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Metallurgy Commons

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University of Tennessee, Knoxville

Theses/Dissertations

Microstructure

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Full-Text Articles in Metallurgy

Microstructure Control And Correlation To Creep Properties In Grade 91 Steel Weldment After Thermo-Mechanical Treatments And An Fe-30cr-3al Alloy Strengthened By Fe2nb Laves Phase, Benjamin Allen Shassere Dec 2016

Microstructure Control And Correlation To Creep Properties In Grade 91 Steel Weldment After Thermo-Mechanical Treatments And An Fe-30cr-3al Alloy Strengthened By Fe2nb Laves Phase, Benjamin Allen Shassere

Doctoral Dissertations

Type IV cracking in weldments of steel pipes after creep deformation is a concern in modern fossil-fueled power plants. Two possible methods for minimizing or eliminating Type IV cracking will be discussed. The first method alters the initial microstructure of typical Grade 91 steel base metal before welding, while the second provides baseline microstructure characteristics and creep performance of a new alloy that is strengthened by the intermetallic Fe2Nb Laves phase. The initial microstructure of the Grade 91 steel can be controlled by Thermo-Mechanical Treatments, which aids in precipitation of fine (5-10 nm) MX particles in austenite before transformation to …


Evaluation Of The Potential For Weld-Related Cracking In Cast 20cr-32ni-1nb Heat-Resistant Stainless Steel, John William Bohling Aug 2016

Evaluation Of The Potential For Weld-Related Cracking In Cast 20cr-32ni-1nb Heat-Resistant Stainless Steel, John William Bohling

Masters Theses

Steam reforming of hydrocarbons is an important process for the production of hydrogen for industrial needs, such as ammonia synthesis. Due to the high temperature conditions (700 °C–900 °C), reformer furnace components require materials with excellent creep properties and thus highly alloyed austenitic stainless steels are typically employed. For reformer outlet manifolds, a cast, heat-resistant stainless steel with the composition 20Cr-32Ni-1Nb (ASTM A351 Grade CT15C) is widely used. However, after service exposure this alloy exhibits problems with liquation cracking in the base metal heat-affected zone (HAZ) during repair welding. In the work presented herein, two heats of material from centrifugally-cast …


Fatigue, Fracture, And Environmentally-Assisted Behavior Of Advanced Engineering Materials, Zhi Tang Dec 2014

Fatigue, Fracture, And Environmentally-Assisted Behavior Of Advanced Engineering Materials, Zhi Tang

Doctoral Dissertations

The objective of the present study is to provide a fundamental understanding of fatigue, fracture, and environmentally-assisted behavior of high-entropy alloys (HEAs). The work involves fatigue, fracture, and environmentally-assisted behavior of a new kind of advanced engineering materials, called HEAs. Three tasks are studied: (1) microstructures and fracture mechanisms of HEAs, (2) fatigue failure and life prediction of HEAs, and (3) corrosion and environmentally-assisted behavior of HEAs.

In the first task, microstructural stability and fracture mechanism of the AlCoCrFeNi alloy are studied and compared with thermodynamic calculations. In the second task, high-cycle fatigue-failure mechanisms of the cold-rolled Al0.5CoCrCuFeNi alloy are …


Deformation Study Of Nanocrystalline Ni-Fe Alloy Using Synchrotron Diffraction, Li Li Aug 2010

Deformation Study Of Nanocrystalline Ni-Fe Alloy Using Synchrotron Diffraction, Li Li

Doctoral Dissertations

This dissertation addresses two critical issues in the deformation of nc metals and alloys: (1) A stress-induced genuine grain growth after the plastic deformation rather than just a change of the grain shape; (2) A systematically quantitative study of micrsostructural evolution during the plastic deformation.

These two critical issues point to the deformation of nc materials with the average-grain sizes within the range of 10 to 50 nm, which is the most interesting and controversial region in the current time. The current study provides a systematic and detailed microstructural evolution for this region, which is definitely beneficial for the investigation …