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2018

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Articles 241 - 270 of 689

Full-Text Articles in Materials Science and Engineering

Spectral-Domain Phase-Sensitive Interferometry For Real-Time Probing Of Electrodeposition Processes, Yujen Chiu Aug 2018

Spectral-Domain Phase-Sensitive Interferometry For Real-Time Probing Of Electrodeposition Processes, Yujen Chiu

Material Science and Engineering Dissertations - Archive

Electrodeposition is a simple, versatile and scalable method for depositing thin metal films on conductive substrates, and it has long been used in large-scale industrial processes for metal film coating. In the last two decades, electrodeposition has entered into the manufacturing processes of electronic devices. Electrodeposition of Cu has become the standard process for the backend processes for almost all microelectronic devices. Electrodeposition of Cu and magnetic materials are used in the fabrication of write/read head in computer hard disk drive. More recently, a unique electrodeposition process, under potential deposition (UPD), has been utilized for atomic layer deposition to generate …

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Investigation Of Surface Contamination In A Cu-Based Al Alloy Occurring During Tem Sample Preparation, Kelly Claunch Aug 2018

Investigation Of Surface Contamination In A Cu-Based Al Alloy Occurring During Tem Sample Preparation, Kelly Claunch

Material Science and Engineering Theses - Archive

This thesis investigates the nature of surface contamination originating from the jet-polishing process on Cu-6 wt% Al TEM disks. During previous TEM imaging and diffraction analysis performed by our group, surface contamination particles, roughly 15-60 nm in diameter, were observed on the surface of the jet-polished TEM disks. Further, TEM diffraction analysis revealed that the contamination particles were growing epitaxially on the Cu matrix. HR-SEM was used to characterize the surface contamination in terms of shape, size, composition, and distribution on the surface of the disks. Through extensive HR-SEM imaging, it was found that surface contamination particles are present on …

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Design Survey Of Laminated Composite I-Beam, Mrinmoy Saha Aug 2018

Design Survey Of Laminated Composite I-Beam, Mrinmoy Saha

All Graduate Plan B and other Reports, Spring 1920 to Spring 2023

Composite I-beams are popular for high-strength low-weight applications. Learning the macro-mechanics and designing the composite I-beam properly are necessary. In this report, a design overview of the composite I-beam is discussed which is based on classical lamination theory where it includes the homogenization approach, the plane stress assumption and the Kirchhoff hypothesis. Using these assumptions, a method was developed to come up with the effective material properties of a beam. Formulas to calculate maximum deflection and maximum bending stress and shear stress and the stress concentration at the connection of web-flange are discussed which describe ways for designing and manufacturing …

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Application Of Nano-Plasmonics For Sers Bio-Detection And Photocatalysis In The Same Platform, Muhammad R. Shattique Aug 2018

Application Of Nano-Plasmonics For Sers Bio-Detection And Photocatalysis In The Same Platform, Muhammad R. Shattique

Graduate Theses/Dissertations

Nano-biological systems interfacing nano-structured solid surfaces with biological compounds such as oligonucleotides or proteins are highly regarded as enabling materials for biosensing and biocatalysis applications. In particular, nanostructures of noble metals such as gold or silver, when exposed to light, exhibit a phenomenon known as surface plasmon resonance. When a proper metal nanostructure (plasmonic substrate) is exposed to light, very efficient absorption of incoming photons is possible, resulting in a buildup of localized high-energy regions, or “hot-spots”, where energetic carriers or “hot carriers” can be created. These hot-carriers can be used to catalyze desired chemical transformations in materials located nearby. …

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The Effects Of Atmospheric Heat Treatments On Tio2 Nanotube Anodes For Lithium-Ion Batteries, Andreas Savva Aug 2018

The Effects Of Atmospheric Heat Treatments On Tio2 Nanotube Anodes For Lithium-Ion Batteries, Andreas Savva

Boise State University Theses and Dissertations

The effects of various heat treatments on the physical and electrochemical properties of anatase TiO2 nanotubes were studied in this work. Well-ordered TiO2 nanotubes were grown via electrochemical anodization and annealed at 450°C to induce a phase transformation to anatase. The heat treatments were conducted under atmospheres of O2, Ar, N2, and water vapor (WV) to create different point defects. The oxygen-deficient atmospheres were used to generate oxygen vacancies in the TiO2 nanotubes, while the water vapor treatment was used to create Ti vacancies by stabilizing them via the protonation of O sites. …

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Microstructure And Mechanical Properties Of Selective Laser Melted Superalloy Inconel 625., Md Ashabul Anam Aug 2018

Microstructure And Mechanical Properties Of Selective Laser Melted Superalloy Inconel 625., Md Ashabul Anam

Electronic Theses and Dissertations

Selective Laser Melting (SLM), a powder based Additive Manufacturing (AM) process, has gained considerable attention in the aerospace, biomedical and automotive industries due to its many potential benefits, such as, capability of fabricating complex three-dimensional components, shortened design to product time, reduction in process steps, component mass reduction and material flexibility. This process uses metallic powder and is capable of fabricating complex structures with excellent microstructure which make SLM not only an improvement over other manufacturing processes but also innovative material processing technology. Inconel 625, a nickel-based super alloy is widely popular in aerospace, chemical and nuclear industries. This alloy …

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High Dynamic Range Optical Devices And Applications., Elijah Robert Jensen Aug 2018

High Dynamic Range Optical Devices And Applications., Elijah Robert Jensen

Electronic Theses and Dissertations

Much of what we know about fundamental physical law and the universe derives from observations and measurements using optical methods. The passive use of the electromagnetic spectrum can be the best way of studying physical phenomenon in general with minimal disturbance of the system in the process. While for many applications ambient visible light is sufficient, light outside of the visible range may convey more information. The signals of interest are also often a small fraction of the background, and their changes occur on time scales so quickly that they are visually imperceptible. This thesis reports techniques and technologies developed …

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Incorporation Of Silica Nanoparticles Into The Underlayer Of Pda/Ptfe Thin Coatings, Adedoyin Abe Aug 2018

Incorporation Of Silica Nanoparticles Into The Underlayer Of Pda/Ptfe Thin Coatings, Adedoyin Abe

Mechanical Engineering Undergraduate Honors Theses

Polytetrafluoroethylene (PTFE) is one of the most low friction and corrosion resistant solid lubricants. Prior studies have shown that a polydopamine (PDA) underlayer enhances the durability of PTFE thin coating. In this study, 100, 200, and 300 µL of aqueous silica nanoparticle (NP) solutions were added to the PDA deposition solution. The durability and coefficient of friction of PDA/PTFE thin coatings on stainless steel substrates are investigated with and without incorporating the silica NPs. The coatings were tested in dry contact conditions using a Universal Mechanical Tester (UMT) with a ball-on-flat configuration in a reciprocating motion. It was found that …

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Modeling And Validations Of Control Parameters For Material Extrusion-Based Additive Manufacturing Of Thixotropic Aluminum Alloys., Lars Herhold Aug 2018

Modeling And Validations Of Control Parameters For Material Extrusion-Based Additive Manufacturing Of Thixotropic Aluminum Alloys., Lars Herhold

Electronic Theses and Dissertations

Additive Manufacturing (AM) with metals has been accomplished mainly through powder bed fusion processes. Initial experiments and simulations using Material Extrusion Additive Manufacturing (MEAM) have been performed by various researchers especially using low melting alloys. Recently Stratasys Inc. submitted a patent application for the use of their Material Extrusion technology also called Fused Deposition Modeling (FDM) where they describe the process using thixotropic semi-solid alloys. Currently this process using semi-solid, engineering type alloys such as A356 or THIXALLOY 540 aluminum have not been researched to evaluate the control parameters. This research combines the in-depth knowledge of applying thixotropic semi-solid aluminum …

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Irradiation Effects On Titanium Dioxide Electrodes For Lithium Ion Batteries, Kassiopeia Ann Smith Aug 2018

Irradiation Effects On Titanium Dioxide Electrodes For Lithium Ion Batteries, Kassiopeia Ann Smith

Boise State University Theses and Dissertations

This dissertation presents the mechanisms of irradiation induced defects and the resulting electrochemical response of TiO2 anode for ­lithium-ion-batteries. The objective is to realize pathways by which irradiation could be used to enhance the energy density of rechargeable lithium ion batteries in order to provide power to applications under extreme environments. Recent studies suggest that the presence of structural defects (e.g. vacancies and interstitials) in metal oxides may enhance the electrochemical charge storage capacity in electrode materials. One approach to induce defect formation in electrode materials is to use ion irradiation, which has been proven to produce point …

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New Methods For Understanding And Controlling The Self-Assembly Of Reacting Systems Using Coarse-Grained Molecular Dynamics, Stephen Thomas Aug 2018

New Methods For Understanding And Controlling The Self-Assembly Of Reacting Systems Using Coarse-Grained Molecular Dynamics, Stephen Thomas

Boise State University Theses and Dissertations

This research aims at developing new computational methods to understand the molecular self-assembly of reacting systems whose complex structures depend on the thermodynamics of mixing, reaction kinetics, and diffusion kinetics. The specific reacting system examined in this study is epoxy, cured with linear chain thermoplastic tougheners whose complex microstructure is known from experiments to affect mechanical properties and to be sensitive to processing conditions. Mesoscale simulation techniques have helped to bridge the length and time scales needed to predict the microstructures of cured epoxies, but the prohibitive computational cost of simulating experimentally relevant system sizes has limited their impact. In …

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Investigations On Hydrothermally Synthesized Co3o4/Mnxco3-Xo4 Core-Shell Nanoparticles, Ning Bian Aug 2018

Investigations On Hydrothermally Synthesized Co3o4/Mnxco3-Xo4 Core-Shell Nanoparticles, Ning Bian

Graduate Theses/Dissertations

Two different morphologies (pseudo-spherical shaped or PS type and hexagonal nanoplate shaped or NP type) and two different concentrations (0.07 M and 0.1 M) of manganese incorporated Co3O4@MnxCo3-xO4 core-shell nanoparticles (CSNs) were investigated, respectively. The motivation of this work is to investigate the magnetic properties of, and specifically the exchange bias, between different shaped CSNs and between different Mn-doped CSNs. A two-step synthesis method was utilized to obtain the CSNs: a soft chemical approach was used to obtain Co3O4 nanoparticles and a hydrothermal nano-phase epitaxy was used to …

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Improving And Augmenting The Anm Model For Three-Dimensional Virtual Concrete, Stephen Thomas Aug 2018

Improving And Augmenting The Anm Model For Three-Dimensional Virtual Concrete, Stephen Thomas

Boise State University Theses and Dissertations

The Anm model used for creating virtual concrete consisting of irregular shapes has been improved by integrating two existing algorithms: the extent overlap box (EOB) method for detecting contact between two irregular shapes and the uniform thickness shell algorithm. The EOB method has been compared with the previously used Newton-Raphson method and shown to be able to detect inter-particle contact with better accuracy and with less computational cost. Two parameters that define the balance between accuracy and performance of the EOB method have been identified and studied. The uniform thickness shell has been used to specify the minimum inter-particle distance …

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Electrocatalytic Properties Of Ni-Fe Basedalloys Toward Oxygen Evolution Reaction, Xiaodan Cui Jul 2018

Electrocatalytic Properties Of Ni-Fe Basedalloys Toward Oxygen Evolution Reaction, Xiaodan Cui

LSU Doctoral Dissertations

In this dissertation, laser-based manufacturing was applied to develop NiFe-based alloys, with focus on their electrochemical characteristics toward oxygen evolution reaction during water electrocatalysis. The targeted electrocatalysts were designed by combining catalysis principles of absorption energy, electronic effect and geometry effect. Firstly, a one-step laser-based manufacturing method was applied to prepare a thin layer of NiFe-based electrodes with varied Ni to Fe ratios to replace high-cost noble metals as the electrocatalyst for oxygen evolution reaction (OER). Since each Ni has 0.6 d-vacancy and each Fe atom has 2.2 d-vacancies. The alloying of Ni-Fe allows electrons flowing from Ni to Fe, …

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The Effect Of Rotational Speed, Friction Duration, And Pressure On Tensile Strength Of Aisi 6061 Welding Joints, Dewi Puspitasari, Poppy Puspitasari, M. Rizka Gita Firmansyah, Solichin Solichin Jul 2018

The Effect Of Rotational Speed, Friction Duration, And Pressure On Tensile Strength Of Aisi 6061 Welding Joints, Dewi Puspitasari, Poppy Puspitasari, M. Rizka Gita Firmansyah, Solichin Solichin

Journal of Mechanical Engineering Science and Technology (JMEST)

Electric arc welding with covered electrodes is ideally suited for flat plates. If this technique is employed for welding rigid bodies, the results would be of poor quality. One viable solution to weld rigid bodies is through friction welding. The study aimed to investigate the tensile strength of specimens subjected to friction welding with variations in rotational speed, friction time, and pressure and to examine the microstructure of friction welding joints. This research used the one-shot case study design and involved descriptive analysis. The descriptive analysis described the results of tensile testing and microstructure of welding joints. Results showed that …

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Pine Flower Waste Innovation As A Plant Based Program Augmented Reality, Ayik Bela Saputra, Imam Muhtarom, Ni’Matul Rochmaniyah, Ardhana Iswari Citra Padmi, Ika Rahmawati Jul 2018

Pine Flower Waste Innovation As A Plant Based Program Augmented Reality, Ayik Bela Saputra, Imam Muhtarom, Ni’Matul Rochmaniyah, Ardhana Iswari Citra Padmi, Ika Rahmawati

Journal of Mechanical Engineering Science and Technology (JMEST)

Indonesia one of the tropical countries in the world can not be separated from environment problems like other developing countries. One of the causes of declining environment quality is the decline of forests in Indonesia. In 2009, Indonesia’s forest area was by more than half, to about 88 million hectares. By the year 2013 the number is about 82 million hectares. One of the efforts to promote environment education is to familiarize planting plants to children from an early age from the school environment to the family environment. Therefore it is necessary an alternative in the form of planting media …

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Effect Of Mnfe2o4 Nanoparticles To Reduce Co And Hc Levels On Vehicle Exhaust Gas Emissions, Poppy Puspitasari, Sukarni Sukarni, Amir Hamzah Jul 2018

Effect Of Mnfe2o4 Nanoparticles To Reduce Co And Hc Levels On Vehicle Exhaust Gas Emissions, Poppy Puspitasari, Sukarni Sukarni, Amir Hamzah

Journal of Mechanical Engineering Science and Technology (JMEST)

The air pollution particle emitted from transportation in Indonesia Bay 2015 consist of 70.50% CO; 18.34% HC; 8.89% NOx; 0.88% SOx; 1.33%. These gases are very harmful to humans. To reduce the toxic gas effect, special treatment is needed, one of them is by applying catalyst on exhaust system. MnFe2O4 has the potential to bind the CO and HC elements contained in the exhaust gas. This study aims to investigate the effect of MnFe2O4 addition on catalityc converter towards CO gas and HC emissions of motor vehicles. Therefore, the percentage of exhaust reduction with and without applying MnFe2O4 on varied …

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Damage Simulation Of Pre-Forming V-Neck Plates With Variations In Material Type, Time And Temperature Using The Taguchi Method, Avita Ayu Permanasari, Rr. Poppy Puspitasari, Kevin Valiant Cahya, Mahfud Ihsan Jul 2018

Damage Simulation Of Pre-Forming V-Neck Plates With Variations In Material Type, Time And Temperature Using The Taguchi Method, Avita Ayu Permanasari, Rr. Poppy Puspitasari, Kevin Valiant Cahya, Mahfud Ihsan

Journal of Mechanical Engineering Science and Technology (JMEST)

In metal forming, damage can be caused by several factors: load on the workpiece, initial heating temperature, and temperature due to the friction between the die and the material for pre-forming. The metal forming process can be executed in 2 ways, namely by hot working and cold working. During these two types of mechanical working process, the metal undergoes plastic deformation. In hot working, the required deformation force is relatively low, and changes in mechanical properties are also insignificant. In cold working, a higher force is required, but the strength of the metal will increase significantly. The use of simulation …

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Mechanical Properties And Permeability Of Sand Casting Moulds With Eggshells Binder, Maryam Sharifi Jebeli Sharifi Jebeli, Wahyu Kurnianto, Wahono Wahono Jul 2018

Mechanical Properties And Permeability Of Sand Casting Moulds With Eggshells Binder, Maryam Sharifi Jebeli Sharifi Jebeli, Wahyu Kurnianto, Wahono Wahono

Journal of Mechanical Engineering Science and Technology (JMEST)

This research aimed to analyse whether or not eggshell could be a potential addition to sand mould composition as a binding material together with bentonite. Different amounts of eggshell material, i.e. 4%, 7%, 10% and 3%, were added to each sample. This study was a type of pre-experimental design called the one-shot case study. Among all sand moulds under study, sample 3 10% ES in dry conditions had the highest tensile, compressive and shear strengths of 0.09 Kg/cm2, 3.11 Kg/cm2 and 1.13 Kg/cm2, respectively. The results of the permeability test with heat treatment at 110˚C for 60 minutes showed that …

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Properties Of Cassava Starch Based Bioplastic Reinforced By Nanoclay, Nanang Eko Wahyuningtiyas, Heru Suryanto Jul 2018

Properties Of Cassava Starch Based Bioplastic Reinforced By Nanoclay, Nanang Eko Wahyuningtiyas, Heru Suryanto

Journal of Mechanical Engineering Science and Technology (JMEST)

Synthetic Synthetic plastic is chemical materials which cause severe environmental problems. Incinerating plastic waste leads to release of hazardous gases, which is not good for humans. Bioplastic can help reduce the dependence on fossil fuels and petroleum, that bioplastic can solve the problem of synthetic plastic use. This research aims to define the properties of the cassava starch-based bioplastic reinforced by nanoclay. Methods were experimental with bioplastic component of cassava starch, glycerol as plasticizer and nanoclay as reinforcement. The bioplastic was analyzed using XRD, tensile test, moisture absorption, biodegradability, and compared with another bioplastic. The results show that the addition …

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59th Annual Rocky Mountain Conference On Magnetic Resonance Jul 2018

59th Annual Rocky Mountain Conference On Magnetic Resonance

Rocky Mountain Conference on Magnetic Resonance

Final program, abstracts, and information about the 59th annual meeting of the Rocky Mountain Conference on Magnetic Resonance, co-endorsed by the Colorado Section of the American Chemical Society and the Society for Applied Spectroscopy. Held in Snowbird, Utah, July 22-27, 2018.

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A Rheometry Method To Assess The Evaporation-Induced Mechanical Strength Development Of Polymer Solutions Used For Membrane Applications, Eduard Caicedo Casso, Jessica L Sargent, Rachel M. Dorin, Ulrich B. Wiesner, William A. Phillip, Bryan M. Boudouris, Kendra Erk Jul 2018

A Rheometry Method To Assess The Evaporation-Induced Mechanical Strength Development Of Polymer Solutions Used For Membrane Applications, Eduard Caicedo Casso, Jessica L Sargent, Rachel M. Dorin, Ulrich B. Wiesner, William A. Phillip, Bryan M. Boudouris, Kendra Erk

School of Materials Engineering Faculty Publications

Rotational and oscillatory shear rheometry were used to quantify the flow behavior under minimal and significant solvent evaporation conditions for polymer solutions used to fabricate isoporous asymmetric membranes by the self-assembly and non-solvent induced phase separation (SNIPS) method. Three different A-B-C triblock terpolymer chemistries of similar molar mass were evaluated: polyisoprene-^-polystyrene-6-poly(4-vinylpyridine) (ISV); polyisoprene-6- polystyrene-6-poly(V,A-dimethylacrylamide) (ISD); and polyisoprene-Z>-polystyrene-h-poly(fer/- butyl methacrylate) (ISB). Solvent evaporation resulted in the formation of a viscoelastic film typical of asymmetric membranes. Solution viscosity and film viscoelasticity were strongly dependent on the chemical structure of the triblock terpolymer molecules. A hierarchical magnitude (ISV>ISB>ISD) was observed …

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Design Of Lattice Structures With Graded Density Fabricated By Additive Manufacturing, Wenjin Tao, Yong Liu, Austin T. Sutton, Krishna C. R. Kolan, Ming-Chuan Leu Jul 2018

Design Of Lattice Structures With Graded Density Fabricated By Additive Manufacturing, Wenjin Tao, Yong Liu, Austin T. Sutton, Krishna C. R. Kolan, Ming-Chuan Leu

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Lattice structures fabricated by Additive Manufacturing (AM) processes are promising for many applications, such as lightweight structures and energy absorbers. However, predicting and controlling of their mechanical behaviors is challenging due to the complexity of modeling and the uncertainties exist in the manufacturing process. In this paper, we explore the possibilities enabled by controlling the local densities. A set of lattice structures with different density gradients are designed using an implicit isosurface equation, and they are manufactured by Selective Laser Melting (SLM) process with 304L stainless steel. Finite element analysis and compression test are used to evaluate their mechanical properties. …

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Tunable Plasmonic Resonances In Highly Porous Nano-Bamboo Si-Au Superlattice-Type Thin Films, Ufuk Kılıç, Alyssa Mock, René Feder, Derek Sekora, Matthew J. Hilfiker, Rafal Korlacki, Eva Schubert, Christos Argyropoulos, Mathias Schubert Jul 2018

Tunable Plasmonic Resonances In Highly Porous Nano-Bamboo Si-Au Superlattice-Type Thin Films, Ufuk Kılıç, Alyssa Mock, René Feder, Derek Sekora, Matthew J. Hilfiker, Rafal Korlacki, Eva Schubert, Christos Argyropoulos, Mathias Schubert

Department of Electrical and Computer Engineering: Faculty Publications

We report on fabrication of spatially-coherent columnar plasmonic nanostructure superlattice-type thin films with high porosity and strong optical anisotropy using glancing angle deposition. Subsequent and repeated depositions of silicon and gold lead to nanometer-dimension subcolumns with controlled lengths. The superlattice-type columns resemble bamboo structures where smaller column sections of gold form junctions sandwiched between larger silicon column sections (“nano-bamboo”). We perform generalized spectroscopic ellipsometry measurements and finite element method computations to elucidate the strongly anisotropic optical properties of the highly-porous nano-bamboo structures. The occurrence of a strongly localized plasmonic mode with displacement pattern reminiscent of a dark quadrupole mode is …

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Synthesis And Characterization Of Polyaniline Agglomerates And Polyaniline Nanoparticles To Use As Printed Sensors To Detect Spoilage Of Catfish During Refrigerated Storage, Vashti Martae Campbell Jul 2018

Synthesis And Characterization Of Polyaniline Agglomerates And Polyaniline Nanoparticles To Use As Printed Sensors To Detect Spoilage Of Catfish During Refrigerated Storage, Vashti Martae Campbell

LSU Master's Theses

There is growing interest in the development of sensors contained in packaging for seafood that are applicable at the consumer level to monitor freshness in a non-destructive manner. Total volatile basic nitrogen (TVB-N) analysis indicates the freshness of seafood. TVB-N analysis is sensitive to the spoilage compounds comprised of ammonia, trimethylamine, dimethylamine, and biogenic amines commonly found in seafood and whose concentration increases when spoilage microbial growth occurs. However, TVB-N analysis is laborious and is not suitable for use at the consumer level. Polyaniline (PANI) is a polymer that may be used as a sensor for detecting TVB-N in seafood. …

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The Effect Of Processing Conditions On The Energetic Diagram Of Cdte Thin Films Studied By Photoluminescence, Shamara P. Collins Jul 2018

The Effect Of Processing Conditions On The Energetic Diagram Of Cdte Thin Films Studied By Photoluminescence, Shamara P. Collins

USF Tampa Graduate Theses and Dissertations

The photovoltaic properties of CdTe-based thin films depend on recombination levels formed in the CdTe layer and at the heterojunction. The localized states are resultant of structural defects (metal sublattice, chalcogen sublattice, interstitial), controlled doping, deposition process, and/or post-deposition annealing. The photoluminescence study of CdTe thin films, from both the bulk and heterojunction, can reveal radiative states due to different defects or impurities. Identification of defects allows for potential explanation of their roles and influence on solar cell performance. A thorough understanding of the material properties responsible for solar cell performance is critical in further advancing the efficiency of devices. …

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Properties Of Matter, Mike Jackson, Holly Haney Jul 2018

Properties Of Matter, Mike Jackson, Holly Haney

High School Lesson Plans

Students will investigate the relationship(s) between thermal and electrical properties of matter. First, students will use a multimeter and temperature probe to investigate the relationship between electrical resistance and temperature of an electrical resistor composed of metals. They will then graph collected data to analyze the relationship and draw a conclusion as to their relationship. They will then perform the same investigation on a thermal resistor made of a semiconducting substance and analyze that collected data. Finally, using ClaimEvidence-Reasoning (CER) structure, students will use their experimental evidence to state the similarities and differences between the electro-thermal properties of metals and …

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Molecular Assembly Of Monolayer-Protected Gold Nanoparticles And Their Chemical, Thermal, And Ultrasonic Stabilities, Steven Ray Isaacs Jul 2018

Molecular Assembly Of Monolayer-Protected Gold Nanoparticles And Their Chemical, Thermal, And Ultrasonic Stabilities, Steven Ray Isaacs

Masters Theses & Specialist Projects

Gold monolayer-protected nanoclusters (MPCs) with average diameters of 1-5 nm protected by alkane- and arenethiolates were synthesized. Mixed-monolayer protected nanoparticles (MMPCs) were prepared by functionalizing hexanethiolate-protected MPCs with either 11-mercaptoundecanoic acid (MUA-MMPC), 11-mercaptoundecanol (MUO-MMPC), or 4-aminothiophenol (ATP-MMPC) using ligand place exchange. Presentation of various chemical reagents such as nucleophile, acid, or base and change in physical environment through ultrasonic and thermal irradiation resulted in changes to particles and their physical properties. Thermogravimetric analysis (TGA) was used to measure maximum temperature of the derivated thermogravimetric peaks (Tmax,DTG) as a means of comparing temperature dependence of mass loss. The absorption spectrum within …

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Structural Transformations In Porous Glasses Under Mechanical Loading. I. Tension, Nikolai V. Priezjev, Maxim A. Makeev Jul 2018

Structural Transformations In Porous Glasses Under Mechanical Loading. I. Tension, Nikolai V. Priezjev, Maxim A. Makeev

Mechanical and Materials Engineering Faculty Publications

The evolution of porous structure and mechanical properties of binary glasses under tensile loading were examined using molecular dynamics simulations. We consider vitreous systems obtained in the process of phase separation after a rapid isochoric quench of a glass-forming liquid to a temperature below the glass transition. The porous structure in undeformed samples varies from a connected porous network to a random distribution of isolated pores upon increasing average glass density. We find that at small strain, the elastic modulus follows a power-law dependence on the average glass density and the pore size distribution remains nearly the same as in …

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Detonation Synthesis Of Alpha-Variant Silicon Carbide, Martin Langenderfer, Catherine E. Johnson, William Fahrenholtz, Vadym Mochalin Jul 2018

Detonation Synthesis Of Alpha-Variant Silicon Carbide, Martin Langenderfer, Catherine E. Johnson, William Fahrenholtz, Vadym Mochalin

Mining Engineering Faculty Research & Creative Works

A recent research study has been undertaken to develop facilities for conducting detonation synthesis of nanomaterials. This process involves a familiar technique that has been utilized for the industrial synthesis of nanodiamonds. Developments through this study have allowed for experimentation with the concept of modifying explosive compositions to induce synthesis of new nanomaterials. Initial experimentation has been conducted with the end goal being synthesis of alpha variant silicon carbide (α-SiC) in the nano-scale. The α-SiC that can be produced through detonation synthesis methods is critical to the ceramics industry because of a number of unique properties of the material. Conventional …

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