Metallurgy Commons^™

Humidity And Temperature Boundaries For Biofilm Formation In Yucca Mountain, Terry Ann Else, Penny S. Amy, James Jay, Amy J. Smiecinski

Publications (YM)

To determine the long-term success of the recommended Yucca Mountain high-level nuclear waste repository, studies of bacterial colonization and biofilm development are needed. Bacteria involved in microbially-influenced corrosion and degradation are known to form biofilms with the potential to impact the integrity of repository packaging and structural materials. Temperature and humidity are environmental factors that can greatly affect biofilm formation. Therefore, it is necessary to determine the temperature and humidity conditions that affect biofilm formation. Microcosms, which simulated the repository environment of Yucca Mountain, were placed at temperatures ranging from 30° C to 70° C and in relative humidities ranging …

Evaluation Of Lead Anode Reactions In Acid Sulfate Electrolytes: Ii. Manganese Reactions, Pu Yu, Thomas J. O'Keefe

Materials Science and Engineering Faculty Research & Creative Works

Lead alloys containing calcium-tin, silver, or similar combinations are the primary insoluble anodes used for copper and zinc electrowinning. One potential concern with these anodes is the detrimental effect on cathode purity from incorporation of lead corrosion products. Other factors which are important to process economics are the reaction potential and overpotential required for oxygen evolution. In addition to the inherent overpotential, impurities in the electrolyte can have a significant polarization impact, such as the films that may form when manganese is present. In order to gain a better understanding of the fundamental behavior of various concentrations of manganese ions …

Design And Analysis Of A Process For Melt Casting Metallic Fuel Pins Incorporating Volatile Actinides, Yitung Chen, Darrell Pepper, Randy Clarksean

Fuels Campaign (TRP)

UNLV has developed and will continue to develop process models for the analysis of melt casting processes. This work will continue to be performed under the guidance of Argonne National Laboratory (ANL) engineers to ensure that their knowledge and experience benefits the project. The research to be conducted during the second year will center on performing detailed analyses on a conceptual design of an inductively heated skull-crucible casting furnace. Processing conditions will be analyzed, basic models utilized, and detailed heat and mass transfer models will be developed to analyze the most promising processes. The goal of this second year is …

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Ii, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces led to the use of a buffered chemical polishing procedure for surface cleaning to get good performance of the cavities. This proposal discusses the second phase of research in the second year of the project.

The first phase (starting Summer 2001) has resulted in improving the basic understanding of multipacting and the process of chemical etching. Based …

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada, Las Vegas (UNLV) and Idaho State University (ISU) is to evaluate the feasibility of determining residual stresses of welded (after pre-straining) engineering materials using a new nondestructive technique based on positron annihilation spectroscopy. The proposed technique is to use γ-rays 2 from a small MeV electron Linac to generate positrons inside the sample via pair production. This method can be used for materials characterization and investigation of defects in thick samples that could not be accomplished by conventional positron techniques or other nondestructive methods. The data generated will …

The Effect Of Temperature On The Optical Absorptive And Reflective Behavior Of Metals, Thomas A. Hunyady

Mechanical & Aerospace Engineering Theses & Dissertations

In the five decades since its invention, the laser has been used to commercially process materials in an increasingly diverse number of ways. The precise control over the delivery of the incident energy that is afforded by a laser allows for a wide variety of applications. All of these processes depend in some way on two important physical properties of the material being treated. These properties are known as the optical reflectivity and absorptivity of a material. The values of each of these properties are different for each material and are influenced by a number of factors, including surface roughness, …

Integrating Passenger And Modulo As Learning Tools For Collaborative Engineering Education, Kalamullah Ramli, Frank Schwarz, Stefan Werner, A Halim Shamsuddin, Axel Hunger

Makara Journal of Technology

The University of Indonesia (UI), Gerhard Mercator University (GMU), the Universiti Kebangsaan Malaysia (UKM) have agreed to cooperate as partners to develop a joint bachelor (3+1) and masters (1+1) degree, and collaborate in the research fi elds of multimedia- and internet-based learning and application level active networks. This paper describes the introduction of the Offshore Project and the extending of information technology applications to the partner institutions in this international cooperation which would very much enhance the operations of the new initiative in engineering education, which could provide students in far distance with more fl exible learning environment.

Study Effect Of Salt Washing Process On Content And Iodium Stability Of Salt, Nelson Saksono

Makara Journal of Technology

Effect of Salt Washing Process on Content and Iodium Stability of Salt. Salt washing process should increase the salt quality. It should clean the salt from sludge or clay and also reduce the impurity compound such as Mg, Ca and the reductor content. The objective of these reseach is to assess the effect of washing process on the content og hygroscopic impurities compound (Ca and Mg), and reductor content of salt. The research also investigate the water absorbing, pH, KIO3 content as function of time to obtain effect of washing process on KIO3 stability in salt. The experiment result shows …

Object Classfification In Computer Vision With Discriminant Analysis, Amir Hamzahan

Makara Journal of Technology

A robotic sensor system is always supported by a computer system called ‘computer vision’. The important concept of computer vision is object classfifi cation. In this study two algorithms for object classifi cation in this system will be compared. Firstly, A simple method that do not need complex computation and that considered as an informal method is called binary tree decision structure. This method is based on modest caracteristic decriptors of an object such as vertical line, horizontal line or ellipse line. Unfortunately this method has weakness in recognize an image that contaminated by a noise. Secondly, a more formal …

Making Alloys (Ti1 - Xalx) N Using Plasma Cvd Technique From Alcl3 Powder, H2 And N2 Gas ,With Solvent Ticl4, Keba Moto

Makara Journal of Technology

The substitution of Ti atoms by Al atoms in TiN lattice sites to form (Ti1-xAlx)N is clearly demonstrated by the coatings which were deposited on steel substrate and using plasma CVD technique. The presence of Al atoms in TiN lattice site is shown by means of XRD and EDX techniques: lattice parameters decreasing of TiN as the fraction of Al increases (XRD) and precipitation of hexagonal AlN phase (XRD) as the fraction of Al exceeding 0.8 (EDX). The hardness of these coating are just around 30 GPa, which is beyond the values reported in literatures.

Effects Of 0.25 % Mo (Molybdenum) Which Is Contained In The Ductile Cast Iron On Mechanical Properties Of Austempered Ductile Iron (Adi)., Nukman Nukman, Bustanul Arifin, Bambang Sugiarto

Makara Journal of Technology

The aim of this research is to investigate the effects of 0.25 % Mo (Molybdenum) which is contained in the ductile cast iron on mechanical properties of Austempered Ductile Iron (ADI). The various temperatures and the holding times are used in the heat treatment processes. Using a given 0.25 % Mo in the ductile iron, ADI's alloyed developes a higher ultimate tensile stress value and decreases the elongation if we compare with the as cast (non alloy ductile iron). The higher impact energy value obtained at 9000 C austenization and 375o C austempering temperatures during 60 minutes holding times. The …

The Manufacturing Properties Of Galvanised Steel Sheet With Hexagonal And Tetragonal Network Of Circle Holes, Rahmat Saptono

Makara Journal of Technology

Galvanized steel sheet of 0.8 mm in thickness was drilled with circle holes of 2.5 mm diameter and spacing arranged in tetragonal and hexagonal pattern. The manufacturing properties of specimen were studied through drawing and stretching simulative test. It was concluded from the results that, at high ratio of punch to hole diameter (40/2.5), the drawing properties (LDR) of both square and hexagonal perforated sheet were slightly lower than that of solid sheet, while hexagonal perforated showing LDR somewhat higher than the square one. The stretching properties (LDH) of sheet, however, were much lower than that of solid sheet while …

Develops The Software Of Dsp Processor For The Cdma Circuitry, Arman Djohan D.

Makara Journal of Technology

This research develops the software of DSP Processor type TMS320C54X for the CDMA circuitry. This research apply two algorithms namely Mathematic Algorithm and table lookup Algorithm. From both algorithms, the research examine what algorithm have the fasted processing time and the smallest memory occupation. From the examination results the Mathematic Algorithm have 20.62 milliseconds processing time and the Table lookup algorithm have 14.08 milliseconds processing time. The Table lookup algorithm have the fastest processing time because the Matematic algorithm need the rounding process of the fi gure. Eventhough such processing time is not exceed from the 125 millisecond of delay …

Environment-Induced Degradation And Crack-Growth Studies Of Candidate Target Materials: Aaa Task-4 Quarterly (December 1, 2001 – February 28, 2002) Report, Ajit K. Roy, Brendan O'Toole

Transmutation Sciences Materials (TRP)

The primary objective of this task is to evaluate the effect of hydrogen on environment-assisted cracking of candidate materials for applications in spallation-neutron-target (SNT) systems such as accelerator production of tritium (APT) and accelerator transmutation of waste (ATW). The materials selected for evaluation and characterization are martensitic stainless steels including HT- 9, EP 823 and 422. The susceptibility to stress corrosion cracking (SCC) and hydrogen embrittlement (HE) of these alloys will be evaluated in environments of interest using tensile specimens under constant load and slow-strain-rate (SSR) conditions. The extent and morphology of cracking of these alloys will further be evaluated …

Development Of A Mechanistic Understanding Of High-Temperature Deformation Of Alloy Ep-823: Aaa Task-10 Quarterly (12/1, 2001 –02/28, 2002) Report, Ajit K. Roy, Brendan O'Toole

Transmutation Sciences Materials (TRP)

The objective of this task is to evaluate the elevated temperature tensile properties of Alloy EP-823, a leading target material for accelerator-driven waste transmutation applications. The test material will be thermally treated prior to evaluation of its tensile properties at temperatures relevant to the transmutation applications. The deformation characteristics of tensile specimens, upon completion of testing, will be evaluated by surface analytical techniques including scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The overall results are expected to provide a mechanistic understanding of high-temperature deformation behavior of Alloy EP-823 as a function of heat treatment.

Highlights of Accomplishment

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Fretting Fatigue Behavior Of A Titanium Alloy Ti-6al-4v At Elevated Temperature, Onder Sahan

Theses and Dissertations

The purpose of this research is to investigate the fretting fatigue behavior of the titanium alloy Ti-6Al-4V at elevated temperature is investigated. Fretting and plain fatigue experiments are conducted at 260 °C. Crack initiation location and crack initiation orientation is measured and fretting and plain fatigue life data of the specimens from these tests are obtained. Fatigue parameters capable of predicting the number of cycles to specimen failure, the crack location and the crack orientation along the contact surface are analyzed. The parameters are calculated by using the computed stresses and strains obtained from the finite element analysis. The mechanisms …

Third Quarter Report, Covering January Through March 2002, John Farley

Transmutation Sciences Materials (TRP)

Progress from June 2001-November 2001 was presented at the winter meeting of the American Nuclear Society in Reno (November 12-15, 2001), and incorporated into a refereed conference proceeding. A copy of the refereed conference proceeding has been provided to Tony Hechanova. In brief, the paper described the new program to examine the corrosive effects of lead-bismuth eutectic (LBE) on steels. We employed various types of surface studies (Scanning Electron Microscope [SEM], and X-ray Photoelectron Spectrometry [XPS]) to examine steel samples that had been exposed to LBE for various lengths of time at various temperatures. The goal is to understand the …

Modeling, Fabrication, And Optimization Of Niobium Cavities – Phase I: Quarterly Progress Report November 20, 2001 - February 20, 2002, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Multipacting is one of the major loss mechanisms in RF superconductivity cavities for accelerators. This loss mechanism limits the maximum amount of energy/power supported by the cavities. Optimal designs have been identified in others’ studies. In practice, these designs are not easily manufactured. Chemical etching processes used to polish the cavity walls result in a nonuniform surface etch. A nonuniform surface etch will leave some unclean areas with contaminants and micron size particles. These significantly affect multipacting. Further, a nonuniform etch will leave areas with damaged grain structure, which is not good for superconducting properties. Typically, the depth of chemical …

Modeling Corrosion In Oxygen Controlled Lbe Systems With Coupling Of Chemical Kinetics And Hydrodynamics: Quarterly Progress Report 11/16/01- 2/15/02, Samir Moujaes, Yitung Chen

Transmutation Sciences Materials (TRP)

The Lead-Bismuth eutectic (LBE) has been determined from previous experimental studies by the Russians and the European scientific community to be a potential material that can be used as a spallation target and coolant for the AAA proposed application.

Properly controlling the oxygen content in LBE can drastically reduce the LBE corrosion to structural steels. However, existing knowledge of material corrosion performance was obtained from point-wise testing with very limited density. The transport of oxygen and corrosion products, their interaction and variation of corrosion/precipitation along the flow are not well understood.

The first subtask of this project involves using a …

Design And Analysis For Melt Casting Metallic Fuel Pins Incorporating Volatile Actinides: Quarterly Progress Report 11/16/01- 2/15/02, Yitung Chen, Randy Clarksean, Darrell Pepper

Fuels Campaign (TRP)

An important aspect of the Advanced Accelerator Applications (AAA) program is the development of a casting process by which volatile actinide element (i.e., americium) can be incorporated into metallic alloy fuel pins. The traditional metal fuel casting process uses an inductively heated crucible.

This process works well for the fabrication of metal fuel pins traditionally composed of alloys of uranium and plutonium, but does not work well when highly volatile actinides are included in the melt. The problem occurs both during the extended time period required to superheat the alloy melt as well as when the chamber must be evacuated. …

Hydrogen-Induced Embrittlement Of Candidate Target Materials For Applications In Spallation-Neutron-Target Systems, Ajit K. Roy, Brendan O'Toole

Transmutation Sciences Materials (TRP)

The purpose of this project is to evaluate the effect of hydrogen on cracking of candidate target materials for applications in spallation-neutron-target (SNT) systems such as accelerator production of tritium (APT) and accelerator transmutation of waste (ATW). The test materials will undergo appropriate thermal treatments prior to being hydrogen-charged by potentiostatic cathodic polarization technique in a simulated aqueous environment at different temperatures of interest. The specimens, upon completion of testing, will be metallographically examined. Further, the scanning electron microscopy (SEM) will be used to determine the extent and nature of cracking in the specimens tested. The thrust of the proposed …

Effect Of Cr3+ And So42- On The Structure Of Rust Layer Formed On Steels By Atmospheric Corrosion, Masato Yamashita, Hitoshi Uchida,, Desmond C. Cook .

Physics Faculty Publications

The effect of chromium ion (Cr³⁺) and sulfate ion (SO₄^2-) on the structure of the rust layer formed by thin electrolyte-film corrosion of low-alloy steels has been examined. By using X-ray diffraction spectroscopy, it was found that coexistence of Cr³⁺ and SO₄^2- in the electrolyte film covering the steel surface quickly forms the Cr-goethite (α-(Fe _1-X, Cr_X)OOH) layer which has been known as the final protective rust layer. Scanning vibrating electrode measurements showed that the rust layer formed under the electrolyte film containing Cr³⁺ and SO₄^{2- …}

Misinformation [1], Hollis P. Leighly

Materials Science and Engineering Faculty Research & Creative Works

No abstract provided.

Evaluating And Monitoring Nucleation And Growth In Copper Foil, Ye Kun Lee, Thomas J. O'Keefe

Materials Science and Engineering Faculty Research & Creative Works

The electrodeposition of copper foil for use in electronic materials applications is a complex and demanding process. The specific aspects of producing and controlling the structure-property-performance requirements of the foil are important because of the stringent demands placed on their use in printed circuit boards and similar products. In this paper, a brief review of the electrodeposition process for raw copper foil is presented. Since electrolyte additives play such a significant role in the copper-deposition process, the effects of two essential additives, chloride ion and an organic (e.g., glue or gelatine), on the foil are described. Also, the influence of …

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Ii Second Quarterly Report, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces lead to the use of a buffered chemical polishing produce for surface cleaning to get good performance of the cavities. Up to this point, the second phase has resulted in the design of an experimental setup for the fluid flow experiment. Other experimental activities include the evaluation of a vacuum system are underway. Little reportable progress has …

Modeling, Fabrication, And Optimization Of Niobium Cavities, Robert A. Schill Jr., Mohamed Trabia, Yitung Chen

Transmutation Sciences Materials (TRP)

All technologies for the transmutation of nuclear waste require a large source of neutrons. One of the principal methods of generating these neutrons is by using a particle accelerator to bombard a heavy metal target. One of the more promising designs for particle accelerators for transmutation systems is the Superconducting Radio Frequency (RF) high-current linear accelerator (linac). The power supplies for these systems have three major components: niobium cavities, power couplers, and cryomodules. This research project will develop models to predict the behavior and performance of the niobium cavities, which will then be used to design and optimize the superconducting …

Experimental Investigation Of Steel Corrosion In Lead Bismuth Eutectic (Lbe): Characterization, Species Identification, And Chemical Reactions, John Farley, Dale L. Perry, Allen L. Johnson

Transmutation Sciences Materials (TRP)

The goal of the present research is to achieve a basic understanding of corrosion of steels by Lead Bismuth Eutectic (LBE). Liquid LBE is under consideration in the transmuter as both a spallation target and as a blanket coolant. There have been previous studies of LBE, especially by the Russians, who have over 80 reactor-years experience with LBE coolant in their Alpha-class submarine reactors. However, a fundamental understanding and verification of its role in the corrosion of steels is still very incomplete. We have begun a program of post-experiment testing and analysis on steel samples that have been in intimate …

Corrosion Of Steel By Lead Bismuth Eutectic, John Farley, Dale L. Perry, Allen L. Johnson

Transmutation Sciences Materials (TRP)

This research program will analyze various steel samples that have been exposed to LBE as part of the national program to develop LBE and transmutation technologies. This information will be paramount in developing engineering efforts to control, avoid, and/or minimize the effect of corrosion of steels by LBE in transmuter and LBE systems. Additionally, this program provides UNLV researchers with hands-on experience that will be crucial in developing the UNLV LBE program, supporting the University’s mission with the ISTC target complex, and the future development of additional facilities to examine LBE systems.

The research group plans to test the hypothesis …

Corrosion Of Steel By Lead Bismuth Eutectic: Year 1 Annual Report, John Farley

Transmutation Sciences Materials (TRP)

The goal is to investigate the corrosion of stainless steel by lead-bismuth eutectic (LBE), which has been proposed for use as a blanket coolant and a spallation target in the transmuter.

Hydrogen-Induced Embrittlement Of Candidate Target Materials For Applications In Spallation-Neutron-Target Systems, Ajit K. Roy, Brendan O'Toole, Zhiyong Wang, David W. Hatchett

Transmutation Sciences Materials (TRP)

Spallation-neutron-sources, such as those under investigation for use in accelerator-driven transmutation systems, generate neutrons through the collision of high-energy protons, or charged hydrogen atoms, with heavy metal targets such as lead. As a result, these systems also tend to deposit a significant amount of hydrogen in the materials of the transmuter target and superstructure. This can result in accelerated corrosion and changes in the properties of the exposed materials. Of particular importance is a phenomenon called hydrogen embrittlement, in which materials lose their ductility (ability to deform under stress) and become brittle (more susceptible to fracture) after reacting with hydrogen. …