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Articles 301 - 329 of 329

Full-Text Articles in Materials Science and Engineering

An Investigation Of Graphite Peek Composite Under Compression With A Centrally Located Circular Discontinuity, Benjamin Wham Ii Mar 1993

An Investigation Of Graphite Peek Composite Under Compression With A Centrally Located Circular Discontinuity, Benjamin Wham Ii

Theses and Dissertations

The purpose of this thesis was to determine (both experimentally and analytically) the initiation and progression of failure, stress-strain response, and the failure loads of Graphite/Polyetheretherketone (Gr/PEEK) laminates, incorporating a centrally located circular discontinuity, loading in axial compression at room temperature. The laminates studied were (0°)16,(90°)16, (0°/90°)4S, (± 45°)4S, and (0°/±45°/90°)2S. The specimens were loaded within a Boeing Open Hole Compression Fixture. The micromechanical failure modes were identified using a Scanning Electron Microscope. The analytical progression of failure was predicted using a nonlinear finite element code developed by Dr. R.S. …

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Design And Performance Evaluation Of A Gas Chromatograph Micromachined In A Single Crystal Silicon Substrate, Rocky R. Reston Mar 1993

Design And Performance Evaluation Of A Gas Chromatograph Micromachined In A Single Crystal Silicon Substrate, Rocky R. Reston

Theses and Dissertations

This investigation designed and developed a miniature gas chromatograph (GC) using silicon micromachining techniques. The GC is composed of a miniature sample injector (10 µl sample loop); a 0.9 m long, rectangular-shaped (300 µm width and 10 micrometers height) capillary column coated with a 0.2 µm thick copper phthalocyanine (CuPc) stationary phase; and a dual-detector scheme incorporating a CuPc-coated chemiresistor and a 125 µm diameter thermal conductivity detector bead. Micromachining was employed to fabricate the sample injector interface, the GC column, and the dual-detector cavity. A novel processing technique was developed to sublime the CuPc stationary phase coating on the …

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Luminescence Study Of Ion-Implanted And Mbe-Grown Er-Doped Gaas And AlXGa1-XAs, Jose E. Colon Mar 1993

Luminescence Study Of Ion-Implanted And Mbe-Grown Er-Doped Gaas And AlXGa1-XAs, Jose E. Colon

Theses and Dissertations

The excitation and de-excitation mechanisms of the 1.54 microns emissions, from ion implanted and MBE grown GaAs:Er and AlxGa1-xAs:Er, were studied through luminescence experiments. Experimental techniques included photoluminescence, time resolved photoluminescence, and selective excitation photoluminescence. The Er3+ emissions were studied as a function of Er concentration, aluminum mole friction, n- and p-type doping level, and annealing temperature. In addition oxygen co-doping studies were done in order to determine the role played by oxygen in the Er3+ luminescence.

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The Effect Of Oxide Layers And Boron Doping On The Breakdown Of High Purity Silicon, Brian A. Hibbeln Dec 1992

The Effect Of Oxide Layers And Boron Doping On The Breakdown Of High Purity Silicon, Brian A. Hibbeln

Theses and Dissertations

For many applications such as lasers and radar drive circuits, there exists a need for solid state high voltage, high current switches. Current gaseous discharge switches fail to satisfy the ruggedness, reliability, and lifetime requirements of today's systems. A promising alternative is the Photoconductive Semiconductor Switch (PCSS). The limiting factor in the operation of these switches is the occurrence of breakdown through channels formed slightly below the surface. A theory on the formation of these channels is presented based upon band bending at the metal-semiconductor interface, a nonhomogeneous space charge due to irregular trap distributions, and thermal runaway in localized …

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Investigation Of Fatigue Behavior In Notched Cross-Ply Titanium Metal Matrix Composite At Elevated Temperature, Robert P. Baker Dec 1992

Investigation Of Fatigue Behavior In Notched Cross-Ply Titanium Metal Matrix Composite At Elevated Temperature, Robert P. Baker

Theses and Dissertations

The objective of this research was to investigate the initiation and progression of damage which develops in notched (0/90)2S SCS-6/Ti-15-3 at elevated temperature. Testing consisted of a monotonic tensile test at 427°C followed by fatigue testing performed under load control with a stress ratio of 0.1 at a frequency of 10 Hz. A crack was defined to have initiated when it had attained a length greater than or equal to 0.124 mm. Crack initiation and progression was monitored by strain and modulus observations and visual inspection via telemicroscope. The cracks were recorded with edge and face replicas. Metallographic and …

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Behavior Of A Titanium Matrix Composite Under Quasi-Static Tensile And Compressive Loading, Keith L. Bearden Dec 1992

Behavior Of A Titanium Matrix Composite Under Quasi-Static Tensile And Compressive Loading, Keith L. Bearden

Theses and Dissertations

Quasi-Static tensile and compressive testing was performed on a unidirectional titanium matrix composite. The specific material was SCS-9/β 21S. The initial tensile and compressive modulus for both laminates was the same. The ninety degree laminate had a tensile and compressive modulus of 115.89 GPa. The zero degree laminate had a tensile and compressive modulus of 197.51 GPa. The ninety degree laminate exhibited a three stage stress/strain response in tension. The first stage is completely linearly elastic, however, partial debonding of the fiber from the matrix was observed. This partial debased did not effect the stress/strain response. The second stage is …

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Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite Under Tension-Tension And Tension-Compression Loading, Frank A. Opalski Dec 1992

Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite Under Tension-Tension And Tension-Compression Loading, Frank A. Opalski

Theses and Dissertations

A study was conducted which investigated the behavior of a cross-ply [0/90]2S Nicalon/Calcium-Aluminosilicate (Nicalon/CAS) ceramic matrix composite at room temperature under tension-compression fatigue loading. Material behavior and damage was recorded by stress-strain curves, elastic modulus, hysteretic energy density, and acetate replication techniques. Tension-tension fatigue tests at a load ratio R of 0.1 (R = σmin/σmax) were completed which determined that 140 MPa was the maximum stress allowable in which cycle runout (1,000,000 cycles) would occur. Above this value, transverse crack density increased with respect to cycles and failure ultimately occurred. Tension-compression tests were then performed …

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Computational And Experimental Investigation Into Fracture Of Brittle Fiber - Brittle Matrix Composite Systems, James P. Solti Dec 1992

Computational And Experimental Investigation Into Fracture Of Brittle Fiber - Brittle Matrix Composite Systems, James P. Solti

Theses and Dissertations

Experimental and computational analyses provided an improved understanding of quasi-static fracture in model composite systems. Constant displacement compression tests using borosilicate glass double cleavage drilled compression test templates provided qualitative assessments of localized toughening for crack growth near cylindrical inclusions. Large crack-tip stress fields induced interfacial slip and separation prior to arrival of the main crack. Debonding and the proliferation of secondary matrix cracks characterized the role of bridging fibers along weak interfaces. Strong residual normal compressive interfacial stresses diminished the influence of crack-tip stresses; however, slip was still observed. VHS tape and computer enhanced photos record a history of …

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Excitation And De-Excitation Mechanisms Of Er-Doped Gaas And Algaas, David W. Elsaesser Dec 1992

Excitation And De-Excitation Mechanisms Of Er-Doped Gaas And Algaas, David W. Elsaesser

Theses and Dissertations

Electrical and optical characterization have been performed on GaAs and AlxGa1-xAs samples doped with Er either by ion implantation or during Molecular Beam Epitaxial (MBE) growth. Deep Level Transient Spectroscopy (DLTS) and Temperature-Dependent Hall Effect (TDH) measurements indicated the presence of two hole traps in Er-doped GaAs, at 35 and 360 meV above the valence band maximum. The former (shallower) center was thought to be due to Er substituting for a Ga atom (ErGa) and giving rise to an isoelectronic impurity potential. The second center was attributed to an Er atom occupying an interstitial …

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Phase Conjugation In Optical Fiber Via Stimulated Brillouin Scattering With Feedback From A Barium Titanate Crystal, Patrick R. Emmert Dec 1992

Phase Conjugation In Optical Fiber Via Stimulated Brillouin Scattering With Feedback From A Barium Titanate Crystal, Patrick R. Emmert

Theses and Dissertations

The goal of this thesis was to obtain phase conjugation in multi-mode optical fiber via stimulated Brillouin scattering (SBS) with the aid of a barium titanate crystal which formed a phase conjugate cavity for the Stokes beam. SBS was demonstrated but the SBS threshold was unaffected by the presence of the barium titanate crystal and no evidence for the presence of phase conjugation in the optical fiber was obtained.

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Behavior Of A Quasi-Isotropic Ply Metal Matrix Composite Under Thermo-Mechanical And Isothermal Fatigue Loading, Karl A. Hart Dec 1992

Behavior Of A Quasi-Isotropic Ply Metal Matrix Composite Under Thermo-Mechanical And Isothermal Fatigue Loading, Karl A. Hart

Theses and Dissertations

This study investigated the behavior of the SCS6/Ti-15-3 metal matrix composite with a quasi-isotropic layup when tested under static and fatigue conditions. Specimens were subjected to in-phase and out-of-phase thermo- mechanical and isothermal fatigue loading. In-phase and isothermal loading produced a fiber dominated failure while the out-of-phase loading produced a matrix dominated failure. Also, fiber domination in all three profiles was present at higher maximum applied loads and al three profiles demonstrated matrix domination at lower maximum applied loads. Thus, failure is both profile dependent and load equipment. Additional analyses, using laminated plate theory, Halpin-Tsai equations, METCAN, and the Linear …

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Open And Filled Hole Static Tensile Strength Characterization Of Metal Matrix Composite Scs-9/Β21s, Jacob T. Roush Dec 1992

Open And Filled Hole Static Tensile Strength Characterization Of Metal Matrix Composite Scs-9/Β21s, Jacob T. Roush

Theses and Dissertations

SCS-9/β21s has a reduced gauge thickness, in comparison with other metal matrix composites, due to a smaller diameter fiber. This reduced gauge thickness makes it an attractive candidate for the skin of hypersonic vehicles. Tensile testing of (0/90)2s and (O/±45/90)s laminates was performed at room temperature, 482°C, and 650°C. Both notched and unnotched specimens were tested. Notched specimens, open and filled hole, had a width-to-diameter ratio of six. Materials 7075-T6 and Mar-m-246 were used as pins in the filled hole tensile testing. Analytical work was completed to predict material properties, elastic and plastic stress concentration factors, residual stresses, …

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Behavior Of A Centrally Notched Cross-Ply And Unidirectional Ceramic Matrix Composite In Tension-Compression Fatigue, William A. Weidenaar Dec 1992

Behavior Of A Centrally Notched Cross-Ply And Unidirectional Ceramic Matrix Composite In Tension-Compression Fatigue, William A. Weidenaar

Theses and Dissertations

Centrally notched (hole), cross-ply, ((0/90)2)s, and unidirectional, (0)8 laminates of Silicon Carbide fiber-reinforced Aluminosilicate glass, SiC/1723, were fatigue tested under tension-compression loading with a load ratio of -1. Damage accumulated continuously for both lay- ups, leading to eventual failure and a reduced fatigue life. Critical damage in the cross-ply consisted of longitudinal cracks in the 90° plies growing and combining with transverse cracks to effectively eliminate the 90° plies' load carrying capability and allowing the specimen to buckle. Critical damage in the unidirectional lay-up consisted of longitudinal cracks which initiated at the shear stress concentration …

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Stratified Plate Model For Composite Plate Analysis, Richard A. Coveno Dec 1992

Stratified Plate Model For Composite Plate Analysis, Richard A. Coveno

Theses and Dissertations

This study continues the investigation of the stratified plate model for the analysis of composites plates. The strata theory models a composite plate as a stack of isotropic matrix and orthotropic, fiber dominated layers. Energy methods are used to derive a set of partial differential equations and boundary conditions as a function of the displacement. An assumed displacement field, of a polynomial in z and a Sine/Cosine function in x and y, generates a solution to a simply supported composite plate with cross plies. A cylindrical bending example is also solved with a polynomial in z and Sine/Cosine function in …

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Effect Of Thickness And Ply Layup On The Collapse Characteristics Of Cylindrical Composite Shells With Large Cutouts, James C. Hatfield Dec 1992

Effect Of Thickness And Ply Layup On The Collapse Characteristics Of Cylindrical Composite Shells With Large Cutouts, James C. Hatfield

Theses and Dissertations

This study involved a numerical and experimental investigation of the geometric instability(collapse loads/displacements) of vertically unsupported graphite/epoxy cylindrical shell panels undergoing axial compression. Symmetric quasi-isotropic and cross-ply laminates, with and without 4 X4 centralized cutouts, were investigated for three thicknesses:8,16,and 24 plies. The experimental data was compared to results from SHELL, a geometrically nonlinear finite-element computer program which incorporates a parabolic transverse shear strain distribution through the thickness. Good correlation was obtained for shells with large cutouts between the SHELL numerical data and the experimental results. This research verified that the SHELL program will provide good predictions of the collapse …

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Cathodoluminescence Spectroscopy Of Zinc Germanium Phosphide Zngep2, Michael R. Gregg Dec 1992

Cathodoluminescence Spectroscopy Of Zinc Germanium Phosphide Zngep2, Michael R. Gregg

Theses and Dissertations

Zinc Germanium Phosphide (ZnGeP2) is a nonlinear semiconductor suitable for use as a laser tuning element over the two to six micron wavelength range. Although this crystal has been studied in the past, its luminescent properties are not yet well understood. In this present study, ZnGeP2 has been examined using cathodoluminescence spectroscopy (CL). Specifically, the spectral dependence of the CL was obtained as a function of electron beam energy, beam current and temperature. The resulting CL was found to be polarized with a peak structure that was dependent on the polarization. This peak structure observed by CL …

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Processability Of Polythiophene Thin Films By Ultraviolet Photo Bleaching, Derek D. Fletcher Dec 1992

Processability Of Polythiophene Thin Films By Ultraviolet Photo Bleaching, Derek D. Fletcher

Theses and Dissertations

Materials possessing strong 𝜒(3) optical properties such as Polythiophene are sought for the production of optical switches. Polythiophene thin films produced by plasma enhanced CVD show a surface rms roughness of 10-15 angstroms over single square micron areas which is acceptable for wave guiding in the near IR. This research investigates permanently changing the optical properties of such a thin film by exposure to UV radiation (254 nm, 35 mW/cm2), known as photo bleaching, in hope of creating a refractive index boundary for use in total internal reflection. After 60 minutes exposure the refractive index shows …

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A Response Surface Methodology Study Of Ferroelectric Memory Devices, Kevin C. Smith Mar 1992

A Response Surface Methodology Study Of Ferroelectric Memory Devices, Kevin C. Smith

Theses and Dissertations

Fatigue in ferroelectric memory devices was studied. The application of fatigue pulses to a ferroelectric sample was controlled by the RT-66 Ferroelectric Tester, a variation of the Sawyer-Tower circuit. The RT-66 also controlled data collection following the fatiguing process. Seven variables were evaluated for their potential- affect on fatigue. A sequence of fatigue tests, which varied the settings of these variables, was developed using Response Surface Methodology (RSM) experimental designs. Least-squares regression models were developed once a particular RSM set of design experiments was completed. These models were evaluated using RSM tools, and the analysis of these models allowed the …

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Characterizing The Sensitivity, Selectivity, And Reversibility Of The Metal-Doped Phthalocyanine Thin-Films Used With The Interdigitated Gate Electrode Field-Effect Transistor (Igefet) To Detect Organophosphorous Compounds And Nitrogen Dioxide, Clayton P. Howe Dec 1991

Characterizing The Sensitivity, Selectivity, And Reversibility Of The Metal-Doped Phthalocyanine Thin-Films Used With The Interdigitated Gate Electrode Field-Effect Transistor (Igefet) To Detect Organophosphorous Compounds And Nitrogen Dioxide, Clayton P. Howe

Theses and Dissertations

This study investigated the sensitivity, reversibility, and selectivity of the thin film coatings used on the interdigitated gate electrode field effect transistor (IGEFET) gas microsensor. These responses were quantified based on the dc resistance changes and frequency domain responses of the microsensor. The thin-film materials included: copper phthalocyanine (CuPc), nickel phthalocyanine (NiPc), and cobalt phthalocyanine (CoPc). The challenge gases included: diisopropyl methylphosphonate (DIMP), dimethyl methylphosphonate (DMMP), nitrogen dioxide, ammonia, and boron trifluoride. Tests of the CuPc thin-films and nitrogen dioxide challenges established the primary set of test parameters expected to maximize the selectivity, sensitivity, and reversibility of the thin-film coatings. …

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Crack Growth Rate Modeling Of A Titanium-Aluminide Alloy Under Thermal-Mechanical Cycling, John J. Pernot Dec 1991

Crack Growth Rate Modeling Of A Titanium-Aluminide Alloy Under Thermal-Mechanical Cycling, John J. Pernot

Theses and Dissertations

In this study, a model is developed to predict crack growth rates in a titanium-aluminide alloy under thermal-mechanical fatigue (TMF). This TMF crack growth rate prediction model, which requires only isothermal data to define its parameters, is distinguished from earlier models in two ways. First, it accounts for mechanical-fatigue and environmental crack growth rate contributions while it also considers a retardation mechanism thought to be caused by creep blunting of the crack tip. This is the first study to account for such a retardation mechanism during TMF. The second uniqueness of the model is that its general form can account …

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Thermomechanical Fatigue Of Scs-6/Β21-S [0/90]2s Composite, Dana G. Hanson Dec 1991

Thermomechanical Fatigue Of Scs-6/Β21-S [0/90]2s Composite, Dana G. Hanson

Theses and Dissertations

The objective of this study was to investigate the material behavior of SCS-6/β21-S [0/90]2s in a thermomechanical fatigue environment. Samples of the SCS-6/β21-S composite were subjected to in-phase and out-of-phase cyclic loading; four samples were tested under in-phase conditions and eight samples were tested under out-of-phase conditions. Stress, temperature, and total strain values were acquired during the test sequence and analyzed for indication of possible trends. Experimental results indicated in-phase specimen possessed shorter fatigue lives then their out-of-phase counterparts above the static first ply failure of the matrix. The out-of-phase specimen showed a shorter fatigue life below the first …

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Failure Characterization Of A Fiber Reinforced Ceramic Matrix Composite With Circular Holes, Daniel E. Bullock Dec 1991

Failure Characterization Of A Fiber Reinforced Ceramic Matrix Composite With Circular Holes, Daniel E. Bullock

Theses and Dissertations

The purpose of this study was to investigate the performance of a fiber reinforced ceramic matrix composite with circular holes. The specific objectives were to (1) determine the relationship between tensile failure stress and the ratio of hole diameter to specimen width, and (2) to examine the initiation and progression of damage. The ceramic matrix composite used was SiC/ 1723, composed of continuous silicon titanium carbide fibers in an aluminosilicate glass ceramic matrix. Uniaxial tensile tests were performed at room temperature on two different layups; unidirectional [0]8, and [0/90]2s symmetric. Each layup was tested at three diameter-to-width …

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Calculated Point Defect Properties Of The Intermetallic Compounds Nickel Titanium (Niti) And Iron Titanium (Feti), Russell T. Lutton Mar 1991

Calculated Point Defect Properties Of The Intermetallic Compounds Nickel Titanium (Niti) And Iron Titanium (Feti), Russell T. Lutton

Theses and Dissertations

Atomistic simulation with a modified version of the DYNAMO code was used to calculate the point defect properties of the intermetallic compounds nickel titanium and iron titanium. The calculated energies are believed to be experimentally accurate to within +/- 0.1 eV. Vacant Ni or Fe lattice sites were preferred and had energies of 6.356 eV for NiTi and 5.899 eV for FeTi. Removing a Ti atom resulted in a neighboring antisite defect caused by migration of a Ni or Fe atom into the vacant Ti site. These configurations had energies of 7.024 eV for NiTi and 6.336 eV for FeTi. …

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Low Temperature Photoluminescence Study Of Holmium And Thulium Implanted Into Iii-V Semiconductors And Silicon, Eric Silkowski Dec 1990

Low Temperature Photoluminescence Study Of Holmium And Thulium Implanted Into Iii-V Semiconductors And Silicon, Eric Silkowski

Theses and Dissertations

Low temperature photoluminescence studies were performed on holmium implanted into InP, GaAs, and Si; and thulium implanted into AlGaAs, GaAs, and Si. Samples were annealed by the conventional furnace and rapid thermal techniques. None of the characteristic 4f emissions of holmium were found in the spectral region of .73 to 1.55 eV. AlGaAs:Tm showed strong thulium emissions in the .93 to 1.03 eV region. These emissions were studied and compared to those in GaAs:Tm. Low and high temperature annealed samples showed evidence of trivalent Tm centers. Temperature dependence studies showed that thulium 4f emissions were present above 200 K but …

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Characterization Of Barium Titanate As An Optical Amplifier, George A. Vogel Dec 1990

Characterization Of Barium Titanate As An Optical Amplifier, George A. Vogel

Theses and Dissertations

The introduction of two-beam coupling in photorefractive materials has resulted in an extensive amount of research into their use as optical processing/computing elements. This dissertation develops the theoretical equations for two-beam coupling in barium titanate as an optical amplifier. One of the factors which limits the optical gain in photorefractive crystals is the loss of pump beam power to the amplification of parasitic light (beam fanning). This parasitic light is produced by light scattered from the pump beam by imperfections on both the crystal face and within the crystal. Through the analysis of signal and noise amplification as functions of …

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Angle Of Arrival Detection Through Artificial Neural Network Analysis Of Optical Fiber Intensity Patterns, Scott Thomas Dec 1990

Angle Of Arrival Detection Through Artificial Neural Network Analysis Of Optical Fiber Intensity Patterns, Scott Thomas

Theses and Dissertations

The optical sensors of United States Air Force reconnaissance vehicles, such as satellites, are subject to temporary or permanent blinding from hostile (or threat) laser radiation. By detecting and determining the angle of arrival (AOA) of the hostile radiation, the reconnaissance vehicle may be able to protect its optical sensors by taking evasive maneuvers or by shutting down the optical sensor (such as closing a shutter) until the threat has passed. In addition, the vehicle can relay information to its ground terminal allowing the intelligence community to determine the source of the hostile laser radiation. This thesis demonstrated that an …

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Investigation Of Damage Mechanisms In A Cross-Ply Metal Matrix Composite Under Thermo-Mechanical Loading, Joel J. Schubbe Dec 1990

Investigation Of Damage Mechanisms In A Cross-Ply Metal Matrix Composite Under Thermo-Mechanical Loading, Joel J. Schubbe

Theses and Dissertations

Metal matrix composites (MMCs) are rapidly becoming strong candidates for high temperature and high stiffness structural applications such as the Advanced Tactical Fighter (ATF). This study systematically investigated the failure modes and associated damage in a cross-ply, [0/90]2s SCS6/Ti-15-3 metal matrix composite under in-phase and out-of-phase thermomechanic fatigue. Initiation and progression of fatigue damage were recorded and correlated to changes in Young's Modulus of the composite material. Experimental results show an internal stabilization of reaction zone size but degradation and separation from constituent materials under extended cyclic thermal loading. Critical to damage were transverse cracks initiating in the 90° …

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Fluorescent Lifetime Measurements Of Rare Earth Elements In Gallium Arsenide, Danny J. Topp Dec 1990

Fluorescent Lifetime Measurements Of Rare Earth Elements In Gallium Arsenide, Danny J. Topp

Theses and Dissertations

Lifetime measurements of the excited states of three GaAs semiconductors doped with the rare earth elements Erbium (ER), Praseodymium (Pr) , and Thulium (Tm) has been studied using a pulsed nitrogen laser and germanium detector. The measurements were made with an experimental set up with a system response time of 0.34 micro seconds. A 330 milliwatt nitrogen laser with a wavelength of 3370 angstrums was used to excite transitions of the rare earth elements.

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Investigation Of The Platinum-Rich Portion Of The Platinum-Tantalum Phase Diagram, Bob Dean Browning Aug 1961

Investigation Of The Platinum-Rich Portion Of The Platinum-Tantalum Phase Diagram, Bob Dean Browning

Theses and Dissertations

The Pt-Ta binary system was investigated at two isotherms;1000°C and 1500°C, and at eleven alloy compositions in the range of 50 to 100 atomic percent platinum. The alloys were examined by x-ray diffraction and metallography. Three intermetallic compounds, Pt2Ta, Pt3Ta, and Pt4Ta were found to exist in this composition range. The Pt4Ta intermetallic appeared only at the 1500°C isotherm. Platinum dissolved tantalum substitutionally to 90 atomic percent at 1500 °C and to approximately 80 atomic percent at 1000 °C.

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