical Al nanodots, and a flat Al/a-Si layered thin film have been studied using nanoindentation and nano-scale dynamic mechanical analysis (nano-DMA) techniques. Fatigue testing with nano-DMA shows that the deformation resistance of CSNs persists through 5.0 × 10⁴ loading cycles at estimated contact pressures greater than 15 GPa. When the a-Si shell …

Understanding The Evolution Of Surface Texture Under Boundary Lubrication, Salil T. Bapat

Graduate Theses and Dissertations

The objective of this research was to understand the evolution of surface texture under boundary/mixed lubrication (BL). Significant material/energy losses occur during BL because of direct contact between the two surfaces. Traditionally, tribofilms have been studied extensively for BL while textures have been used as a static engineering design parameter to enhance lubricant film properties. However, texture is dynamic at the tribological mating interface, where both physical and chemical interactions are continuously modulated. The evolution and the interplay between the tribofilm and texture is least studied in the literature, which is the focus of this research.

MoS2-based lubricants, known for …

Active Permanent Magnet Attitude Control For Cubesats Using Mu-Metal Shielding, Maxwell Martin

Mechanical Engineering Undergraduate Honors Theses

Cube-Satellites (CubeSats) are nanosatellites composed of cube shaped units, each nominally 10cm to a side and around 1kg in mass. Due to their inherent size and weight limitations, it is often impractical to use conventional attitude, or rotational, control methods such as thrusters on these small satellites. Several methods, including magnetorquer rods and small reaction wheels, are often used instead of traditional methods to work around the size and weight limitations. As a new alternative to these methods, a permanent magnet mounted on a rotatable shaft could be used to achieve attitude control. In much the same way that a …

Non-Covalent Functionalization Of Graphene Films For Uniform Nanoparticle Deposition Via Atoic Layer Deposition, Ty Seiwert

Mechanical Engineering Undergraduate Honors Theses

Graphene functionalized with platinum (Pt) and palladium (Pd) has proven to be highly effective as a hydrogen sensor. Deposition methods such as Atomic layer deposition (ALD) can be further enhanced by pretreating the graphene with a non-covalent surfactant prior to nanoparticle deposition. In this study, graphene-based sensing devices will be fabricated by ALD deposition. The graphene will be non-covalently functionalized using sodium dodecyl sulfate (SDS) anionic surfactant prior to ALD deposition. The aim of this study is to test the deposition pattern achieved by varying the amount of time that graphene is treated with the SDS surfactant. Initially, ALD deposition …

Phase Field Model Of Thermally Induced Phase Separation (Tips) For The Formation Of Porous Polymer Membranes, Ashley Green, Aria Green

Mechanical Engineering Undergraduate Honors Theses

Most membrane research and development has been done through experimental work, which can be costly and time consuming. An accurate computational model would greatly reduce the need for these experiments. The focus of the research presented in this paper is to create an accurate computational model for membrane formation using thermally induced phase separation (TIPS). A phase field model is employed to create this model including the Cahn Hilliard Equation and Flory Huggins Theory. This model produced computational results that correspond well with theoretical and experimental results. The model was then adapted to correspond to the PVDF/DPC polymer-solvent system by …

Baseline Data From Servo Motors In A Robotic Arm For Autonomous Machine Fault Diagnosis, Jacob Brown

Mechanical Engineering Undergraduate Honors Theses

Fault diagnosis can prolong the life of machines if potential sources of failure are discovered and corrected before they occur. Supervised machine learning, or the use of training data to enable machines to discover these faults on their own, makes failure prevention much easier. The focus of this thesis is to investigate the feasibility of creating datasets of various faults at both the component and system level for a servomotor and a compatible robotic arm, such that this data can be used in machine learning algorithms for fault diagnosis. The faults induced at the component level in different servomotors include: …

Effects Of Hydration And Mineralization On The Mechanical Behavior Of Collagen Fibrils, Marco Fielder

Graduate Theses and Dissertations

Bone is a composite biomaterial with a structural load-bearing function. Understanding the biomechanics of bone is important for characterizing factors such as age, trauma, or disease, and in the development of scaffolds for tissue engineering and bioinspired materials. At the nanoscale, bone is primarily composed of collagen protein, apatite crystals, and water. Though several studies have characterized nanoscale bone mechanics as the mineral content changes, the effect of water, mineral, and carbon nanotube (CNT) content and distribution in fibril gap and overlap regions is unexplored. This study used molecular dynamics to investigate the change in collagen fibril deformation mechanisms as …

Development Of Microdialysis Probes In Series Approach Toward Eliminating Microdialysis Sampling Calibration: Miniaturization Into A Pdms Microfluidic Device, Randy Espinal Cabrera

Graduate Theses and Dissertations

A new microdialysis sampling method and microfluidic device were developed in vitro. The method consisted of using up to four microdialysis sampling probes connected in series to evaluate the relative recovery (RR) of different model solutes methyl orange, fluorescein isothiocyanate (FITC)-dextran average mol. wt. 4,000 (FITC-4), FITC-10, FITC-20, and FITC-40. Different flow rates (0.8, 1.0, and 1.5 µL/min) were used to compare experimentally observed relative recoveries with theoretical estimations. With increasing the number of probes in series, the relative recovery increases and ~100% (99.7% ± 0.9%) relative recovery for methyl orange was obtained. For larger molecules such as fluorescein isothiocyanate …

Phase Transitions In Monochalcogenide Monolayers, Mehrshad Mehboudi

Graduate Theses and Dissertations

Since discovery of graphene in 2004 as a truly one-atom-thick material with extraordinary mechanical and electronic properties, researchers successfully predicted and synthesized many other two-dimensional materials such as transition metal dichalcogenides (TMDCs) and monochalcogenide monolayers (MMs). Graphene has a non-degenerate structural ground state that is key to its stability at room temperature. However, group IV monochalcogenides such as monolayers of SnSe, and GeSe have a fourfold degenerate ground state. This degeneracy in ground state can lead to structural instability, disorder, and phase transition in finite temperature. The energy that is required to overcome from one degenerate ground state to another …

Exploring Energy, Comfort, And Building Health Impacts Of Deep Setback And Normal Occupancy Smart Thermostat Implementation, Zachary Ethan Alderman

Graduate Theses and Dissertations

As smart thermostat adoption rates continue to increase, it becomes worthwhile to explore what unanticipated outcomes may result in their use. Specific attention was paid to smart thermostat impacts to deep setback and normal occupancy states in a variety of conditions while complying with the ventilation and temperature requirements of ASHRAE 90.2-2013. Custom weather models and occupancy schedules were generated to efficiently explore a combination of weather conditions, building constructions, and occupancy states. The custom modeling approach was combined with previous experimental data within the Openstudio graphics interface to the EnergyPlus building modeling engine. Results indicate smart thermostats add the …

3d Printed Pcu/Uhmwpe Polymeric Blends For Artificial Knee Meniscus, Raissa Araujo Borges

Graduate Theses and Dissertations

3D printing was used to fabricate porous artificial knee meniscus material from biocompatible polymeric blends of polycarbonate-urethane (PCU) and ultra-high-molecular-weight polyethylene (UHMWPE) to enable “weep” lubrication that mimics the native meniscus. 3D printed and molded pure PCU, as well as molded PCU and UHMWPE, were used for comparison. Preliminary printing was done to evaluate the impact of process parameters on the results. The samples were subject to a variety of rotational oscillating friction and wear tests under simulated body fluid and loading conditions to replicate the natural motion of the knee. Results show that 3D printed PCU samples yielded a …

Developing Methods Of Obtaining Quality Failure Information From Complex Systems, Oladapo Olalekan Bello

Graduate Theses and Dissertations

The complexity in most engineering systems is constantly growing due to ever-increasing technological advancements. This result in a corresponding need for methods that adequately account for the reliability of such systems based on failure information from components that make up these systems.

This dissertation presents an approach to validating qualitative function failure results from model abstraction details. The impact of the level of detail available to a system designer during conceptual stages of design is considered for failure space exploration in a complex system. Specifically, the study develops an efficient approach towards detailed function and behavior modeling required for complex …

Deformation Behavior Of Al/A-Si Core-Shell Nanostructures, Robert Andrew Fleming

Graduate Theses and Dissertations

Al/a-Si core-shell nanostructures (CSNs), consisting of a hemispherical Al core surrounded by a hard shell of a-Si, have been shown to display unusual mechanical behavior in response to compression loading. Most notably, these nanostructures exhibit substantial deformation recovery, even when loaded much beyond the elastic limit. Nanoindentation measurements revealed a unique mechanical response characterized by discontinuous signatures in the load-displacement data. In conjunction with the indentation signatures, nearly complete deformation recovery is observed. This behavior is attributed to dislocation nucleation and annihilation events enabled by the 3-dimensional confinement of the Al core. As the core confinement is reduced, either through …

A Spreadsheet Algorithm For Determining The Economic Feasibility Of Micro-Chp Systems In The Arkansas Manufacturing Sector, Ford R. Lewallen

Graduate Theses and Dissertations

Combined heat and power (CHP) systems are not new to the market. However, advances in technology, specifically MicroTurbines, have presented new opportunities for installations of micro-CHP units - defined as 50 kWe to 300 kWe, specifically at small- to medium-sized industrial facilities. One pressing concern is whether or not an industrial plant has a high enough process thermal load requirement to fully utilize the energy output.

This thesis will discuss simulations that were run on several actual electric and thermal load combinations, which correspond to types of manufacturing facilities commonly found in Arkansas. Analysis of the plant usage profiles will …

An Economic Analysis Of Residential Photovoltaic Systems With And Without Energy Storage, Rodney Moses Kizito

Graduate Theses and Dissertations

Residential photovoltaic (PV) systems serve as a source of electricity generation that is separate from the traditional utilities. Investor investment into residential PV systems provides several financial benefits such as federal tax credit incentives for installation, net metering credit from excess generated electricity added back to the grid, and savings in price per kilowatt-hour (kWh) from the PV system generation versus the increasing conventional utility price per kWh. As much benefit as stand-alone PV systems present, the incorporation of energy storage yields even greater benefits. Energy storage (ES) is capable of storing unused PV provided energy from daytime periods of …

Energy From Chemical Reactions: Understanding The Combustion Engine, Tammy Guthrie, Kathy Prophet, Greg Herzig, Cassie Kautzer

Middle School Lesson Plans

Automobiles produce a large amount of heat generated by the burning of gasoline. Burning gasoline is a chemical reaction that causes a phase change. This is called combustible energy. During combustion fuel combines with oxygen to release energy (such as heat, light, sound) along with another product that is often considered waste. Most of the energy produced is not used to power the automobile, but is released as heat. 19.3 pounds of the greenhouse gas, carbon dioxide, is produced from the combustion of 1 gallon of U.S. gasoline according to the U.S. Energy Information Administration.

Kinetic Energy Investigation, Mike Jackson

High School Lesson Plans

Students will build a mouse trap powered car that converts elastic potential energy contained in the trap’s spring to linear kinetic energy of the car. The release of this energy results in a net force which leads to linear acceleration. This acceleration can be measured with Vernier Logger Pro®, and using Newton’s Second Law of Motion, the net force can be calculated. Finally, using the concept of work, the final kinetic energy of the car can be calculated. Once students become familiar with the calculation of work and energy, the teacher will challenge the students to modify their cars to …

Computer Simulation Of Pore Migration Due To Temperature Gradients In Nuclear Oxide Fuel, Ian Wayne Vance

Graduate Theses and Dissertations

A phase-field simulation model is being presented that captures the thermal-gradient-driven migration of pores in oxide fuel associated with fuel restructuring. The model utilizes a Cahn-Hilliard equation supplemented with an advection term to describe the vapor transport of fuel material through the pore interior due to gradients in vapor pressure. In addition, the model also captures changes in a migrating pores’ morphology. Simulations demonstrate that the model successfully predicts pore migration towards the hottest portion of the fuel, the centerline. The simulations also demonstrate changes in pore shape that are in agreement with previous experimental observations. Initially isotropic pores are …

Characterization Of Plastic Deformation Evolution In Single Crystal And Nanocrystalline Cu During Shock By Atomistic Simulations, Mehrdad Mirzaei Sichani

Graduate Theses and Dissertations

The objective of this dissertation is to characterize the evolution of plastic deformation mechanisms in single crystal and nanocrystalline Cu models during shock by atomistic simulations. Molecular dynamics (MD) simulations are performed for a range of particle velocities from 0.5 to 1.7 km/s and initial temperatures of 5, 300 and 600 K for single crystal models as well as particle velocities from 1.5 to 3.4 km/s for nanocrystalline models with grain diameters of 6, 11, 16 and 26 nm. For single crystal models, four different shock directions are selected, <100>, <110>, <111> and <321>, and dislocation density behind the shock wave …

Feasibility Of Using Oxide Thickness Measurements For Predicting Crack Growth Rates In P91 Steel Components, Ralph Edward Huneycutt Iv

Graduate Theses and Dissertations

There are only few methods available for predicting the age of cracks that are found in high

temperature structural components during service; among the promising ones is the oxide

thickness measurement technique. Oxide thickness profiles are taken from crack surfaces of

components and used for predicting the rates of crack propagation. This technique is particularly

suitable for high temperature components fabricated from ferritic steels commonly used in power

plants that run on fossil fuels. To implement this technique, it is necessary to fully understand the

kinetics of high temperature oxidation in these steels. In this study, the oxidation characteristics

of …

Blood-Brain Barrier-On-A-Chip Systems Based On 3d Printing, Cade I. Harding

Mechanical Engineering Undergraduate Honors Theses

This research focused on the design and testing of a blood-brain barrier (BBB)-on-a-chip microfluidic device produced using 3D printing. First, COMSOL simulations were used to define dimensions of the microchannel that would most accurately replicate the flow environment imposed on the blood-brain barrier, the wall shear stress being the most important characteristic. In using COMSOL, water was used as the simulated fluid and also the testing fluid in the fabricated devices. Therefore, the microsystem is designed to produce the BBB environment using water instead of blood. The numerical simulation parameters were based on theoretical calculations performed to scale up the …

Chip-Package Interfacial Stress Analysis And Reliability Implications For Flip-Chip Power Devices, Jonathan Gh Treco

Mechanical Engineering Undergraduate Honors Theses

The solder in flip-chip assemblies experience high stress and strain because of thermal mismatch induced deformation. These deformations occur because of the differences of coefficient of thermal expansion between flip-chip assembly materials. The similarly in stress profiles between thermal induced and shear induced stress in solder joints enable the use of die shear testing as a representative technique for relating the max stress the flip-chip can withstand to cyclic thermal fatigue failures. In this work, two electronic device sample preparation types are evaluated: One set of samples are soldered together and other set of samples use epoxy as an adhesive. …

Optimization Of Reduced Graphene Oxide Deposition For Hydrogen Sensing Technologies, Matthew Pocta

Mechanical Engineering Undergraduate Honors Theses

Graphene is known to be a key material for improving the performance of hydrogen sensors. High electrical conductivity, maximum possible surface area with respect to volume, and high carrier mobility are a few of the properties that make graphene ideal for hydrogen sensing applications. The problem with utilizing graphene is the difficulty in depositing uniform, thin layers onto substrate surfaces. This study examines a new method of optimizing graphene deposition by utilizing an airbrush to deposit both graphene oxide (GO) and reduced graphene oxide (rGO) onto glass substrates. The number of depositions were varied among samples to study the effect …

System-Layout-Dependent Thermally Induced Solder Stress & Reliability Implications, Ange C. Iradukunda

Mechanical Engineering Undergraduate Honors Theses

Electronic flip chip assemblies consist of dissimilar component materials, which exhibit different CTE. Under thermal cyclic operating conditions, this CTE mismatch produces interfacial and interconnect stresses, which are highly dependent on system layout. In this paper, sensitivity analyses are performed using ANSYS FEA to establish how the proximity and arrangement of neighboring devices affect interconnect stress. Flip chip alignment modes ranging from edge-to-edge to corner-to-corner are studied. Results of these FEA studies, demonstrated that closely packing devices together has the effect of making them act as one. This results in a significant increase in the thermomechanical stresses induced on peripheral …

Determining Drag Forces On 3d Printed Shark Skin And The Conditions In Which Drag Forces Are Reduced, Kayla M. Bartnicke

Mechanical Engineering Undergraduate Honors Theses

ABSTRACT

This project was conducted at the University of Arkansas with access to 3D printers and a water tunnel. The project examines drag forces over 3D-printed shark skin. Shark skin was chosen to be studied because of its unique three-pronged denticle shape and the assumption that this unique shape has a purpose, such as drag reduction.

A shark denticle was designed using SolidWorks software, multiplied 164 times creating a total skin area of 17.5 in², and printed using both a MakerBot Replicator 2 3D printer and an Ultimaker 2 Go 3D printer. The shark skin was initially printed …

Selective Resistive Sintering: A Novel Additive Manufacturing Process, Austin Bryan Van Horn

Graduate Theses and Dissertations

Selective laser sintering (SLS) is one of the most popular 3D printing methods that uses a laser to pattern energy and selectively sinter powder particles to build 3D geometries. However, this printing method is plagued by slow printing speeds, high power consumption, difficulty to scale, and high overhead expense. In this research, a new 3D printing method is proposed to overcome these limitations of SLS. Instead of using a laser to pattern energy, this new method, termed selective resistive sintering (SRS), uses an array of microheaters to pattern heat for selectively sintering materials. Using microheaters offers significant power savings, significantly …

Haul Truck Tires Recycling, Omkar Bhave

Chemical Engineering Undergraduate Honors Theses

The disposal of large Off-the-Road (OTR) tires is an increasingly important concern. These tires can weigh up to 8,450 pounds with an overall diameter and width of approximately 140.7 inches and 45.1 inches respectively. OTR tires are used for mining vehicles such as haul trucks, wheel loaders, backhoes, graders, and trenchers.[1] These new tires cost between $38,000 and $50,000 each, depending on multiple factors including oil prices and the cyclical nature of the industry. Haul trucks contain six tires per vehicle, and mines replace these tires around every 9-12 months.[2] Statistics regarding discarded OTR tires are not provided by the …

The Effect Of Process Parameters And Surface Condition On Bond Strength Between Additively Manufactured Components And Polymer Substrates, Bharat Bhushan Chivukula

Graduate Theses and Dissertations

Additive patching is a process in which printers with multiple axes deposit molten material onto a pre-defined surface to form a bond. Studying the effect of surface roughness and process parameters selected for printing auxiliary part on the bond helps in improving the strength of the final component. Particularly, the influence of surface roughness, as established by adhesion theory, has not been evaluated in the framework of additive manufacturing (AM). A full factorial design of experiments with five replications was conducted on two levels and three factors, viz., layer thickness, surface roughness, and raster angle to examine the underlying effects …

4d Printing Dielectric Elastomer Actuator Based Soft Robots, Jiyu Cai

Graduate Theses and Dissertations

4D printing is an emerging technology that prints 3D structural smart materials that can respond to external stimuli and change shape over time. 4D printing represents a major manufacturing paradigm shift from single-function static structures to dynamic structures with highly integrated functionalities. Direct printing of dynamic structures can provide great benefits (e.g., design freedom, low material cost) to a wide variety of applications, such as sensors and actuators, and robotics. Soft robotics is a new direction of robotics in which hard and rigid components are replaced by soft and flexible materials to mimic mechanisms that works in living creatures, which …

Go With The Flow –Thermoelectric Energy, Shawn Bell

Middle School Lesson Plans

In this unit, students will learn how thermal energy be transferred and transformed. They will carry out investigations to gather evidence to support an explanation about direct conversion of heat into electrical energy. They will develop a model that shows the components of the system and changes in the system being investigated, and they will use evidence from the investigation to construct an explanation for how the energy flows.