Mechanical Engineering Commons^™

Multifunctional Carbon/Epoxy Glass Microballons Nanocomposite, Ephraim Fentahun Zegeye

LSU Doctoral Dissertations

Glass microballoons have high strength, low thermal and electrical properties, and provide closed cell porosity to reduce the density of composites. On the other hand, filamentous carbon nanostructures have excellent mechanical, thermal, and electrical properties that make them naturally multifunctional. This work presents a method of developing low-density multifunctional nanocomposites utilizing glass microballoons and carbon nanostructures. Two different approaches are investigated. In the first approach, carbon nanotubes (CNTs) are used as a filler material to fabricate nanocomposites containing glass microballoons (CNT-syntactic foams). The weight percent of CNTs is varied from 0 to 0.8 wt%. In this method, CNTs were grown …

Multiscale Viscoplastic-Viscodamage Analysis Of Shape Memory Polymer Fibers With Application To Self Healing Smart Materials, Amir Shojaei

LSU Doctoral Dissertations

Self-healing smart material systems have been introduced into the research arena and they have already been deployed into industrial applications. The Close-Then-Heal (CTH) healing mechanism for polymeric self-healing systems is addressed herein and then a new generation of Shape Memory Polymer (SMP) based self-healing system is proposed in this work. This system incorporates SMP fibers to close the cracks while the embedded Thermoplastic Particles (TPs) are diffused into the crack surfaces upon heating and provide a molecular level of healing. The SMP fiber manufacturing procedure is briefly addressed in this work in which the bobbin of SMP fibers are heat …

Pdms Based Waveguides For Microfluidics And Eocb, Weiping Qiu

LSU Master's Theses

Due to the low cost, fast and ease of molding, PDMS has become one of the most popular materials for microfluidics devices, bioMEMS applications. Meanwhile, the integration of different functional components on to one single chip (or Lab on a Chip) is the dream for many scientists and engineers in the related area. In addition to the necessary mechanical components for accommodating the reactions, such as pumps, valves, mixers and so on, optical components such as waveguides, lens, interferers are all desired to be lumped into such a system.

The waveguide for such a system requires the material to have …

Small Footprint High Flow Rate Microdevice For Rare Target Cell Capture, Taehyun Park

LSU Doctoral Dissertations

A novel high flow rate cell capture design was introduced to overcome the limitations of the current technologies or methods for rare target cell capture. Even though the rare target cell capture using BioMEMS technology has great potential for cancer diagnosis, previous rare cell capture research could not overcome the limitations of low flow rate or low recovery rate. Rare cell research requires precise sample preparation for accurate results. A new method of preparation for a single or a precise number of target cell was introduced. Current sample preparation methods which are not suitable for rare cell research, such as …

A Biomimic Self-Healing Shape Memory Polymer Based Syntactic Foam For Smart Structural Composites, Jones Nji

LSU Doctoral Dissertations

This study explored the development of a new self-healing Polystyrene Shape Memory Polymer (PSMP) based syntactic foam for service life extension in structural polymeric composites. The objective was to self-heal structural-length scale damage in an autonomous, efficient, timely and repeatable manner at the molecular-length scale. Self-healing is achieved through a novel two step close-then-heal (CTH) self-healing scheme, designed to mimic the natural biological process of wound healing in humans. A new methodology to fabricate three-dimensional (3-D) fiber reinforced shape memory polymer syntactic foam for structural applications was developed. The effect of impact energy on the ability for the 3-D fiber …

On The Thermodynamics Of Degradation, Mehdi Amir Darehbidi

LSU Doctoral Dissertations

All materials when subjected to fatigue loading are prone to failure if the number of cycles exceeds a certain level. Prediction of the number of cycles to failure is, therefore, of utmost importance in nearly all engineering applications. The existing methods for evaluating the fatigue life are tedious, expensive, and extremely time consuming as fatigue often takes many thousands to millions of cycles until failure occurs. Therefore, methods that can readily estimate the number of cycles to failure are highly desirable. In this work, innovative solutions to fatigue problems are presented and their practical significance is discussed. The premise of …

Effect Of Piezoelectric Actuation On Curved Beams And Single Lap Joints, Calicia Johnson

LSU Master's Theses

Piezoelectric materials have seen a significant usage increase over the past decade. They have been found to be effective as either sensors or actuators in smart structure applications, which allows them to act more as an adaptive system rather than a passive system. Piezoelectric materials are very effective transducers which convert mechanical energy into electrical energy, known as the direct piezoelectric effect or they have the ability to convert electrical energy to mechanical energy, known as the converse piezoelectric effect. The absence of additional mechanical parts, its lightweight and high strength to weight ratio is what make piezoelectric materials so …

The Design And Modification Of A Sputter System For Dc Reactive Sputtering Of Alumina And Zirconia Thin Films, Diane Van Ho

LSU Master's Theses

Yttria-stabilized zirconia (7% YSZ) is the most used material for thermal barrier coatings (TBCs) to reduce the conductive heat transfer on turbine blades, but it is not resistant to infrared radiation. In order to reduce radiation heat transfer, alternating materials, such as alumina and zirconia, can be used to fabricate multi-layer coatings in which each layer is optimized to reflect a targeted range of wavelength. This research aims to fabricate these multi-layer coatings by reactive magnetron sputtering. Reactive magnetron sputtering is the sputtering of an elemental target in the presence of a reactive gas that will react with the target …

Two-Stage Biaxial Thermomechanical Cycle Of Shape Memory Polymer Based Syntactic Foam, Abraham Michael King

LSU Master's Theses

A shape memory polymer (SMP) is a polymeric material that exhibits shape memory behavior. It can be “programmed” to take on a desired shape and “recovered” to revert back to its original shape. This ability to remember multiple shapes and switch between them with the application of a stimulus from an outside source is very desirable in certain applications. By dispersing glass microspheres in a SMP matrix, a syntactic foam is created that retains much of the shape memory capabilities but has higher strength and lower density than the pure SMP. These characteristics make this material a good candidate for …

Pool Boiling Enhancement Via Micro Ratchets, Lance Austin Brumfield

LSU Master's Theses

Nucleate boiling is an attractive method for achieving high heat flux at low superheat temperatures. It is frequently used for industrial applications such as heat exchangers and is being considered to cool advanced central processing units (CPU) which produce heat fluxes on the order of 1 MW/m2 and are becoming increasing less efficient to cool via forced conduction of air. The issues with implementing nucleate boiling as a cooling mechanism lies in the difficulty of quantifying the complex and numerous mechanisms which control the process. A comprehensive nucleate boiling model has yet to be formulated and will required in order …

Gas Turbine Blade Tip And Near Tip Heat Transfer With Film Cooling, Gregory Kramer

LSU Master's Theses

Gas turbine blade tips experience very high thermal loads due to high temperature combustion gases and tip leakage flows. This leads to the tip region being very susceptible to experiencing failures. To better understand these effects, experiments were performed in a suction-type low speed wind tunnel cascade to determine heat transfer coefficients and film cooling effectiveness distributions on a highly-loaded 2-D gas turbine blade model in the tip and near-tip regions. The blade shape was generated to match the pressure coefficients of the operating turbine blade design. The model featured multiple tip and pressure side film cooling holes and a …

Design, Fabrication And Characterization Of A New Wind Tunnel Facility – Linear Cascade With A Wake Simulator, Jean-Philippe Junca-Laplace

LSU Master's Theses

A new wind tunnel has been designed and constructed at the LSU Mechanical Engineering Laboratories. The objective was to design a versatile test facility, suitable for a wide range of experimental measurements on turbine blades. The future study will investigate the impact of unsteady inflow conditions on film cooling performance. More specifically, it will study how the unsteady flow due to the upstream passing wakes coming from the front row vane affects the film cooling performances on the turbine blades. The test section consists of a four passage linear cascade composed of three full blades and two shaped wall blades. …

Thermodynamic Approach To Fatigue Failure Analysis In Metals And Composite Materials, Mehdi Naderi Abadi

LSU Doctoral Dissertations

Fatigue is a dissipative process and must obey the laws of thermodynamics. In general, it can be hypothesized that the degradation of machinery components is a consequence of irreversible thermodynamic processes that disorder a component, and that degradation is a time dependent phenomenon with increasing disorder. This suggests that entropy —a fundamental parameter in thermodynamics that characterizes disorder— offers a natural measure of component degradation. The majority of the existing methods for prediction of fatigue are limited to the study of a single fatigue mode, i.e., bending or torsion or tension-compression. Further, the variability in the duty cycle in a …

Embedded Piezoelectric Fiber Composite Sensors For Applications In Composite Structures, Hari Prasad Konka

LSU Doctoral Dissertations

Health monitoring of the composite structures is an important issue that must be addressed. Embedded sensors could be an effective way to monitor the health of composite structures continuously and which could also avoid the catastrophic failures of composite structures. Piezoelectric-fiber-composite sensors (PFCS) made from micro-sized Lead Zirconate Titanate (PZT) fibers have great advantages over the traditional bulk PZT sensors for embedded sensor applications. PFCS as an embedded sensor will be an ideal choice to continuously monitor the stress/strain levels and health conditions of composites. This work presents a critical study on using PFCS as an effective embedded sensor within …

V2o5-Wo3 Composite Films And Surface-Coated Licoo2 For Enhanced Li-Ion Intercalation Properties, Chuan Cai

LSU Master's Theses

We have investigated the enhanced Li-ion intercalation properties of two different materials, which are V2O5-WO3 composite and surface-coated LiCoO2. A simple and novel solution processing method is employed to prepare V2O5-WO3 composite films that demonstrate enhanced Li-ion intercalation properties for applications in Li-ion batteries or electrochromic displays. This solution processing method employs precursors that only contain the elements of V, W, O and H, which avoids impurity elements such as Na that has been commonly used in other solution methods (e.g. using precursors of sodium metavanadate and sodium tungstate solution). The V2O5-WO3 composite films show enhanced Li-ion intercalation properties compared …

Molecular Dynamics Simulation Studies Of Surface-Stress Effects In Metallic Nanostructures, Jijun Lao

LSU Doctoral Dissertations

Using molecular dynamics (MD) simulations we investigate the surface-stress-induced structural transformations and pseudoelastic behavior in palladium (Pd) crystalline nanowires. For a <100> initial crystal orientation our studies indicate that the surface stress can cause Pd nanowires to spontaneously undergo structural changes with characteristics that are determined by the wire cross-sectional area. Specifically, when the cross-sectional area is below 2.18nm x 2.18nm the wire changes spontaneously its crystal structure from the initial fcc structure to a body-centered-tetragonal (bct) structure. In wires of larger cross-sectional area (i.e., 2.57nm x 2.57nm) the structural transformation is achieved via a spontaneous lattice reorientation leading to an …

Fabrication And Property Study Of Plasma Sprayed Alumina Coatings And Magnetron Sputtered Multilayers, Ranran Liu

LSU Doctoral Dissertations

In this study, air or atmospheric plasma spraying (APS), one of thermal spraying processes, was used to produce alumina coatings and single splats. Nanoindentation technique was used to measure the mechanical properties, such as hardness and elastic modulus, of APS alumina coatings and single splats. The detailed procedures to calculate elastic modulus and hardness, and testing parameters for nanoindentation have been provided. This study revealed that the phase combination of α-Al2O3 and γ-Al2O3 played an important role in the scattering distribution of nanoindentation results on APS alumina coatings. In addition, nanoindentation technique was used to predict the phase information of …

Macroinstability And Perturbation In Turbulent Stirred Tank Flows, Somnath Roy

LSU Doctoral Dissertations

Impeller stirred tank reactors (STRs) are commonly used in the chemical processing industries for a variety of mixing and blending technologies. In this research, a numerical study of flow and mixing inside turbulently agitated STRs are carried out. An immersed boundary method (IBM) is utilized to represent moving impeller geometries in the background of multi-block structured curvilinear fluid. The IBM This curvilinear-IBM methodology is further combined with the large eddy simulation (LES) technique to address the issue of modeling unsteady turbulent flows in the STR. Verification of the combined IBM-LES implementation strategy in curvilinear coordinates is done through comparisons with …

Phase Investigation Of Zirconia Fibers And Their Applications On Solid Oxide Fuel Cells (Sofcs), Luping Li

LSU Master's Theses

Pure zirconia nanofibers were fabricated by electrospinning zirconia-polymer precursor and subsequent annealing. Fiber properties such as polymer decomposition, crystallization formation, phase transformation, surface morphologies, etc., were investigated by various techniques, including thermogravimetric analysis (TGA) and differential thermal analysis (DTA), high temperature differential scanning calorimeter (HTDSC), powder X-ray diffractometer (XRD), field emission scanning electron microscopy (FESEM), etc. It was found the crystallization of as-spun fibers started at 450 °C and the initial crystallized zirconia phase was tetragonal (t), which began transforming to monoclinic (m) phase at 650 °C as evidenced by XRD; HTDSC showed at different thermal circles, the m-to-t transformation …

Degradation Behavior Of Shape Memory Polymer Due To Water And Diesel Fuel, Mohammad Nazmul Hasan Nahid

LSU Master's Theses

Shape memory polymers (SMP) are smart materials, which have the ability to memorize the original or permanent shape. Owing to this characteristic SMP can be used as a sensor, a transplant, as well as structural materials in wide range of applications. Despite its importance, its degradation behavior is still not completely known; and only a limited amount of work has been reported in the literature. In this thesis, the experiments have been carried out to evaluate the degradation behavior of Veriflex- SMP (industry supplied SMP samples) upon exposure to two different types of liquids; water and diesel fuel separately. It …

Characterization Of Composite Piezoelectric Materials For Smart Joint Applications, Hari Prasad Konka

LSU Master's Theses

Piezoelectric materials have the ability to provide desired transformation from mechanical to electrical energy and vice versa. When a mechanical force is applied to the piezoelectric material an electrical voltage is generated and when an electrical voltage is applied to the piezoelectric material it gets strained or deformed. Owing to these characteristics piezoelectric materials can be used as a sensor, an actuator, as well as a power generation unit. The high brittleness property of the original piezoelectric material is one of the major constraints in using them in the engineering applications. In order to overcome this disadvantage the composite piezoelectric …

Design And Fabrication Of Micronozzles For Drug Delivery Applications, Yuxuan Zhou

LSU Master's Theses

Inhaled drug is an important drug delivery route. It is widely used in medications for respiratory disorders. However, it has some significant limitations, for examples, concentration of drug, output, and particles size, are not accurately controlled in most of the available drug delivery systems today. Various new devices and technologies continue to be developed and introduced. Vibrating orifice is one of them. The critical issue of vibrating orifice technology is the fabrication of micro-nozzles. Traditional technique to fabricate these nozzles is to use dry etching method, which tends to be expensive and inconvenient for mass production. Other two optional fabrication …

A Portable Phonatory Feedback Device For Patients With Speech Disorders, Richie Sajan

LSU Master's Theses

Vocal intensity-related speech disorders such as dysarthria and vocal nodules can limit quality of life and reduce the patient’s ability to interact with family, socialize, or pursue employment. Behavioral speech therapies exist to address these issues but have limited effectiveness because they are expensive and clinic-based. The ability to monitor vocal intensity outside of the clinical setting will greatly aid in the treatment of these speech disorders, enabling patients to make quicker progress by reinforcing techniques learned in the clinic. The Voice Volume Monitor (VVM) is a portable and cost-effective therapeutic aid designed for this purpose, providing real-time feedback regarding …

Computational Examination Of Compaction Wave-Boundary Interaction In Granular Explosive, Anirban Mandal

LSU Master's Theses

Interactions between initially planar, piston supported compaction waves in heterogeneous energetic solids and macro-scale rigid boundaries were computationally examined for a wide range of piston impact speeds (20 ≤ U_p ≤ 500 m/s) and initial solid volume fractions of the material (0.73 ≤ ϕ₀ ≤ 0.90). The response of the material was described by a continuum theory that accounts for both elastic and inelastic compaction in a thermodynamically consistent manner. Initial conditions were imposed by interpolating the spatial structure of one-dimensional steady compaction waves onto two-dimensional domains considered in this study. For a planar wedge boundary, the peak …

Enhancement Of Single-Lap Joint Strength Under Tension Using Piezoelectric Actuation, Ryan Michael Meyer

LSU Master's Theses

Composite adhesively bonded joint structures have seen increased use over conventional riveted due to their ease of manufacturing and quality strength-to-weight ratios. However, adhesively bonded joints lack the rigidity and failure strength of riveted assemblies, due to high stress concentrations which develop in the adhesive layer, which makes them prone to undesirable deformation and failure. Piezoelectric materials feature the ability to produce mechanical strain when subjected to an applied voltage and vice-versa. Therefore, it is proposed to use piezoelectric actuators to transmit counterbalancing forces to increase the rigidity and strength of composite joints. Existing studies have been limited in that …

Model-Based Nonlinear Control Of Active Tilting-Pad Bearings, An Wu

LSU Doctoral Dissertations

A promising mechanical bearing candidate for active operation is the tilting-pad bearing. The proposed active tilting-pad bearing has linear actuators that radially translate each pad. The use of feedback control in determining the actuator forces allows for the automatic, continuous adjustment of the pad position during the operation of the rotating machine. In the first part of the dissertation, we develop a nonlinear dynamic model of the active bearing system. The hydrodynamic force produced by the fluid film is modeled as a nonlinear, squeeze-film damper plus repellent spring. A model-based nonlinear controller is then designed to exponentially regulate the rotor …

Study Of Microstructure Effect On The Thermal Properties Of Yttria-Stabilized-Zirconia Thermal Barrier Coatings Made By Atmospheric Plasma Spray And Pressing Machine, Monica Bohorquez De Silva

LSU Doctoral Dissertations

Thermal barrier coatings (TBCs) are used in gas turbine engines to achieve a higher working temperature and thus lead to better efficiency. Yttria-Stabilized-Zirconia (YSZ), a material with low thermal conductivity, is commonly used as the top coat layer to provide the thermal barrier effect. In this dissertation the thermo-physical properties of a variety of TBCs samples made out of different fabrication techniques were investigated and compared. The first set of samples was fabricated using a pressing machine device to fabricate 0.5 inch diameter disk shaped YSZ-Al2O3 samples. The YSZ-Al2O3 powder mixture was made of 0, 1, 2, 3, 4 and …

Modeling And Simulation For Shape Memory Polymer Based Self-Healing Syntactic Foam, Wei Xu

LSU Doctoral Dissertations

Syntactic foams, renowned for their low density and high mechanical properties, are enjoying continuing growth in various civilian and military sectors. However, like laminated composites, foam cored structures are vulnerable to impact damages and suffering from inabilities in repairing macro-scale cracks. A self-healing mechanism for structural damage is genuinely desired. A recent development in self-healing structural damage is a two-step close then heal (CTH) scheme proposed by Li and Nettles [1] and elucidated by Li and Uppu [2], by mimicking the self-healing process of human skin. This concept has been further demonstrated in Nji and Li’s work [3] that a …

Elastohydrodynamic Analysis Of Spur Gears Using Load-Sharing Concept: Running-In And Steady-State, Saleh Akbarzadeh

LSU Doctoral Dissertations

Gears are widely used in industry and hence their performance is of vital importance. Under the typical operating conditions of gears, the lubricant layer formed between the teeth of the pinion and the gear cannot completely separate the surfaces and contact of asperities of the pinion and gear occurs. This case is usually referred to as mixed lubrication problem. In this research the load-sharing concept has been employed to predict the performance of the pinion-gear system. The load-sharing concept is an efficient method to solve the mixed lubrication problem and is capable to predict the thickness of the lubricant film, …

Fabrication, Characterization, Modeling And Testing Of A Nanostructured Bulk Thermoelectric Cooler, Dinesh Pinisetty

LSU Doctoral Dissertations

New generation micro/nano devices are emerging to monitor, control and act on living systems. Particularly, in the field of cryobiology, there is a need to monitor and control temperature at the cellular level. An important step towards achieving this aim is to fabricate a novel bulk nanostructured thermoelectric cooler (TEC). As a first step towards achieving efficient localized control of temperature in biological systems, Bismuth-telluride (Bi2Te3) and Antimony-Telluride (Sb2Te3) arrays of nanowires and nanotubes were fabricated, characterized and modeled. A thermal conductivity model originally developed by Dames and Chen for superlattice nanowires was extended to nanotubes. Based on this model …