Metallurgy Commons^™

The Characterization And Nanomechanical Properties Of Microstructurally Complex Systems, Kerry Ann Baker

Theses and Dissertations--Chemical and Materials Engineering

Since the dawn of civilization, the use of metals has played an integral role in the evolution of human society. Over the years, and with the introduction of new engineering and science, we have learned how to combine metals to create new metallic systems. We have expanded our understanding of dealloying and chemical reactions, and, in doing so, we created nanoporous metals. Our use of metals has evolved from basic alloys such as bronze and steel to more complex alloys such as multi-principal element alloys. Nanoporous gold is an advanced metallic system that can be created through the dealloying process. …

Parametric Optimization Of Friction Stir Welding Of Aa6061-T6 Samples Using The Copper Donor Stir-Assisted Material Method, Aiman H. Al-Allaq, Joseph Maniscalco, Srinivasa Naik Bhukya, Zhenhua Wu, Abdelmageed Elmustafa

Mechanical & Aerospace Engineering Faculty Publications

This study presents an optimization of the process parameters for the effect of copper (Cu) donor material percentage on the friction stir welding (FSW) of AA6061-T6 alloy. Extensive factorial experiments were conducted to determine the significance of the rotational speed (ω), the transverse speed (v), the interface coefficient of friction (μ), and the Cu donor material percentage in the plunge, left, right, and downstream zones. Design Expert 13 software was used to identify the number of simulation experiments to be conducted using the Abaqus simulation software. From Design Expert 13, which is a thorough multi-objective optimization analysis software, we were …

Effect Of Boron In Cast Iron, Suyash Durendra Pawaskar

Masters Theses

"Boron, mostly considered a residual element, has started to cause issues in the cast iron foundries by causing a decrease in the strength of pearlitic gray and ductile iron castings. Because of the increase in the use of boron-added steel scrap from automotive steel and a lack of agreement on the critical levels of boron in cast iron, foundries are facing difficulties in controlling the microstructure of gray iron castings when boron is present. The current investigation was designed to analyze the effects of boron in cast irons and predict a mechanism to understand its effects with a vision of …

Strengthening Of 7175 Aluminum Alloy Through Multi-Step Aging Process, Colin E. Masterson, Ryland W. Jolliffe

Materials Engineering

7175 is a heat-treatable aluminum alloy commonly used in aerospace forgings. This alloy is aged with a multi-step heat treatment. This treatment must balance strength with stress corrosion cracking resistance through a degree of overaging. The team was tasked by Weber Metals to increase the strength of this treatment without sacrificing stress corrosion cracking resistance. Both two-step and retrogression and reaging treatments were tested in experiments to find a heat treatment that could increase the yield and tensile strength by 1-2 ksi while maintaining a minimum electrochemical conductivity equivalence of 38% relative to copper. Two-step aging is the more conventional …

Exploring Rapid Solidification And Equal Channel Angular Pressing In The Fabrication Of Mg-Based Alloys For Medical Applications, Emily Tom

Dissertations, Master's Theses and Master's Reports

The development of magnesium bioresorbable implants has become increasingly popular due to the increased need for temporary implants and magnesium’s excellent biocompatibility and suitable elastic modulus. Even though magnesium is an excellent candidate, when alloyed with other metals magnesium’s corrosion rate becomes too rapid for bioresorbable medical applications. The investigation into novel processing techniques to control the formation of precipitates to improve mechanical strength and ductility as well as corrosion rates has become of interest. This work investigates the combination of two nonequilibrium processing techniques, rapid solidification (RS) and equal channel angular pressing (ECAP), and the effects it has on …

Boron Nitride Nanotube Based Lightweight Metal Matrix Composites: Microstructure Engineering And Stress-Transfer Mechanics, Pranjal Nautiyal

FIU Electronic Theses and Dissertations

Lightweight metals, such as Aluminum, Magnesium and Titanium, are receiving widespread attention for manufacturing agile structures. However, the mechanical strength of these metals and their alloys fall short of structural steels, curtailing their applicability in engineering applications where superior load-bearing ability is required. There is a need to effectively augment the deformation- and failure-resistance of these metals without compromising their density advantage.

This dissertation explores the mechanical reinforcement of the aforementioned lightweight metal matrices by utilizing Boron Nitride Nanotube (BNNT), a 1D nanomaterial with extraordinary mechanical properties. The nanotubes are found to resist thermo-oxidative transformations up to ~750°C, establishing their …

Materials-Processing Relationships For Metal Fused Filament Fabrication Of Ti-6al-4v Alloy., Paramjot Singh

Electronic Theses and Dissertations

Additive manufacturing (AM) is at the mainstream to cater the needs for rapid tooling and small-scale part production. The metal AM of complex geometries is widely accepted and promoted in the industry. While several metal AM technologies exist and are matured to a level where expectation in terms of design and properties are possible to realize. But the metal AM suffers from the heavy expense to acquire equipment, isotropic property challenges, and potential hazards to work with loose reactive metal powder. With this motivation, the dissertation aims to develop the fundamental aspects to print metal parts with bound Ti-6Al-4V powder …

A Study On Ultrasonic Energy Assisted Metal Processing : Its Correeltion With Microstructure And Properties, And Its Application To Additive Manufacturing., Anagh Deshpande

Electronic Theses and Dissertations

Additive manufacturing or 3d printing is the process of constructing a 3-dimensional object layer-by-layer. This additive approach to manufacturing has enabled fabrication of complex components directly from a computer model (or a CAD model). The process has now matured from its earlier version of being a rapid prototyping tool to a technology that can fabricate service-ready components. Development of low-cost polymer additive manufacturing printers enabled by open source Fused Deposition Modeling (FDM) printers and printers of other technologies like SLA and binder jetting has made polymer additive manufacturing accessible and affordable. But the metal additive manufacturing technologies are still expensive …

Development Of Stage-I Tempered High Strength Cast Steel For Ground Engaging Tools, Viraj Ashok Athavale

Doctoral Dissertations

"Ground Engaging Tools (GET) are the expendable replacement parts used in heavy machinery used with mining or construction equipment. GET’s protect the expensive machine components from the wear and tear found common in high-impact or high-abrasion environments. The goal of this project is to develop advanced next-generation alloy choices that outperforms the existing GET materials. A method of predicting tempered hardness of mixed microstructures was formulated. Using this model, two alloy series viz. Cr-Ni-Mo and Mn-Si-Mo-V were proposed and experimented with the goal of obtaining a high strength and impact resistant cast steel. Cast iterations of Cr-Ni-Mo alloy series were …

Characterization Of Process Induced Defects In Laser Powder Bed Fusion Processed Alsi10mg Alloy, Edward Stugelmayer

Graduate Theses & Non-Theses

Additive manufacturing using laser powder bed fusion (AM-LPBF) methods have recently experienced rapid growth and development, having the potential to replace manufacturing by plastic deformation, precision machining, or casting. AM offers advantages such as the freedom to design highly complex geometries, time and cost savings through material usage efficiency and shortened production cycles, and the potential for improved mechanical properties. Process induced defects, however, result in degradation and scattering of mechanical properties and hinder the widespread adoption of AM-LPBF in industry. This investigation focuses on the effects of varying energy density and build orientation on the evolution of process induced …

Evaluation Of Metallurgical And Mechanical Properties Of Alsi10mg Produced By Selective Laser Melting, Luke J. Suttey

Graduate Theses & Non-Theses

Selective laser melting (SLM) additive manufacturing (AM) of metal powders has long been a focus in the study of AM due to the possibility of weight reduction, complex shape formation, and production cost savings. Although applicable to a variety of metals SLM AM of the AlSi10Mg alloy was studied in an attempt to characterize the effect of processing parameter and build angle variation on the final microstructural, fractographic, and mechanical properties of parts produced without any thermal post-processing techniques. Research was conducted on five build angles (0°, 30°, 45°, 60°, and 90°), and three Global Energy Densities (GED) (37.15, 45.39, …

Physical And Mechanical Properties Of Palm Kernel Oil-Based Polyester Polyurethane/Multi-Walled Carbon Nanotube Composites, Khairul Anuar Mat Amin, Muhammad Alif Zailani, Nurul Nabilah Zulkifli, Khairiah Haji Badri

Makara Journal of Technology

In this study, polyurethane (PU) films from palm kernel oil-based polyester (PKO-p) incorporated multi-walled carbon nanotubes (MWNTs) are prepared via a evaporative casting method. Nanoparticle fluid dispersions containing 0.02%, 0.03%, and 0.05% wt. of MWNTs are added into PKO-p based resin and mixed by digital probe sonicator for 30 min followed by mixing with isocyanate to produce PU-MWNTs composite films. The mechanical properties, swelling, water vapour transmission rate (WVTR) and conductivity of the PU-MWNTs composite films are examined. Results show that the toughness (T) or flexibility, the tensile strength (TS), and Young’s modulus (YM) values of PU-MWNTs composite films increase …

Microstructural Evolution And Mechanical Properties Of Zn-Ti Alloys For Biodegradable Stent Applications, Zhiyong Yin

Dissertations, Master's Theses and Master's Reports

Stents made of biodegradable metallic materials are increasingly gaining interest within the biomaterials field because of their superior mechanical properties and biodegradation rates as compared to polymeric materials. Zinc and its alloys have been developed and investigated as possible candidates for biodegradable stent applications in the last five years. This study intended to formulate and characterize a new series of Zn-Ti alloys, with titanium additions of less than 1-3 wt%, with the primary objective to develop and select an alloy that meets benchmark values of mechanical properties for biodegradable stents. A series of Zn-Ti alloys was formulated through vacuum induction …

Mechanical Properties Of Stainless Steels With Heterogeneous Nanostructures, Hiromi Miura, Masakazu Kobayashi, Natuko Sugiura, Naoki Yoshinaga

The 8th International Conference on Physical and Numerical Simulation of Materials Processing

No abstract provided.

Slm Processing-Microstructure-Mechanical Property Correlation In An Aluminum Alloy Produced By Additive Manufacturing, Bryce Abstetar

Graduate Theses & Non-Theses

Additive manufacturing has become a highly researched topic in recent years all over the world. The current research evaluates the merits of additive manufacturing based on the mechanical, microstructural, and fracture properties of additive manufactured AlSi10Mg test specimens. The additive manufactured build plates consisted of tensile and fatigue test specimens. They were printed in the 0°, 30°, 60°, and 90° orientations relative to the build platform. Tensile and dynamic fatigue tests were conducted followed by microstructural characterization and fracture analysis. A wrought 6061 T6 aluminum alloy was also tested for comparison. Tensile tests revealed similar ultimate tensile strengths for all …

Thermal Processing And Mechanical Properties Of Beta Phase Titanium Alloys For Biomedical Applications, Ethan Wood

Graduate Theses & Non-Theses

The past few decades have seen an increase in the use of beta titanium alloys as structural biomaterials. Their combination of excellent mechanical properties, corrosion resistance and biocompatibility, along with a lower Young’s modulus than stainless steel, cobalt-chromium and commercially pure titanium make the beta titanium alloys ideal biomaterials. This work evaluates the use of three beta titanium alloys for biomedical applications. Three beta titanium alloys, Ti 15-3-3-3, Ti SP-700 and Ti Beta-C, underwent thermal processing to optimize mechanical properties. The alloys were subjected to tensile testing, hardness testing, fatigue testing, optical microscopy and SEM fracture analysis in order to …

Influence Of Grain Size And Widmanstätten Colonies On Variability Of Tensile Properties Of Forged Ti-6al-4v, Blake T. Gaspar

Master's Theses

When testing forgings for specifications, it was found that some parts did not meet the requirements for mechanical properties. This triggered an investigation into two of the parts from the lot that did not meet specification. The ultimate reason for failure was due to lower than necessary yield strength and ultimate tensile strength values, as well as unwanted variability between regions of the part. Therefore, samples of the regions were tensile tested to determine the differences that existed in yield strength, ultimate tensile strength, and elongation. After tensile testing, quantitative metallography and fractography were conducted to identify aspects of the …

Medium Density Fibreboard Made Of Acetylated Sludge From Paper Mill, Luthfi Hakim, Evalina Herawati, I Nyoman Jaya Wistara

Makara Journal of Technology

Medium Density Fibreboard Made of Acetylated Sludge from Paper Mill. Research of using sludge as raw material for making medium density fibreboard (MDF) was useful to create additional value of sludge. The objective of the research was to evaluate physical properties, mechanical properties, and durability of MDF from acetylated sludge in 4 levels of acetate anhydride (0%, 3%, 5%, and 7%) with 3 replicates. The MDF was made using dry process. After materials were mixed with adhesives, they were pressed using hotpress under 170 oC temperature and 45 Pa pressure for 25 minutes. The size of the MDF sample was …

Effect Of Copper Addition On Mechanical Properties And Electrical Conductivity Of Pp/C-Cu Bipolar Plate Composites, Anne Zulfia, Taufik Abimanyu, Verina Warga Dalam

Makara Journal of Technology

Effect of Copper Addition on Mechanical Properties and Electrical Conductivity of PP/C-Cu Bipolar Plate Composites. Bipolar plate is a major component in PEM fuel cell which possess main function of collecting and removing electrons from anode to cathode. Therefore, materials for bipolar plates produced must have high electrical conductivity. To obtain bipolar plate materials which is cheap, lightweight and high conductivity, so it is developed bipolar plates material based on PP/C-Cu composite. PP/C-Cu composites has been made by mixing all materials then compounding, rheomix, hot blending and hot press. Cu (Copper) has been used various from 0.1 wt%, 1 wt% …

Mechanical Properties Of Ramie Fiber Reinforced Epoxy Lamina Composite For Socket Prosthesis, Tresna P. Soemardi, Widjajalaksmi Kusumaningsih, Agustinus Purna Irawan

Makara Journal of Technology

Mechanical properties of ramie fiber reinforced epoxy lamina composite for socket prosthesis. This paper presents an investigation into the application of natural fiber composite especially ramie fiber reinforced epoxy lamina composite for socket prosthesis. The research focuses on the tensile and shear strength from ramie fiber reinforced epoxy lamina composite which will be applied as alternative material for socket prosthesis. The research based on American Society for Testing Material (ASTM) standard D 3039/D 3039M for tensile strength and ASTM D 4255/D 4255M-83 for shear strength. The ramie fiber applied is a fiber continue 100 % Ne14'S with Epoxy Resin Bakelite …