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Articles 31 - 60 of 111
Full-Text Articles in Metallurgy
Investment Cast C450 Microstructural Characterization In Golf Club Heads, Kenneth Yin-Fai Lau
Investment Cast C450 Microstructural Characterization In Golf Club Heads, Kenneth Yin-Fai Lau
Materials Engineering
Two types of tensile bars were observed in this study of golf iron heads for TaylorMade Golf. As-cast and as-cast then machined tensile bars. The tensile bars underwent tensile tests to observe tensile strength, percent elongation, and fracture mechanisms. Furthermore, the hardness of the tensile bars was also taken despite seeing no difference in sample types. However, the as-cast samples did not consistently meet the requirements of percent elongation > 10.00% as there was a sample with 0.00% and another with 1.26%. These samples also showed brittle fracture, instead of the desired cup-and- cone ductile fracture. To investigate further, transverse sections …
Modifying Casting Parameters To Improve The High Temperature Ductility Of Investment Cast Nickel-Based Superalloy Pwa 1455, Lars Alexander Hedin, Cole Magnum Introligator
Modifying Casting Parameters To Improve The High Temperature Ductility Of Investment Cast Nickel-Based Superalloy Pwa 1455, Lars Alexander Hedin, Cole Magnum Introligator
Materials Engineering
PCC Structurals, an industry leader in superalloy investment castings, has observed inconsistencies in the stress rupture performance of polycrystalline nickel-based superalloy PWA 1455. PCC has changed their casting parameters to reduce the thermal gradient during cooling but have been unable to correlate these changes with an increase in stress rupture elongation. Metallographic examination of past samples indicated microstructures composed of non- equiaxed dendritic grains with mean diameter of .021 inches along the test axis. A similar study on polycrystalline superalloys has indicated that excessive superheat temperatures above the liquidus can result in large grains identical to those observed, limiting the …
Effect Of Overaging On Tensile Properties Of 2219-T852 Aluminum, Austin Bitter, Tristan Koyamatsu
Effect Of Overaging On Tensile Properties Of 2219-T852 Aluminum, Austin Bitter, Tristan Koyamatsu
Materials Engineering
This project investigated the overaging performance of aluminum alloy 2219-T852 for use in high temperature applications. 2219 aluminum is an alloy containing 5.8 to 6.8 percent copper, and is classified as a high strength age hardenable alloy. The sponsor for this project, Weber Metals, hopes to use 2219 Al to replace titanium in certain applications above the thermal limits of typical high strength Al. To test its performance, they manufactured round tensile samples and delivered them in peak aged, T852 condition. These samples were then overaged at a range of times and temperatures. The times in this experiment were one …
In Situ Sem Solidification Study Of Ga And Egain: A Characterization Technique For Monitoring The Microstructural Evolution Of Liquid Metals, Jeremy Geovann Del Aguila
In Situ Sem Solidification Study Of Ga And Egain: A Characterization Technique For Monitoring The Microstructural Evolution Of Liquid Metals, Jeremy Geovann Del Aguila
Materials Engineering
Scanning electron microscopy (SEM) video recording is used to characterize the solidification of small volumes of 99.999% pure gallium (Ga) and eutectic gallium-indium (eGaIn) under a high vacuum environment. Specimen are superheated to 55℃ using a hot plate, cast into spherical droplets, and cooled in situ by means of a Peltier cooling stage. Special attention is given to the preparation of the specimen prior to viewing because of gallium and its alloys’ nature to form an oxide layer when melted and air cooled. The oxide acts as a skin that inhibits the observation of microstructural features during solidification. Heated samples …
An Evaluation Of Ultrasonic Shot Peening And Abrasive Flow Machining As Surface Finishing Processes For Selective Laser Melted 316l, Rhys Gilmore
Master's Theses
Additive Manufacturing, and specifically powder bed fusion processes, have advanced rapidly in recent years. Selective Laser Melting in particular has been adopted in a variety of industries from biomedical to aerospace because of its capability to produce complex components with numerous alloys, including stainless steels, nickel superalloys, and titanium alloys. Post-processing is required to treat or solve metallurgical issues such as porosity, residual stresses, and surface roughness. Because of the geometric complexity of SLM produced parts, the reduction of surface roughness with conventional processing has proven especially challenging. In this Thesis, two processes, abrasive flow machining and ultrasonic shot peening, …
Temper Response Of A Vanadium Microalloy Steel, Bradley W. Hostetler
Temper Response Of A Vanadium Microalloy Steel, Bradley W. Hostetler
Materials Engineering
This investigation details the effect of a quench-and-temper processing treatment on the mechanical properties of a microalloy steel being considered for use as a pipeline flange. Microalloy steels are normally processed via Thermo-Mechanically Controlled Processing (TMCP) due to the increased strength from ferrite grain refinement; however, the geometry of a pipeline flange requires post processing beyond TMCP which diminishes the strengthening effect provided by TMCP. The purpose of this research project is to determine the mechanical properties produced when a vanadium microalloy steel is quenched and tempered. The two major considerations are the effect of tempering time on properties and …
Anomalous 304 Stainless Steel Mechanical Properties In Medical Guide Wires, Andrew Joseph Freeman
Anomalous 304 Stainless Steel Mechanical Properties In Medical Guide Wires, Andrew Joseph Freeman
Materials Engineering
Stainless steel medical guide wire cores, processed by Abbott Vascular, are returning anomalous mechanical properties upon strain hardening and heat treatment. As theory dictates, mechanical strength properties increase with strain hardening, and decrease with an annealing treatment. The opposite response is being observed. This is counter intuitive to fundamental materials knowledge, and a perfect materials engineering paradox. This project was designed to characterize these behaviors, and attempt to determine causation. To accomplish this, tensile testing of all processing steps mapped the mechanical property evolution of the wire. Published literature research revealed the potential of nitrogen and chromium solid state diffusion …
The Effects Of Varying Composition And Build Direction On Direct Metal Deposition Fabricated Inconel 718, Abigail P. Nilan, Jessica M. Fordham
The Effects Of Varying Composition And Build Direction On Direct Metal Deposition Fabricated Inconel 718, Abigail P. Nilan, Jessica M. Fordham
Materials Engineering
Inconel 718 (IN718) is a popular wrought superalloy, and is currently being investigated for additive manufacturing (AM) applications in the aerospace industry. However, overaging and the presence of microcracks have caused a significant reduction in properties. The purpose of this study is to meet or exceed the mechanical properties of wrought IN718 by varying the composition and build direction of the AM alloy. Alternative compositions were selected with Oerlilon Metco’s Rapid Alloy Development (RAD) software, and differ in niobium content, which increases the fraction of the primary strengthening phase (γʺ). Direct metal deposition (DMD) was used to fabricate the samples, …
Investigation Of Narloy-Z Yield Strength In Response To Changes In Ingot Processing And Heat Treatment, Stanley C. Goto, Sarah E. Wattenberg
Investigation Of Narloy-Z Yield Strength In Response To Changes In Ingot Processing And Heat Treatment, Stanley C. Goto, Sarah E. Wattenberg
Materials Engineering
This study investigates the effect of cooling rate on the yield strength of NARloy-Z. NARloy-Z is a copper-based alloy with 3 wt.% silver and 0.5 wt.% zirconium. The types of NARloy-Z were classified by the ingot processing (old or new) and the material lot (old or new). There were three variations of NARloy-Z in this study: old processing and material (Old/Old); old processing and new material (Old/New); and new processing and material (New/New). NARloy-Z undergoes a braze thermal cycle and age (BTCA) heat treatment for its application, and a single cooling rate within the BTCA was manipulated in this study. …
Effects Of Head Formation And Heat Treatment On The Mechanical Properties Of Connecting Rod Bolts, Caleb A. Leavitt, Matthew R. Lauretta
Effects Of Head Formation And Heat Treatment On The Mechanical Properties Of Connecting Rod Bolts, Caleb A. Leavitt, Matthew R. Lauretta
Materials Engineering
Oliver Racing Parts (ORP; Charlevoix, Michigan) is looking to optimize their manufacturing process for high-strength connecting rod bolts. A high yield strength is desired for the bolts because deformation would result in catastrophic engine failure. The bolts were made of H11, a chromium hot-work tool steel; and MLX17, a precipitation hardenable stainless steel. Tensile testing was performed to determine the tensile and yield strengths of the bolts. Fracture surfaces were imaged via scanning electron microscopy to characterize the failure modes. To observe the effects of bolt heading on microstructure and bolt strength, two batches of MLX17 were prepared; one batch …
Characterization Of Slm Printed 316l Stainless Steel And Investigation Of Microlattice Geometry, Finley H. Marbury
Characterization Of Slm Printed 316l Stainless Steel And Investigation Of Microlattice Geometry, Finley H. Marbury
Materials Engineering
The goal of this project was firstly to characterize Cal Poly’s SLM printed 316L stainless steel. SEM analysis showed Cal Poly’s as-printed 316L material to have a cellular dendritic microstructure containing mostly austenite and a small amount of δ-ferrite. After being heat treated to eliminate warp, its yeild and ultimate tensile strength were on par with the literature, however higher modulus and lower elongation were observed. XRD analysis confirmed residual stresses in the material, and that grains are preferentially oriented in both heat treated and non heat treated samples. The amount of porosity in the material was found to be …
Characterization Of The 15-5 Stainless Steel Electric Discharge Machining Recast Layer, Julian R. Lohser, Rhys W. Gilmore
Characterization Of The 15-5 Stainless Steel Electric Discharge Machining Recast Layer, Julian R. Lohser, Rhys W. Gilmore
Materials Engineering
Electric discharge machining (EDM) is a non-conventional machining process that is used for tough, hard materials or materials that require no tool force. Wire EDM produces a recast layer and heat-affected zone as a result of rapid melting and quenching at the surface of the cut. A secondary machining operation has been required to remove this layer. Previous estimates of the depth of the recast layer are likely too conservative due to improvements in the technology; therefore, the goal of this study is to characterize and more accurately investigate the size of the layer. Two EDM machine parameters, voltage and …
Tensile Properties Of High-Strength Connecting Rod Bolts, Leland K. Lam
Tensile Properties Of High-Strength Connecting Rod Bolts, Leland K. Lam
Materials Engineering
Oliver Racing Parts (ORP) is looking to optimize the manufacturing process for high-strength connecting rod bolts. A high yield strength is desired for the bolts because deformation would result in a loss of engine performance. A high tensile strength is also necessary to prevent catastrophic failure if deformation occurs. A high ductility as a proxy for toughness is attractive for resisting crack nucleation and growth during cyclic loading. Bolts were made of MP35N, a nickel-cobalt multiphase alloy; MLX-17, a precipitation hardenable stainless steel; 8740, a low alloy steel; and H11, a chromium hot-work tool steel. The temperature of the most …
Straightening Of Investment Casting Ni-Based Superalloys, Silvia Squillaci, Janessa Cabrera
Straightening Of Investment Casting Ni-Based Superalloys, Silvia Squillaci, Janessa Cabrera
Materials Engineering
Samples belonging to four different designs of afterburner flaps, available in the as-cast, solutionized and aged conditions, underwent 4-point bend testing to fracture to investigate straightening. The average maximum load values of the second design samples in the as-cast, solutionized and aged conditions were respectively 33 kN, 29 kN and 27 kN. Regarding the fourth design samples, the average maximum load for the as-cast, solutionized and aged conditions were respectively 23 kN, 28 kN, and 25 kN. The other parameter measured during testing was the maximum extension at fracture. All as-cast samples belonging to the second design fractured at values …
Effect Of Composition And Build Direction On Additively Manufactured Hastelloy X Alloys, Justin A. Spitzer, Jeffrey T. Schloetter, Sarah Zerga
Effect Of Composition And Build Direction On Additively Manufactured Hastelloy X Alloys, Justin A. Spitzer, Jeffrey T. Schloetter, Sarah Zerga
Materials Engineering
Microcracking has caused premature failure and reduction in properties in additively manufactured (AM) Hastelloy X. The purpose of this research is to meet or exceed the mechanical properties of wrought Hastelloy X by modifying the composition and build direction of Hastelloy X manufactured using Direct Metal Deposition (DMD). Tensile testing, scanning electron microscopy (SEM), and metallography were performed on the samples. ANOVA was used to analyze the dependence that the properties had on build direction and composition. The nominal composition wrought samples had a yield strength of 310.1 MPa and a 60.79% Elongation. Alloy P60-X18 in a horizontal build had …
Comparison Of Intrusive And Non-Intrusive Methods For Corrosion Monitoring Of Fuel Processing Systems, Armando Jacob Espinoza, Thomas Conner Field
Comparison Of Intrusive And Non-Intrusive Methods For Corrosion Monitoring Of Fuel Processing Systems, Armando Jacob Espinoza, Thomas Conner Field
Materials Engineering
This presentation contains an assessment of the best overall corrosion monitoring device, intrusive or non-intrusive, for use in the petrochemical industry. Corrosion in the petrochemical industry is a large issue because it causes a deterioration of pipe integrity in fuel processing systems. A reduction of pipe wall integrity due to corrosion could result in a leak or an explosion of fuel processing lines since those systems function at high pressures. The use of corrosion monitoring systems in the petrochemical industry helps to detect early signs of corrosion prior to failure so that proper maintenance can be performed to prevent catastrophe. …
Predicting Service Life Of 347 Stainless Steel Pipes By Carburization Rate Measurement, Tyler L. Sura
Predicting Service Life Of 347 Stainless Steel Pipes By Carburization Rate Measurement, Tyler L. Sura
Materials Engineering
Chevron Corporation and other refiners face challenges predicting the service life of piping in coker furnaces. This is largely due to a build up coke on a single surface of the piping. This coke build up results in carbon penetration into the surface of the 347 stainless steel used for the pipes. Carbon penetration can lead to degradation of the surface and ultimately, the failure of the pipe. Current modeling software has difficulty predicting the influence of sulfur on the carbon penetration rate. This study aims to provide a baseline for further study into the subject. The carbon penetration rate …
Development Of Low Cost Braze Alloys For Aerospace Applications, Alyssa M. Elliott, Sandy Babich, Blake Whitmee
Development Of Low Cost Braze Alloys For Aerospace Applications, Alyssa M. Elliott, Sandy Babich, Blake Whitmee
Materials Engineering
Non-precious metal braze alloys can help lower the cost of brazing, which is a commonly-used joining process in the aerospace industry. A-286, a stainless steel superalloy, and Inconel© 718, a nickel-based superalloy, are both commonly used alloys at Aerojet Rocketdyne. Both alloys were brazed into butt joints using nickel-based braze alloys: AMS 4776, 4777, and 4778. The brazed samples were machined into a modified version of the ASTM E8 subsize specimen samples and tensile tested to compare the strength and calculated elongation of the brazed samples to the base metals’ properties. All of the brazed samples fractured at the joint, …
Preliminary Investigations Into Selective Laser Melting, David Takeo Otsu
Preliminary Investigations Into Selective Laser Melting, David Takeo Otsu
Master's Theses
Selective laser melting is a promising metallic additive manufacturing process with many potential applications in a variety of industries. Through a gracious donation made by Lawrence Livermore National Laboratory, California Polytechnic State University received and installed an SLM 125 HL selective laser melting machine in February 2017. As part of the initial setup effort, a preliminary machine verification study was conducted to evaluate the general print quality of the machine with default parameter settings. Coincidentally, the as-printed microstructure of SLM components was evaluated through nil strength fracture surface examination, an alternative to conventional polish-and-etch metallography. A diverse set of components …
Kinked Tensile Behavior Of Cold Worked Nitinol, Grant R. Caraway, Samuel J. Canovas
Kinked Tensile Behavior Of Cold Worked Nitinol, Grant R. Caraway, Samuel J. Canovas
Materials Engineering
To characterize the decrease in ductility caused by an induced stress concentration as a function of various levels of cold work and heat treatment, Nitinol medical guide wires with a .004″ diameter were tested using both a standard, straight tensile test and a modified, bent tensile test. The ratio of the two break loads (bent:straight) for identically processed samples was used as a proxy for measuring the ductility of the guide wires: the higher the ratio, the more ductile the sample. The average break load ratio as a function of increased cold work, decreased from 1.27 to 0.91 for the …
Comparison Study Of Tensile Strength , Ductility, And Fracture Mode Of H11, Arp 2000, And Mp35n Connecting Rod Bolts For Use In High Performance Racing Engines, Megan Mccabe, Samuel Randall
Comparison Study Of Tensile Strength , Ductility, And Fracture Mode Of H11, Arp 2000, And Mp35n Connecting Rod Bolts For Use In High Performance Racing Engines, Megan Mccabe, Samuel Randall
Materials Engineering
Oliver Racing Parts (ORP) has historically purchased connecting rod bolts made of high strength, high cost, nickel-cobalt alloy, MP35N, and a medium strength, low cost, proprietary tool steel called ARP 2000. ORP has recently acquired capabilities to manufacture their own bolts. To determine the quality of their product as it compares to their previous supplier, ORP produced three different types of ⅜” diameter bolts: one set of bolts made of MP35N, and two sets of H11 bolts, designated H11A and H11B for their respective processing. The H11, ARP 2000, and MP35N bolts were tensile tested using a custom designed test …
Superalloy Metallurgy A Gleeble Study Of Environmental Fracture In Inconel 601, Alan C. Demmons
Superalloy Metallurgy A Gleeble Study Of Environmental Fracture In Inconel 601, Alan C. Demmons
Master's Theses
At temperatures above 0.5 Tm and in aggressive atmospheres predicting alloy performance is particularly challenging. Nickel alloys used in regimes where microstructure and properties are altered dynamically present unique requirements. Exposure may alter properties with unexpected early failure. The Gleeble is a valuable tool for investigation and simulation of thermo-mechanical properties of an alloy in various regimes up to the threshold of melting. In this study, four regimes of temperature and strain rate were simulated in an argon atmosphere to both investigate and document normal and abnormal failure modes. Commercial Inconel 601 was tested in selected regimes and in two …
Welding Procedure Qualification Of A36 Steel Plates Using The Gtaw And Gmaw Processes, Brecken Deoilers, Neri Lupian, Regan Rumph
Welding Procedure Qualification Of A36 Steel Plates Using The Gtaw And Gmaw Processes, Brecken Deoilers, Neri Lupian, Regan Rumph
Materials Engineering
The purpose of this project was to qualify welding procedure specifications for the Las Positas College welding program using A36 steel in accordance with American Welding Society (AWS) D1.1, B4.0, and B2.1. Qualification was to be performed using both 1G (flat) and 3G (vertical) positions for Gas Tungsten Arc Welding (GTAW) and Gas Metal Arc Welding (GMAW) processes. Required qualification procedures included two face and two root bend tests coupled with a visual inspection for cracks within the weld region greater than ⅛” long, along with two reduced section tensile tests to ensure the tensile strength exceeded 58 ksi if …
Effect Of Thermal Exposure On Tensile Strength And Microhardness Of Welded And Precipitation Hardened Rx82 Aluminum Alloy Extrusions In The T4 And T6 Conditions, Lucien Miller
Materials Engineering
This investigation is focused on the effect paint-bake cycles have on the tensile strength and microhardness of GMAW welded RX82 aluminum extrusions in T4 and T6 base conditions. To simulate the paint-bake cycle, T4 and T6 RX82 aluminum samples were GMAW welded and heat treated at 350°F, 390°F, and 425°F for durations of 30 minutes, 1.0 hour, and 2.0 hours, with five replicates for each treatment. Microhardness profiles of T4 samples treated at 350°F for 30 minutes and 1.0 hour display weld/HAZ HV values of 86.04 and 82.51 respectively, followed by maximums of 123.21 and 121.10. Average ultimate tensile strength …
Investigation Of Outlife Time On The Environmental Durability Of P2-Etched, Adhesively-Bonded Aluminum Alloys Using The Astm Wedge Test, Daniel Gross, Corey Sutton
Investigation Of Outlife Time On The Environmental Durability Of P2-Etched, Adhesively-Bonded Aluminum Alloys Using The Astm Wedge Test, Daniel Gross, Corey Sutton
Materials Engineering
P2 etchant is an environmentally-friendly aluminum etchant which has the potential to replace the Forest Products Laboratory (FPL) etchant as the industry standard. Environmental durability of adhesively-bonded aluminum surfaces etched using a paste version of the P2 etchant were tested using the Boeing-developed wedge test (ASTM D3762 - 03(2010)). This project specifically aimed to examine the relationship between outlife time (the time between etching and adhering) and the ability of bonded aluminum samples to pass the wedge test. Two aluminum alloys, 2024-T3 and 7075-T6, were wedge tested and the etched surfaces examined with an atomic force microscope (AFM) and a …
Effect Of Hydrogen Pick-Up And Release Behavior On The Tensile Properties Of Electroplated 4340m High-Strength Steel, Blake Daylor, Joshua Fisher, Alan Michelen Ruiz
Effect Of Hydrogen Pick-Up And Release Behavior On The Tensile Properties Of Electroplated 4340m High-Strength Steel, Blake Daylor, Joshua Fisher, Alan Michelen Ruiz
Materials Engineering
Hydrogen embrittlement of high-strength steel (4340M) was quantified through tensile testing and fractography (SEM). Three types of samples were obtained: rotating beam fatigue specimens, round (notched) tensile specimens, and flat panel specimens. In addition, three different plating types were analyzed (Ni, Cr, Cd-Ti) with a set of samples that was shot peened and a set that was not. Since some of the samples went through a hydrogen relief bake, another factor in our experiment was the amount of time it took for the samples to reach the baking process after they were electroplated (bake delay). There were three levels of …
Controlling Grain Size In Cold Worked And Annealed 1100 Aluminum To Optimize Ductility In Rocket Diaphragm Systems, Ryan Lewis, Bryce Simmons, Jessica Williams
Controlling Grain Size In Cold Worked And Annealed 1100 Aluminum To Optimize Ductility In Rocket Diaphragm Systems, Ryan Lewis, Bryce Simmons, Jessica Williams
Materials Engineering
Liquid propellant rocket diaphragms require extreme ductility. 1100 Aluminum is used for its high ductility, but the post-processing cold work and subsequent anneal result in excessively large grains. The effect of heat treatment and cold work on grain size in 1100 aluminum was explored. The samples were cold worked to 0, 5, 10, 15 and 30% using tensile elongation. The samples were then heat treated per AMS 2770 with either a "Steel Conduction" (1000 – 1150°F/min) or a "Production" (16 – 18°F/min) heating rate. The grain size of the samples were measured using the mean lineal intercept method. The grain …
Grain Orientation Effects On The Rotating-Bending Fatigue Properties Of Forged 7050-T7452 Aluminum Alloy, Matt Cristler, Jonas Zhang
Grain Orientation Effects On The Rotating-Bending Fatigue Properties Of Forged 7050-T7452 Aluminum Alloy, Matt Cristler, Jonas Zhang
Materials Engineering
In order to investigate the effects of grain orientation on the high cycle fatigue properties of 7050-T7452 aerospace grade aluminum, rotating-bending fatigue tests were performed on longitudinal (LG) and short transverse (ST) specimens taken from two sample sets (Method A and Method B) of open die forged 7050 aluminum. The fatigue specimens were machined to a 0.2" gage diameter and 4" length and subsequently hand polished to a mirror finish to minimize potential crack initiation sites. The tests were conducted on a Fatigue Dynamics RBF-300 HT tester in the fully reversed loading condition, with stress levels varying from 20 ksi …
Metals Additive Manufacturing Powder Aging Characterization, Thomas Russell Lovejoy, Nicholas Karl Muetterties, David Takeo Otsu
Metals Additive Manufacturing Powder Aging Characterization, Thomas Russell Lovejoy, Nicholas Karl Muetterties, David Takeo Otsu
Mechanical Engineering
The metallic additive manufacturing process known as selective laser melting requires highly spherical, normally distributed powder with diameters in the range of 10 to 50 microns. Previous observations have shown a degradation in powder quality over time, resulting in unwanted characteristics in the final printed parts. 21-6-9 stainless steel powder was used to fabricate test parts, with leftover powder recycled back into the machine. Powder samples and test specimens were characterized to observe changes across build cycles. Few changes were observed in the physical and mechanical properties of the specimens, however, there were indications of chemical changes across cycles. Potential …
An Investigation Of Incipient Melting During Solution Heat Treatment Of 7050 Aluminum Forgings And Its Effect On Corrosion Properties, Thomas Kilkenny
An Investigation Of Incipient Melting During Solution Heat Treatment Of 7050 Aluminum Forgings And Its Effect On Corrosion Properties, Thomas Kilkenny
Materials Engineering
7050 alloy (6.2Zn-2.3Mg-2.3Cu-0.12Zr) is a structural aluminum alloy commonly used in the aerospace industry. Its rich chemistry makes it susceptible to incipient melting. Incipient melting is a phenomenon where areas with high local alloy content melt before the rest of the material. This can cause a degradation of mechanical and corrosion properties. A six by four factor solution heat treatment trial was conducted. Six solution heat treatment temperatures, 890- 940°F in 10°F increments, and four times, 1, 2, 4, and 6 hours, were used. Incipient melting was observed in the 910°F, 6 hour solution heat treatment and all 920-940°F solution …