Mechanics of Materials Commons^™

Mechanical Characterization And Modeling Of Rat Myocardia Under The Influence Of Epirubicin, Abdallah Mahmoud Alkhaiyat

Theses and Dissertations

Cancer remains a predominant health challenge that is responsible for a significant portion of global morbidity and mortality. Epirubicin (EPI), a chemotherapeutic anti-cancer drug, has shown remarkable efficacy in combating various malignancies. However, it is known to have undesirable side effects on the heart, collectively referred to as cardiotoxicity. This research investigates the adverse effects of chemotherapy on cardiac contractility through an in vitro examination of the mechanics of healthy and infarcted animal heart tissues. Electrically stimulated slices of rat ventricular tissue were tested using an isometric force measurement tissue bath. The tissue slices were subjected to uniaxial stretching, allowing …

Tensile Creep Of A Hybrid Polymer-Matrix/Ceramic-Matrix Composite At Elevated Temperature, Waleed S. Alshehri

Theses and Dissertations

Advanced aerospace systems require structural materials that can perform reliably in high-temperature environments for long durations. The performance of standard polymer matrix composites (PMCs) in these conditions is often limited by their susceptibility to time-dependent deformation, such as creep. The objective of this research is to characterize the high-temperature creep behavior of a novel unitized material system comprising a polymer matrix composite (PMC) and a ceramic matrix composite (CMC) co-cured together. The PMC part consists of the polyimide matrix reinforced with laminated carbon fibers woven in an eight harness satin weave (8HSW). The CMC part consists of a zirconia-based ceramic …

Shape Memory Behavior In Medium To High Entropy Shape Memory Alloys: Design, Prediction, And Experimental Analysis, Hatim Raji

Theses and Dissertations

This dissertation provides a data-driven system integrating synthetic data generation and machine learning (ML) techniques to create multicomponent SMA compositions with specific transformation temperatures (TTs). Models were trained to represent the nonlinear dependencies influencing martensitic transformation behavior by using elemental, thermodynamic, and process-related aspects. The capacity of the ML models on medium entropy NiTiHfPd and high entropy NiTiHfZrCu systems accuracy was confirmed by experimental validation showing TTs closely matched with model outputs.

Experimental And Theoretical Fracture Analysis Of Additively Manufactured Orthotropic V-Notches, Venkata Siva Sainath Bavapuram

Theses and Dissertations

This study presents a comprehensive investigation into the fracture behavior of additively manufactured orthotropic V-notched components made of Acrylonitrile Butadiene Styrene (ABS) material. The research integrates both theoretical and finite element approaches to evaluate stress intensity factors (SIFs) in Modes-I and II, which are fundamental in characterizing stress field distributions around notches under applied loading conditions. Unlike isotropic materials, where stress fields depend only on geometry of the component, the anisotropic nature of 3D-printed ABS introduces a dependency on material properties that necessitate different approaches to include anisotropy of the material.

Tensile specimens are 3D-printed with specific material orientations to …

Improvement Of Microcracking And Mechanical Properties Of Tungsten Fabricated Via Laser Powder Bed Fusion Through Alloying With Reactive Secondary Constituents, William S. Mockel

Theses and Dissertations

Tungsten (W), a Group VI transition metal, possesses a number of advantageous properties, most notably its impressive mechanical performance at extreme temperatures. While tungsten's nature render traditional manufacturing methods difficult, additive manufacturing through laser powder bed fusion (LPBF) presents a promising avenue for fabricating tungsten components. However, the material’s high ductile-to-brittle transition temperature combined with the embrittling effect of impurities mean that the residual stresses imparted by LPBF result in microcracking in tungsten, degrading its usefulness. This study sought to improve the characteristics of LPBF-W through the removal of embrittling oxygen content via alloying with low concentrations of reactive elements, …

Mechanical Response Of Triply Periodic Minimal Surface Gyroid Structures Under Combined Loading, Jay B. Patel

Theses and Dissertations

This work explored combined tensile and torsional loads applied to additively manufactured Inconel 718 specimens employing Triply Periodic Minimal Surface (TPMS) structures. The gyroid TPMS unit cell was selected with two variations of cylindrical cell maps, a rectangular cell map, and a spherical cell map. All four variants were tested in an axial-torsion test frame at room temperature using equal parts of vertical and angular displacement control until failure. The combined loading in these tests utilized tension and torsion. The data from the tests were compared to finite element analysis (FEA) models to visualize when yielding was predicted. Finally, the …

Fatigue Behavior Of Two Advanced C/Sic Composites At 1200°C In Air, Conner A. Adams

Theses and Dissertations

High-temperature tension-tension fatigue behavior of two advanced carbon/silicon carbide (C/SiC) ceramic matrix composites (CMCs) was investigated. Both composites were reinforced with T300 carbon fibers. Laminated carbon fiber preforms consisted of 24 plies of plain weave fabric in a 0/90 layup. The first composite, C/CVI-SiC, was processed by chemical vapor infiltration (CVI) of SiC into the fiber preform. Prior to the CVI process, the fiber preforms were coated with a duplex pyrolytic carbon and boron carbide fiber coating to create a weak fiber- matrix interphase. The second composite, C/HYPR-SiC, was also processed via CVI, but had an oxidation inhibited matrix comprising …

Fatigue Behavior Of An Advanced Sic/Sic Composite With An Array Of Small Cooling Holes At 1200°C, Tess K. Panchyshyn

Theses and Dissertations

Tension-tension fatigue behavior of an advanced melt-infiltrated (MI) silicon carbide/silicon carbide (SiC/SiC) composite was evaluated, and basic tensile properties measured, at 1200°C in laboratory air.  The composite consists of a melt-infiltrated SiC matrix reinforced with laminated Hi-Nicalon Type-S fibers woven in a 5-harness satin weave. The Hi-Nicalon-S fiber preforms were coated with a boron nitride (BN) fiber coating by chemical vapor infiltration (CVI). The melt-infiltrated matrix was consolidated by combining CVI-SiC with SiC particulate slurry and molten silicon infiltration. The finished ceramic matrix composite (CMC) had a fiber volume fraction of 33%. Additionally, the effect of multiple small holes on …

Insights Into The Characterization And Degradation Of Electrospun Polycaprolactone Scaffolds For Tissue Engineering Applications, Caleb B. Wells

Theses and Dissertations

Electrospun polymeric biodegradable scaffolds are essential in tissue engineering, particularly for Engineered Tissue Vascular Grafts (ETVGs), which promise advancements in treating coronary artery disease, peripheral arterial disease, congenital cardiovascular defects, and renal disease. These scaffolds present a solution to issues with autologous graft availability and durability. While large-diameter grafts in low-pressure environments have seen success, small-diameter grafts in high-flow scenarios remain challenging. Understanding polymeric scaffold degradation and behavior during incubation, especially under dynamic mechanical loading, is vital for clinical translation of small-caliber ETVGs.

This research focuses on characterizing the mechanical and microstructural properties of electrospun polycaprolactone (PCL) scaffolds and their …

Analyzing The Effects Of Ultrafast Laser Processing On Mechanical Properties Of 3d-Printed Pla Parts, Darshan Pramodbhai Yadav

Theses and Dissertations

Recent advances in additive manufacturing technologies have already led to wide-scale adoption of 3D-printed parts in various industries. The expansion in choice of materials that can be processed, particularly using Fused Deposition Modeling (FDM), and the steady advancements in dimensional accuracy control have extended the range of applications far beyond rapid prototyping. However, additive manufacturing still has considerable limitations compared to traditional and subtractive manufacturing processes. This work addresses limitations associated with the as-deposited surface roughness of 3D-printed parts. The effects of roughness-induced stress concentrations were studied on ultimate tensile strength and fatigue life. The samples were manufactured using a …

Nanoscale Modeling Of Membrane Systems Under Mechanical Deformation In Traumatic Brain Injury Using Molecular Dynamics, Anh Thi Ngoc Vo

Theses and Dissertations

Neuronal membrane disruption and mechanoporation are nanoscale damage mechanisms that critically affect brain cell viability during traumatic brain injury (TBI). These nanoscale cellular impairments are elusive in experiments and necessitate in silico approaches such as molecular dynamics (MD) simulations. Implementing MD, this research aims to investigate the effects of different key factors related to membrane deformation and damage, including force field resolutions, lipid compositions, and loading conditions.

To examine the impact of force field resolution, MD deformation simulations were conducted on 1-palmitoyl-2-oleoyl-sn-glycero-3-phosphatidylcholine (POPC) lipid bilayer membranes, using all-atom (AA), united-atom (UA), and coarse-grained Martini (CG-M) force fields. The mechanical responses …

Challenges And Signal Processing Of High Strain Rate Mechanical Testing, Barae Lamdini

Theses and Dissertations

Dynamic testing provides valuable insight into the behavior of materials undergoing fast deformation. During Split-Hopkinson Pressure Bar testing, stress waves are measured using strain gauges as voltage variations that are usually very small. Therefore, an amplifier is required to amplify the data and analyze it. One of the few available amplifiers designed for this purpose is provided by Vishay Micro-Measurements which limits the user’s options when it comes to research or industry. Among the challenges of implementing the Hopkinson technology in the industry are the size and cost of the amplifier. In this work, we propose a novel design of …

Rational Design Of Flexible And Stretchable Electronics Based On 3d Printing, Yuanhang Yang

Theses and Dissertations

Flexible and stretchable electronics have been considered as the key component for the next generation of flexible devices. There are many approaches to prepare the devices, such as dip coating, spin coating, Mayer bar coating, filtration and transfer, and printing, etc. The effectiveness of these methods has been proven, but some drawbacks cannot be ignored, such as lacking pattern control, labor consuming, requiring complex pretreatment, wasting conductive materials, etc.

In this investigation, we propose to adopt 3D printing technology to design flexible and stretchable electronics. The objective is to rationally design flexible and stretchable sensors, simplify the preparation process, form …

Evaluation Of Additively Manufactured Lattices Under High Strain Rate Impact, Derek G. Spear

Theses and Dissertations

Several additively manufactured lattice designs and configurations were evaluated under compression loads under various strain rates from quasi-static to highly dynamic. These experiments examined how the mechanical behavior of the lattice changed based on the lattice design properties and the applied strain rates. The modulus of elasticity, yield strength, plateau stress, and toughness were observed to decrease with an increase in strain rate, revealing that the lattice designs exhibit a negative strain rate sensitivity. A new lattice flow stress model was developed to account for the mechanical response of the lattice and was incorporated into a computational model for simulation. …

Fluid-Structure Interaction Of Nrel 5-Mw Wind Turbine, Mohamed Sayed Elkady Abd-Elhay

Theses and Dissertations

Wind energy is considered one of the major sources of renewable energy. Nowadays, wind turbine blades could exceed 100 m to maximize the generated power and minimize produced energy cost. Due to the enormous size of the wind turbines, the blades are subjected to failure by aerodynamics loads or instability issues. Also, the gravitational and centrifugal loads affect the wind turbine design because of the huge mass of the blades. Accordingly, wind turbine simulation became efficient in blade design to reduce the cost of its manufacturing. The fluid-structure interaction (FSI) is considered an effective way to study the turbine's behavior …

Shock Migration On An Oscillating Straked Delta Wing Using An Unsteady Euler Solver, Alexander J. Brown

Theses and Dissertations

This research contributes to the understanding of Shock Induced Trailing Edge Separation (SITES) as a driver of Limit Cycle Oscillation (LCO) by performing a computational investigation of nonlinear aerodynamic phenomena on a straked delta wing in transonic flow, oscillating in pitch. ZEUS, an Euler-based aeroelastic solver with a boundary layer coupling scheme meant to capture viscous flow effects within the boundary layer, was used to analyze aerodynamic flow around the wing for various mean incidence angles, oscillation amplitudes, and Mach numbers within the transonic region. The dynamic characteristics of the airflow around the wing were investigated in order to characterize …

Experimental And Computational Analysis Of Progressive Failure In Bolted Hybrid Composite Joints, John S. Brewer

Theses and Dissertations

Composite materials are strong, lightweight, and stiff making them desirable in aerospace applications. However, a practical issue arises with composites in that they behave unpredictably in bolted joints, where damage and cracks are often initiated. This research investigated a solution to correcting the problem with composite bolted joints. A novel hybrid composite material was developed, where thin stainless steel foils were placed between and in place of preimpregnated composite plies during the cure cycle to reinforce stress concentrations in bolted joints. This novel composite was compared to control samples experimentally in quasi-static monotonic loading in double shear configuration in 9-ply …

Fatigue Behavior Of An Advanced Melt-Infiltrated Sic/Sic Composite With Environmental Barrier Coating At 1200°C In Air And In Steam, Thaddeus M. Williams

Theses and Dissertations

Advanced aerospace applications such as aircraft turbine engine components, hypersonic flight vehicles, and spacecraft reentry thermal protection systems require structural materials that have superior long-term mechanical properties under high temperature, high pressure, and varying environmental factors, such as moisture. Because of their low density, high strength and fracture toughness at high temperatures SiC fiber-reinforced SiC matrix composites are being evaluated for aircraft engine hot-section components. In these applications the composites will be subjected to various types of mechanical loadings at elevated temperatures in oxidizing environments. Because their constituents are intrinsically oxidation-prone, the most significant problem hindering SiC/SiC composites is oxidation …

Generation Of Warm Dense Plasma On Solar Panel Infrastructure In Exo-Atmospheric Conditions, Harrison C. Wenzel

Theses and Dissertations

The use of a weaponized thermo-nuclear device in exo-atmospheric conditions would be of great impact on the material integrity of orbiting satellite infrastructure. Particular damage would occur to the multi-layered, solar cell components of such satellites. The rapid absorption of X-ray radiation originating from a nuclear blast into these layers occurs over a picosecond time scale and leads to the generation of Warm Dense Plasma (WDP). While incredibly difficult and costly to replicate in a laboratory setting, a collection of computational techniques and software libraries may be utilized to simulate the intricate atomic and subatomic physics characteristics of such an …

Manufacture Of Fused Deposition Modeling Joints Using Ultem 9085, Zane A. Willburn

Theses and Dissertations

The manufacture of joints between a base structure and a structure manufactured via Fused Deposition Modeling (FDM) will be investigated. ULTEM 9085, a high temperature plastic with potential aerospace applications, will be the material used. The specific application this research is focused on is a robotic and mobile FDM printer capable of building structures onto other structures in space. A joint will be formed by fusing the base layer of the printed structure and the top of the base structure together. Tensile testing will be performed to determine the strength of the bond between parts. Tensile specimens will be manufactured …

Creep Of Hafnium Diboride -20 Vol% Silicon Carbide At 1500°C In Air, Glen E. Pry

Theses and Dissertations

Refractory metal borides, commonly referred to as Ultra High Temperature Ceramics (UHTCs), exhibit a number of unique properties, such as extremely high melting temperature and hardness, chemical stability, high electrical and thermal conductivity and corrosion resistance. It has been demonstrated that the addition of SiC improves the oxidation resistance of ZrB2- and HfB2-based UHTCs above 1200°C by modifying the composition of the oxide scale. Addition of SiC retards the oxidation rate of ZrB2 and HfB2 by forming a protective layer of borosilicate glass. Creep deformation is one of the critical criterion for structural application of ceramics at elevated temperatures. Compression …

Tensile Properties And Fatigue Behavior Of Geopolymer Matrix Composites With Carbon Fiber Reinforcement At Elevated Temperature, Steffan M.L. Wilcox

Theses and Dissertations

The tensile stress-strain and tension-tension fatigue of geopolymer matrix composites reinforced with 0/90 carbon fibers was investigated at 23 and 300°C in laboratory air. Geopolymers are inorganic polymeric materials composed of alumina, silica, and alkali metal oxides. Because geopolymers are synthesized as a fluid mixture or particles and liquid, they can be cast into a desired shape, and cured at only slightly elevated temperatures. The relative ease of synthesis and low processing temperatures make geopolymers an attractive choice as a matrix material for composite materials. Geopolymers also offer resistance to heat and oxidizing environments. Currently, geopolymer matrix composites are being …

Consuming Digital Debris In The Plasticene, Stephen R. Parks

Theses and Dissertations

Claims of customization and control by socio-technical industries are altering the role of consumer and producer. These narratives are often misleading attempts to engage consumers with new forms of technology. By addressing capitalist intent, material, and the reproduction limits of 3-D printed objects’, I observe the aspirational promise of becoming a producer of my own belongings through new networks of production. I am interested in gaining a better understanding of the data consumed that perpetuates hyper-consumptive tendencies for new technological apparatuses. My role as a designer focuses on the resolution of not only the surface of the object through 3-D …

Stressed Oxidation Of Hafnium Diboride In Air At 1500°C, Thomas A. Bowen

Theses and Dissertations

Hypersonic vehicles with narrow airfoils produce thin boundary layers and shock temperatures in excess of 2000°C, exceeding the operating limits of traditional aerospace materials. The use of ultra-high temperature ceramics (UHTCs) allows for operating temperatures far exceeding those of metallic alloys. One such UHTC is hafnium diboride (HfB₂). Transition metal diborides generally experience significant oxidation degradation at elevated temperatures. The use of additives, such as silicon carbide (SiC) has been shown to reduce the oxidation of transition metal diborides. This research focused on the compressive creep of HfB₂ with varying amounts of SiC in air at 1500°C. …

Experimental Investigation Of Mechanical Behavior Of An Oxide/Oxide Ceramic Composite In Interlaminar Shear And Under Combined Tension-Torsion Loading, Skyler R. Hilburn

Theses and Dissertations

Creep behavior in interlaminar shear of an oxide-oxide ceramic composite, Nextel 720™/aluminosilicate (N720/AS), was investigated at 1100°C in laboratory air and in steam. The interlaminar shear strength (ILSS) was determined as 7.65 MPa. The creep behavior was examined for interlaminar shear stresses in the 2-6 MPa range. Primary and secondary creep regimes were observed in all tests conducted in air and in steam. Tertiary creep was noted in the tests performed at 6 MPa. Larger creep strains and higher creep strain rates were produced in steam. Surprisingly, the presence of steam had a beneficial effect on creep lifetimes. It appears …

An Experimental Investigation Of Friction Bit Joining In Az31 Magnesium And Advanced High-Strength Automotive Sheet Steel, Rebecca Gardner

Theses and Dissertations

Friction Bit Joining (FBJ) is a recently developed spot joining technology capable of joining dissimilar metals. A consumable bit cuts through the upper layer of metal to be joined, then friction welds to the lower layer. The bit then snaps off, leaving a flange. This research focuses on FBJ using DP980 or DP590 steel as the lower layer, AZ31 magnesium alloy as the top layer, and 4140 or 4130 steel as the bit material. In order to determine optimal settings for the magnesium/steel joints, experimentation was performed using a purpose-built computer controlled welding machine, varying factors such as rotational speeds, …

Effect Of Steam Environment On Creep Behavior Of Nextel720/Alumina-Mullite Ceramic Matrix Composite At Elevated Temperature, Tolga Kutsal

Theses and Dissertations

The tensile creep behavior of an oxide-oxide ceramic matrix composite (CMC) was investigated at 1000 and 1100° C in laboratory air and steam. The oxide-oxide CMC studied in this research was Nextel™ 720/alumina-mullite (N720/AM). The composite consists of N720/fibers with 0°/90° fiber orientation and a porous alumina-mullite matrix. Tensile-strain behavior was investigated and tensile properties measured at 900, 1000 and 1100° C. The effect of loading rate on tensile properties of N720/AM ceramic matrix composite at 1100° C in steam was also examined. Creep-rupture tests were performed at 1100° C in laboratory air and steam, and at 1000° C only …

A Finite Element Evaluation Of An Experiment Related To Coating Damping Properties, Armando Deleon

Theses and Dissertations

Typically turbine engine blades gain protection from thermal damage by the use of hard coatings, such as magnesium aluminate spinel. Known as Thermal Barrier Coatings (TBC's), they have material properties that include several nonlinearities. These TBC's create damping primarily due to their nonlinear dissipation of energy. In order to effectively represent their damping properties, it is necessary to create a method which combines experimentation and analysis. Previous work has shown the need for a beam bounded and loaded in such a fashion that external support energy dissipation functions i.e. boundary conditions and aerodynamics are eliminated. Thus, a new experimental apparatus …

Effects Of Prior Aging At 316°C In Argon On Inelastic Deformation Behavior Of Pmr-15 Polymer At 316°C: Experiment And Modeling, Ozgur Ozmen

Theses and Dissertations

The inelastic deformation behavior of PMR-15 neat resin, a high-temperature polymer, was investigated at 316 deg C. The experimental program was designed to explore the influence of strain rate on tensile loading, unloading, and strain recovery behaviors. In addition, the effect of the prior strain rate on the relaxation response of the material, as well as on the creep behavior following strain controlled loading were examined. The material exhibits positive, nonlinear strain rate sensitivity in monotonic loading and unloading. Early failures occur in the inelastic regime. The recovery of strain at zero stress and creep response are strongly affected by …

Thermomechanical Properties Of Center-Reinforced Aluminum, Geofrey S. Cox

Theses and Dissertations

The rule of mixture approach was shown to produce an accurate theoretical prediction of the room temperature elastic modulus values when compared to the experimental results. The laminate's modulus value remained relatively constant over the -55C to 80C temperature range, indicating stable behavior despite temperature changes. Blunt notch tests also revealed that the laminate's strength was not significantly reduced due to the presence of small holes. Finally, fatigue testing demonstrated that the laminate retains its stiffness properties throughout its fatigue life, until failure.