Metallurgy Commons^™

Morphology And Roughness Of Al2o3 On Ferritic Stainless Steel Foil For Diesel Catalytic Converter Applications, Megan Butala

Materials Engineering

The improved thermal properties of metal-substrate catalytic converters enable effective catalysis sooner after ignition than traditional ceramic monoliths, resulting in less harmful emissions. ACAT Global, a manufacturer of stainless steel catalytic converters, uses ferritic stainless steel substrates for low temperature catalytic converters for diesel automobiles. Production begins with an oxidizing heat treatment to increase surface roughness. The success of the second production step, the application of catalyst-containing ceramic slurry (washcoat), depends on the surface roughness that results from oxidation. Formation of the primary oxide of interest, alumina (Al₂O₃), is controlled by the stainless steel foil composition, …

Discontinuous Grain Boundaries Of Forged René 41, Steven Crump

Materials Engineering

Forged components must pass a grain size specification (grain size, distribution) for acceptance in an application. The varying amounts of plastic deformation during forging can lead to abnormally large recrystallized grain sizes in certain regions of the part, which will not pass specification. The question exists whether these abnormally coarse grains are truly comprised of poly crystalline fine grains with grain boundaries resistant to etching techniques. To investigate this abnormal grain size effect, a cross section of a forged René 41 nickel-based superalloy aircraft engine ring was cut and sectioned into six segments. Those segments were then prepared for microstructural …

Analyzing The Corrosion Resistance Of Ni-Shield 200 Coatings At Different Temperatures When Exposed To Sulphuric Acid, Alex Hussinger

Materials Engineering

Six steel samples each were twin wire arc sprayed with Hastelloy C-276 or Nickel-Shield 200 coatings approximately 0.020″ thick. These samples were then cut into 3″ by 3″ squares. A 2″ diamond grit hole saw was used to abrade and polish to a smooth surface a ring in the middle in order to get an O-ring mechanical seal. The samples were then weighed and loaded into a jig that started from the bottom up with a stainless steel plate, then the sample, then a Viton O-ring, a ¾″ thick glass plate with a 1 3/4″ hole cut in it, another …

Process Optimization For Friction-Stir-Welded Martensitic Steel, M. Ghosh, K. Kumar, R. S. Mishra

Materials Science and Engineering Faculty Research & Creative Works

Advanced high-strength M190 steel sheets were joined by friction-stir welding under different tool rotational and traversing speeds. the optical microstructure of the joints exhibited complete martensite and partial martensite at the weld nugget depending on the cooling rate during welding. the first heat-affected zone outside of the weld nugget revealed ferrite-pearlite phase aggregate, and the second heat-affected zone showed a tempered martensitic structure. the interplay of process variables in terms of peak temperature and cooling rate was studied to observe their effect on joint efficiency under shear testing. the peak hardness at weld nugget was close to the parent alloy …

Characterization Of Positive Macrosegregation At The Subsurface Of Direct-Chill Cast 7050 Aluminum Forging Billets, Aaron Youril

Materials Engineering

Segregation of alloying elements during casting of forging billets may persist to the final forged component leading to unacceptable surface appearance. Determination of the elements or compounds that segregate is the essential first step to solving this problem. Differential Scanning Calorimetry (DSC) was used to determine a composition profile of the macrosegregation occurring at the subsurface of an as-cast 7050 aluminum alloy billet. Data collection was carried out by separating 10 to 20 mg samples from the outer centimeter along the radius of the billet, as well as samples from the bulk interior of the billet for comparison with the …

Effect Of Heating Temperature, Heating Time And Initial Microstructure On Recrystallization Of Waspaloy During Heating For Forging, Marissa Hill

Materials Engineering

A fine, uniform grain size is required for creep limited Waspaloy in aircraft engine applications. Upon heating, Waspaloy does not always recrystallize in a uniform manner resulting in occasional large grains with a majority of the grains meeting the grain size requirements. Waspaloy’s microstructure was analyzed with different heat treatments and in the as-forged condition. The strengthening mechanism is the gamma prime phase. The gamma prime solvus temperature is 1908°F so the different heat treatments were determined around that temperature, as well as the forging temperature range of 1800-2150°F. At the 1850°F heat treatment, the microstructure recrystallized with small grains, …

Material Flow And Microstructural Evolution During Friction Stir Spot Welding Of Az31 Magnesium Alloy, W. Yuan, Rajiv S. Mishra, B. Carlson, R. Verma, R. K. Mishra

Materials Science and Engineering Faculty Research & Creative Works

Material flow and local texture evolution during friction stir spot welding (FSSW) of AZ31 magnesium alloy was characterized by varying tool rotation rates. Texture at various locations of the welded region was measured using electron backscatter diffraction (EBSD). Material flow is significantly influenced by tool rotation rate with a conical step spiral pin tool, and FSSW introduces a unique basal fiber texture in the welded region. Results indicate that local texture evolution is dominated by shear deformation through material flow. the tool shoulder applies both shear and compressive deformation to the upper region material; however, the rotating pin introduces only …

Solar Cell Design Using Metamaterials, Yang Liu, Yitung Chen, Jichun Li

College of Engineering: Graduate Celebration Programs

Natural structure with simultaneous negative permittivity and permeability has not been discovered yet. However, using specially-designed metal embedded in dielectric bodies can achieve a kind of artificial negative index. This periodic structure which is smaller than the guided wavelength is known as a metamaterial. However, recent designs of metamaterials have some disadvantages when they are used in the application of solar cell. The perfect absorption is only within a narrow band, and for most of the solar spectrum, the absorption is no more than 10%. Here, a new kind of absorber for the solar spectrum has been designed and analyzed, …

Cellular Automaton For Simulation Of Oxide Layer Growth Influenced By Chromium Concentration Of Structure Material, Kuan-Che Lan, Yitung Chen, Ge-Ping Yu, Tzu-Chen Hung

College of Engineering: Graduate Celebration Programs

Chromium, an important alloying element, has been added in ferrous and nickel based alloy such as stainless steels and Inconel alloy to improve the corrosion resistance. High corrosion resistance of structural materials in extremely high working temperature is one crucial R&D objective of Gen IV nuclear power plants which propose to raise the thermal efficiency via high working temperature. A cellular automaton (CA) model based on the stochastic approach was proposed to simulate the process of oxidation and corrosion of structural material in flowing fluid. The relation of chromium concentration against oxide layer thickness during a specific period was found. …

Corrosion Rate Of Carbon Steel For Flowline And Pipeline As Transmission Pipe In Natural Gas Production With Co2 Content, Andi Rustandi, Muhammad Adyutatama, Enriko Fadly, Norman Subekti

Makara Journal of Technology

The purpose of this research is to investigate the corrosion rate of carbon steel as flowline and pipeline in natural gas production with CO2 content. The influence of variety of conditions that represent the actual conditions in practice such as CO2 partial pressure and solution composition, particularly NaCl percentage were performed. Research conducted by polarization test and simulation methods using PREDICTTM software. The result of this research is used to illustrate the level of corrosion rate of typical carbon steel i.e. API 5L X-52 occurred in natural gas pipelines due to the effect of dissolved CO2. From the experiments obtained …

Concurrent Engineering Of Tolerance Synthesis And Process Selection For Products With Multiple Quality Characteristcs Considering Process Capability, Mohamad Imron Mustajib

Makara Journal of Technology

The existences of variances that are very difficult to be removed from manufacturing processes provide significance of tolerance to the product quality characteristics target of customer functional requirement. Furthermore, quality loss incurred due to deviation of quality characteristics of the target with a specified tolerance. This article discusses the development of concurrent engineering optimization model of tolerance design and manufacturing process selection on product with multiple quality characteristics by minimizing total costs in the system, namely total manufacturing cost and quality loss cost as functions of tolerance, also rework and scrap costs. The considered multiple quality characteristics have interrelated tolerance …

Modification Of Flow Structure Over A Van Model By Suction Flow Control To Reduce Aerodynamics Drag, Harinaldi Harinaldi, Budiarso Budiarso, Warjito Warjito, Engkos Achmad Kosasih, Rustan Tarakka, Sabar Pangihutan Simanungkalit, I Gusti Made Fredy Lay Teryanto

Makara Journal of Technology

Automobile aerodynamic studies are typically undertaken to improve safety and increase fuel efficiency as well as to find new innovation in automobile technology to deal with the problem of energy crisis and global warming. Some car companies have the objective to develop control solutions that enable to reduce the aerodynamic drag of vehicle and significant modification progress is still possible by reducing the mass, rolling friction or aerodynamic drag. Some flow control method provides the possibility to modify the flow separation to reduce the development of the swirling structures around the vehicle. In this study, a family van is modeled …

Optimizing Fermentation Medium To Produce Cyclosporin A Using Response Surface Methodology, Rofiq Sunaryanto

Makara Journal of Technology

Response surface methodology (RSM) is a three factorial model which illustrates the relationship between one or more independent variables. RSM can be used to optimize the fermentation medium for the production of Cyclosporin A from the isolate Tolypocladium inflatum. The optimal point of the response surface area is predicted by using a seconddegree polynomial model and applying the statistic model obtained from the central composite design (CCD). The results of optimizing the fermentation medium for Cyclopsorin using the three independent variables of glucose, casein, and KH2PO4 show that all three of the independent variables affect the production of Cyclosporin A. …

Age, Gender, And Muscle Strength: A Study Based On Indonesian Samples, Henny Henny, Hardianto Iridiastadi, Iftikar Zahedi Sutalaksana

Makara Journal of Technology

Age and gender have been commonly used as a main criterion in accepting a job aplicant, but it is usually not clear how these affect job performance. While a number of recent studies have been done that describe the relationships between age, gender, and participants capacity (e.g., muscle strength), the results have been inconclusive. In Indonesia, in particular, such issues have been rarely investigated, and it is still important to study the issue since the relationships between these factors are population-specific. This study aimed at describing the relationships between age and muscle strength among workers for both genders. Ninety-six male …

Circularly Polarized Microstrip Array Antenna For Ground Segment In Quasi-Zenith Satellite System, Fitri Yuli Zulkifli, Eko Tjipto Rahardjo

Makara Journal of Technology

In satellite communication system, antenna plays an important role. Therefore, the antenna must meet some requirements, such as high gain, circular polarization, and good directivity. In this paper, a four element linear array triangular patch microstrip antenna with cross slot is designed to be used for Quasi-Zenith satellite system. A simulation study as well as experimental study was carried out. The simulation showed that the 3 dB axial ratio bandwidth of 87 MHz (2.569-2.656 GHz) is achieved while the measured results showed 96 MHz (2.556-2.652 GHz). The linear array of 4 element antenna has a gain of 13.73 dB and …

Tolerance Limit For Trucks With Excess Load In Transport Regulation In Indonesia, Sigit Pranowo Hadiwardoyo, Raden Jachrizal Sumabrata, Mohammed Ali Berawi

Makara Journal of Technology

Reliability of a road is mandatory since damaged will impede the traffic. Destruction is caused by various factors; one of the most important factors is excess load. Overload may give the load of each axle of a vehicle exceeds the determined standard. This condition occurs in trucks exceeding the load limit. In designing the structure of a road based on the method of Directorate General of Highways Ministry of Public Works of the Republic of Indonesia, axle load calculated in equivalent-number, or known as equivalent axle load (EAL), of 8.16 tons of standard axle. Total equivalent-number over the service life …

Earthquake Damage Intensity Relationship For Residential Houses In West Sumatra, Febrin Anas Ismail, Abdul Hakam, Fauzan Fauzan

Makara Journal of Technology

The Sumatra 30 September 2009 earthquake has damaged hundred thousand buildings in West Sumatra Province. The earthquake is located in 100 km offshore of Padang City, the Capital City of the province. Survey has been conducted to assess the damage of the building in few days after the earthquake. In this survey, the damage of buildings are categorised into 3 level that are heavily, moderate and slightly damages. This paper explores the level damage of building and then the intensity of the shaking in the affected area. Then based on the coordinate of every building location, the buildings are scattered …

Evaluation Of Universitas Indonesia’S Recharge Pond Performance And Potential Utilization For Raw Water Source, Nyoman Suwartha, Resky Agaslian Pramadin

Makara Journal of Technology

Evaluasi Kinerja Waduk Resapan UI dan Potensi Pemanfaatannya sebagai Sumber Air Baku. Waduk resapan Universitas Indonesia (UI) telah dibangun sejak 5 tahun yang lalu. Namun kegiatan monitoring dan evaluasinya sangat minim dilakukan. Tujuan dari studi ini adalah untuk mengetahui laju resapan, dan untuk mengevaluasi kondisi kuantitas dan kualitas air waduk resapan selama musim kemarau dan penghujan. Pengukuran kedalaman muka air, intensitas curah hujan dan penguapan dilakukan untuk menentukan ketersediaan air, laju resapan, dan imbangan air waduk. Sejumlah air permukaan diambil dari waduk resapan dan sungai di tiga titik sampling untuk mengetahui kondisi kualitas air eksisting. Hasil studi menunjukkan tidak ada …

Effect Of Methanol Induction And Incubation Time On Expression Of Human Erythropoietin In Methylotropic Yeast Pichia Pastoris, Adi Santoso, Neng Herawati, Yana Rubiana

Makara Journal of Technology

Erythropoietin (EPO) is a glycoprotein hormone consists of 165 amino acids and has molecular mass of 30,400 Daltons. The large quantities of these hormone required to satisfy clinical demand are currently met by recombinant expression in mammalian cell, namely chinese hamster ovary (CHO). Pichia pastoris has become popular yeast based protein production systems to substitute mammalian expression systems. P. pastoris is capable to use methanol as sole carbon and energy source. In this study, recombinant human EPO (rhEPO) protein obtained by expressing the hEPO gene in methylotropic yeast P. pastoris, strain X33. The present work was carried out to study …

Fuel Saving Strategy In Spark Ignition Engine Using Fuzzy Logic Engine Torque Control, Aris Triwiyatno, Sumardi Sumardi

Makara Journal of Technology

In the case of injection gasoline engine, or better known as spark ignition engines, an effort to improve engine performance as well as to reduce fuel consumption is a fairly complex problem. Generally, engine performance improvement efforts will lead to increase in fuel consumption. However, this problem can be solved by implementing engine torque control based on intelligent regulation such as the fuzzy logic inference system. In this study, fuzzy logic engine torque regulation is used to control the throttle position entered by the driver to achieve optimal engine torque. An engine torque vs. throttle position and engine speed mapping …

An Agri-Food Supply Chain Model To Enhance The Business Skills Of Small-Scale Farmers Using Corporate Social Responsibility, Wahyudi Sutopo, Muh. Hisjam, Yuniaristanto Yuniaristanto

Makara Journal of Technology

In general, small-scale vegetable farmers experience problems in improving the safety and quality of vegetables for supplying high-class consumers in modern retailers. Farmer Group and/or Cooperative (FGC) should be able to assist its members to meet the relevant provisions of modern retail on product specifications, delivery terms, and internal business requirements. This study proposed an agri-food supply chain (ASC) model that involves the corporate social responsibility (CSR) activities to enhance the business skills of the FGC as supplier of modern retailer. Multi-objective optimization programming is developed to determine the amount and timing of supply, level of farmers training skills, quality …

Pineapple Liquid Waste As Nata De Pina Raw Material, Agus Sutanto

Makara Journal of Technology

This research aims to study the quantity, quality, ecological and economic feasibility of nata de pina production (NP) from pineapple liquid waste (PLW). The design of the study employs complete random design (CRD) with three treatments: PLW without nutrients addition (A), PLW nutrients addition (B), and PLW stored for six months with nutrients addition (C). The nata de pina’s production factors measured were weight, thickness, fiber content, color, brightness, and residual waste. The highest weight was reached in treatment B (899 grams), followed by treatment A (616.4 grams), and C (477.8 grams). The thickness of NP of the height and …

Modeling Of A New Structure Of Precision Air Conditioning System Using Secondary Condenser For Rh Regulation, Aries Subiantoro, Nasruddin Nasruddin, Feri Yusivar, Muhammad Idrus Al-Hamid, Bagio Budiardjo

Makara Journal of Technology

A dynamic mathematical model for a new structure of precision air conditioning (PAC) has been developed. The proposed PAC uses an additional secondary condenser for relative humidity regulation compared to a basic refrigeration system. The work mechanism for this system and a vapour-compression cycle process of the system are illustrated using psychrometric chart and pressure-enthalpy diagram. A non-linear system model is derived based on the conservation of mass and energy balance principles and then linearized at steady state operating point for developing a 8th-order state space model suited for multivariable controller design. The quality of linearized model is analyzed in …

Microstructure Selection Of Sm–Co–Al Alloys To Increase Magnetization, Brian Dick

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

An ever increasing demand for higher performing magnets drives the need for new and innovative methods to achieve this goal. Sm-Co rare earth permanent magnets have a unique eutectic microstructure that, through refinement, could become a two-phase magnet which would significantly increase their energy product. The eutectic structure of Sm₈Co₉₂ is comprised of αCo rods embedded within a Sm₂Co₁₇ matrix. If the rods are small enough to encourage exchange coupling and the matrix is smaller than the single domain limit, then an efficient two-phase magnet is created.

Refining the Co rods and matrix size …

Hot Deformation Behavior Of Friction-Stir Processed Strip-Cast 5083 Aluminum Alloys With Different Mn Contents, M. A. García-Bernal, Rajiv S. Mishra, R. Verma, D. Hernández-Silva

Materials Science and Engineering Faculty Research & Creative Works

Fine grained 5083 aluminum alloy is the most common Al-Mg alloy for superplastic forming (SPF) of lightweight sheet metal parts in the automotive and aerospace industries. the fine-grained sheet is industrially produced by massive cold rolling of conventionally rolled sheet stock at high cost. Friction stir processing (FSP) as a thermomechanical process is very effective in refining the microstructure of as-cast alloys such as that produced by continuous strip casting (CC). in this work, the effect of friction stirs processing on the superplastic properties of three CC 5083 aluminum alloys, with different Mn content, has been investigated. the three alloys …

Time-Dependent Fatigue Crack Propagation Behavior Of Two Solid-Solution-Strengthened Ni-Based Superalloys—Inconel 617 And Haynes 230, Longzhou Ma, Shawoon K. Roy, Muhammad H. Hasan, Joydeep Pal, Sudin Chatterjee

Environmental Studies Faculty Publications

The fatigue crack propagation (FCP) as well as the sustained loading crack growth (SLCG) behavior of two solid-solution-strengthened Ni-based superalloys, INCONEL 617 (Special Metals Corporation Family of Companies) and HAYNES 230 (Haynes International, Inc., Kokomo, IN), were studied at increased temperatures in laboratory air under a constant stress-intensity- factor (K) condition. The crack propagation tests were conducted using a baseline cyclic triangular waveform with a frequency of 1 3 Hz. Various hold times were imposed at the maximum load of a fatigue cycle to study the hold time effect. The results show that a linear elastic fracture mechanics (LEFM) parameter, …

A Front Tracking Model Of The Maxus-8 Microgravity Solidification Experiment On A Ti-45.5at.% Al-8at.%Nb Alloy, Robin Mooney, Shaun Mcfadden, Marek Rebow, David J. Browne

Articles

On 26th March 2010 the MAXUS-8 sounding rocket was launched from the Esrange Space Center in Sweden. As part of the Intermetallic Materials Processing in Relation to Earth and Space Solidification (IMPRESS) project, a solidification experiment was conducted on a Ti-45.5at.%Al-8at.%Nb intermetallic alloy in a module on this rocket. The experiment was designed to investigate columnar and equiaxed microstructures in the alloy. A furnace model of the MAXUS 8 experiment with a Front Tracking Model of solidification has been developed to determine the macrostructure and thermal history of the samples in the experiment. This paper gives details of results of …

Plastic Strain Accommodation And Acoustic Emission During Melting Of Embedded Indium Particles In Aluminum, Michael M. Kuba

Masters Theses

"Melting of micron-sized (0.2 to 3 µm diameter) indium particles embedded in an aluminum matrix was discovered to produce acoustic emission. Melting of embedded immiscible particles produces a pure dilation during the phase transformation and has no long-range diffusion field to control the speed of transformation. It was found that acoustic emission can no longer be considered as a criterion of displacive transformations and that melting of micron-sized embedded particles is strain energy controlled. Acoustic emission was confirmed to result from the rapid relaxation of aluminum around indium particles embedded on grain boundaries. Prismatic punching of dislocation loops is proposed …

Directional Anisotropy In The Mechanical Behavior Of Friction Stir Processed And Aged Az91 Alloy, Vipin Jain, Wei Yuan, R. S. Mishra, Gouthama, Anil K. Gupta

Materials Science and Engineering Faculty Research & Creative Works

Friction stir processing (FSP) is an emerging grain refinement technique for magnesium alloys. in this study, a cast AZ91 alloy was processed by a single-pass FSP to achieve an average grain size of ∼6 μm in the nugget zone. the FSP is found to introduce texture in the alloy due to preferred alignment of basal poles in the processing direction. the mechanical behavior is significantly influenced by texture. after FSP, the alloy was aged at different temperatures and times for continuous and discontinuous precipitation of β-Mg17Al12. a high anisotropy in yield stress is observed in the processing and transverse direction …

Development Of Third Generation Advanced High Strength Steels, Meghan C. Mcgrath

Doctoral Dissertations

"Lightweight duplex steels with combinations of either bainite, acicular ferrite, and austenite or martensite and austenite were investigated as third generation advanced high strength steels targeted for automotive applications. Large additions of manganese (>13 wt%) and carbon (

Duplex steels with different volume fractions of primary δ -ferrite were used to study the crystallography of austenite formed during the peritectic reaction. Solute profiles across the peritectic interface showed aluminum segregated near the interface which promoted bainitic ferrite formation. Thermal treatments were used to manipulate the concentration and type of oxides and the ferrite plate density was found to correlate …