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Articles 31 - 60 of 84
Full-Text Articles in Engineering Science and Materials
Aqueous Fabrication Of Pristine And Oxide Coated Znse Nanoparticles, Nicholas L. Van Zandt
Aqueous Fabrication Of Pristine And Oxide Coated Znse Nanoparticles, Nicholas L. Van Zandt
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Semiconducting nanoparticles have received significant attention due to their unique optoelectronic properties. Quantum dots (QDs), a class of spherical nanoparticles, possess a size-dependent bandgap and photoluminescence at visible wavelengths. QDs have many applications including biological labelling, solar cells, chemical impurity detection, and optical glasses. Doping QDs into optical glasses is highly desirable. High-quality QDs can be synthesized via liquid solution methods. However, solution-synthesized QDs often degrade over time and they cannot survive incorporation into a glass melt without protection. In this work, the aqueous synthesis of ZnSe QDs and coating with nanometer silica and alumina protective shells are investigated. The …
The Thermal And Mechanical Characteristics Of Lithiated Peo Lagp Composite Electrolytes, Jacob Michael Denney
The Thermal And Mechanical Characteristics Of Lithiated Peo Lagp Composite Electrolytes, Jacob Michael Denney
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Lithium-ion batteries are part of a multibillion-dollar industry that strives to meet the demands for an increasingly advanced technological future. Flexible batteries can be easily adapted from emerging novel wearable electronics to electrical vehicles and advanced solar panels. Solid-state batteries can greatly reduce the risk of fire or leaking hazardous materials due to puncture. For the development of solid-state flexible lithium based batteries polymer-ceramic composites are attractive electrolyte candidates because of their combined properties, such as electrical, thermal and mechanical properties, that not only overcome limitations from the base materials but may also render some enhanced performances resulting from the …
A Numerical Simulation On The Airfoil S833 Equipped With Flapping Trailing Edge Fringes, H. Yu, Zifeng Yang
A Numerical Simulation On The Airfoil S833 Equipped With Flapping Trailing Edge Fringes, H. Yu, Zifeng Yang
Mechanical and Materials Engineering Faculty Publications
Design optimization has been increasingly investigated for an airfoil, aiming to reduce the vorticity in the wake and increase the aerodynamic performance. In the current work, a two-dimensional (2D) S833 airfoil equipped with a flapping fringe at the trailing edge has been studied using computational fluid dynamics (CFD) simulations. The objective is to investigate the influence of the length (Lf) and flapping frequency (f) of the fringe on shedding vortices from the airfoil and the drag and lift coefficients. The validation of the current numerical approach for both static and dynamic motions of the airfoil was conducted. First, four different …
Ab Initio Modeling Of An Electron Transport Layer Interface In Hybrid Perovskite Solar Cells, Krantikumar Subhash Pawar
Ab Initio Modeling Of An Electron Transport Layer Interface In Hybrid Perovskite Solar Cells, Krantikumar Subhash Pawar
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Hybrid organic-inorganic perovskite solar cell is an emerging technology which has shown the fastest advancement in power conversion efficiency within a few years since introduction, thus making it one of the clean energy breakthroughs. These cells are based on thin-film technology which makes them suitable to manufacture using low-cost solution processing methods. As these types of cells are easily tunable with the selection of different materials, interfacial engineering is an important approach to increasing their efficiency. One of the main hurdles in this regard is the loss caused by the recombination of separated charges. An approach to tackle these issues …
Metal Coupon Testing In An Axial Rotating Detonation Engine For Wear Characterization, Gary S. North
Metal Coupon Testing In An Axial Rotating Detonation Engine For Wear Characterization, Gary S. North
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Rotating Detonation Engines (RDE) are being explored as a possible way to get better fuel efficiency for turbine engines than is otherwise possible. The walls of the RDE are subjected to cyclic thermal and mechanical shock loading at rates of approximately 3 KHz, with gas temperatures as high as 2976 K. This project performed testing with Inconel 625 and 304 stainless steel coupons in an RDE outer body to attempt to measure material ablation rates. Significant microstructural changes were observed to include grain growth in both alloys, carbide formation and grain boundary melting in Inconel, and formation of delta ferrite …
Stabilization Of Β-Cristobalite In The Sio2-Alpo4-Bpo4 System, Kathryn Doyle
Stabilization Of Β-Cristobalite In The Sio2-Alpo4-Bpo4 System, Kathryn Doyle
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Fused silica (silica glass) is transparent in the optical and near-infrared and has a low dielectric constant, making it suitable as a window material for radio frequency radiation. However, at high temperatures (>1100C), fused silica will easily creep and lose dimensional stability. Crystallized silica is much more creep resistant than fused silica. Silica crystallizes to many different structures including quartz, tridymite, and α- and β cristobalite. The only cubic polymorph, which is suitable for both optical and radio frequency transmission in polycrystalline form, is β -cristobalite. Unfortunately, this polymorph transforms to α-cristobalite at ~300C, and the volume change during …
Growth Of Two-Dimensional Molybdenum Disulfide Via Chemical Vapor Deposition, Zachary Durnell Ganger
Growth Of Two-Dimensional Molybdenum Disulfide Via Chemical Vapor Deposition, Zachary Durnell Ganger
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Graphene has successfully been a 2D material applied in various fields, but it is not the most appropriate candidate for many electronic devices unless its bandgap structure is tuned through functionalization. Among all other 2D material families, transition metal dichalcogenides (TMDs), represented by molybdenum disulfide (MoS2), are promising and emerging in power electronics due to their large direct bandgap and other electronic properties. 2D MoS2 has been fabricated through different approaches such as mechanical exfoliation, chemical etching, and chemical vapor deposition (CVD). The current major challenge in fabricating 2D MoS2 films is to produce a high-quality large-area monolayer film at …
Hierarchical Carbon Structures With Vertically- Aligned Nanotube Carpets For Oil-Water Separation Under Different Conditions, Kimia Kiaei
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The primary purpose of this study is to investigate the role of surface nano-structuring in fluid separation. It is hypothesized that hierarchical carbon structures consisting of aligned carbon nanotube arrays strongly adhered to the surface of porous carbon solids such as fabric and foam, can be used for separation of polar and non-polar fluids by selective wettability of one fluid and rejection of another. The vertically-aligned carbon nanotube arrays, as synthesized, possess super hydrophobicity demonstrated by high water contact angle on their surfaces. On the other hand, they are incredibly oleophilic, showing a high affinity to adsorb oil. These properties …
Multi-Sensor Approach To Determine The Effect Of Geometry On Microstructure In Additive Manufacturing, Joseph R. Walker
Multi-Sensor Approach To Determine The Effect Of Geometry On Microstructure In Additive Manufacturing, Joseph R. Walker
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Laser powder bed fusion (LPBF) is an additive manufacturing technique used for making complex parts through a layer-by-layer process with fine feature resolution. However, the layer-by-layer process, with complex scanning patterns within each layer, introduces variability in thermal behavior leading to inconsistent microstructure and defects. The in- situ process monitoring approach in this work uses sensors including a high-speed visible camera, thermal camera, and spectrometer to evaluate each location in the LPBF process. Each sensor focuses on a different process phenomenon such as the melt pool or thermal behavior. An experimental study, using metallographic analysis and collection of sensor data, …
Deposition Of Nanoparticles Or Thin Films Via Magnetron Sputtering Towards Graphene Surface Functionalization And Device Fabrication, Bridget Jul Larson
Deposition Of Nanoparticles Or Thin Films Via Magnetron Sputtering Towards Graphene Surface Functionalization And Device Fabrication, Bridget Jul Larson
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Graphene, a 2-dimensional single layer of carbon, has high carrier mobility, strength and electrical conductivity. Due to the absence of a band gap and chemical reactivity, pristine graphene has less competitiveness in semiconductors and sensors. Functionalizing graphene is imperative in the development of advanced applications. Among various wet chemical or physical vapor deposition, magnetron sputtering is cost-effective, minimum maintenance, user-friendly, and can be used to rapidly deposit nano-particulates or thin films with less contaminations on any substrates surface. This study is to investigate the morphology evolution of the deposited films using magnetron sputtering and to find appropriate conditions for nanoparticulate …
Preparation And Characterization Of Porous Pdms For Printed Electronics, Eyad Khalid M. Balbaid
Preparation And Characterization Of Porous Pdms For Printed Electronics, Eyad Khalid M. Balbaid
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Fabricating an elastomeric substrate with internal features could provide a novel structure with distinctive mechanical properties that allow them to stretch, bend and absorb the impact force. To date, polydimethylsiloxane (PDMS) is a great candidate as a substrate for flexible electronic applications, due to easy fabrication, high stability and low cost. In the current thesis, porous PDMS samples are fabricated and characterized based on the particle size and the fusion of salt and sugar treated micro-regions. The liquid PDMS is prepared by mixing the silicon elastomer base (Sylgard 184) and elastomer curing agent using volume ration 10:1. The salt and …
In Situ Defect Detection Using Three Color Spectroscopy In Laser Powder Bed Additive Manufacturing, Andrew Drieling
In Situ Defect Detection Using Three Color Spectroscopy In Laser Powder Bed Additive Manufacturing, Andrew Drieling
The University Honors Program
Additive Manufacturing (AM) provides a way to create parts that would be extremely difficult or impossible with conventional manufacturing processes. However, AM also introduces defects, which are detrimental to the mechanical performance. These defects are potentially unknown until post-processing inspection and testing, wasting time and resources on an unusable part or initiating unexpected failure. Historically, spectroscopy has successfully been used for in situ monitoring of laser welding, using changing parameters in the generated plume to predict defects. In situ monitoring using a visible spectrometer for fabrication of Alloy 718 on a test bed laser powder bed fusion system is performed. …
Electronic And Crystalline Characteristics Of Mixed Metal Halide Perovskite Semiconductor Films, Patrick Joseph Cleaver
Electronic And Crystalline Characteristics Of Mixed Metal Halide Perovskite Semiconductor Films, Patrick Joseph Cleaver
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Solar technology has a long history of incremental improvements in cost, reliability and efficiency. However, solar cells based on lead halide perovskite films have made more rapid leaps forward in the past 10 years, making it the fastest growing solar technology in terms of efficiency. Leaders in academia and industry continue to find success in overcoming manufacturability and stability issues, but have not yet discovered a high-efficiency perovskite film without the use of toxic lead. Probing less toxic analogs to the highly efficient lead halide, a series of thin films with perovskite structures, i.e. A2BB’X6 where A = Cs or …
Microstructural Characterization Of LensTm Ti-6al-4v: Investigating The Effects Of Process Variables Across Multiple Deposit Geometries, Laura Christine Davidson
Microstructural Characterization Of LensTm Ti-6al-4v: Investigating The Effects Of Process Variables Across Multiple Deposit Geometries, Laura Christine Davidson
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Laser based additive manufacturing of Ti-6Al-4V components is under consideration for aerospace applications. The mechanical properties of the finished components depend on their microstructure. Process mapping compares process variables such as heat source power, heat source travel speed, material feed rate, part preheat temperature and feature geometry to process outcomes such as microstructure, melt pool geometry and residual stresses. In this work, the microstructure of two-dimensional pads, multilayer pads, thin walls, and structural components at the steady state location was observed. A method for measuring β grain widths that allows for the calculation of standard deviations, confidence intervals, and variances …
Defect Engineering: Novel Strengthening Mechanism For Low- Dimensional Zinc Oxide Nanostructures, Seyed Emad Rezaei
Defect Engineering: Novel Strengthening Mechanism For Low- Dimensional Zinc Oxide Nanostructures, Seyed Emad Rezaei
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The advent of nanomaterials has opened a new avenue for designing and fabricating materials with unique properties, e.g., superior mechanical properties. Based on a common notion, the perfect structures are assumed to exhibit better mechanical properties, such as higher yield strength and Young's modulus. Therefore, researchers have devoted an extensive amount of time to decrease defect concentration by fabricating materials with the micro/nanoscale, e.g., nanowires (NWs) and nanobelts (NBs), to enhance the mechanical characteristics of the system. However, defects are a part of the fabrication process and precise control over synthesizing procedure is needed to eliminate them from the material. …
Functionalization And Characterization Of Chemical Vapor Deposited Graphene Sheets Towards Application In Chemical Vapor Sensing, Nicholas Alexander Engel
Functionalization And Characterization Of Chemical Vapor Deposited Graphene Sheets Towards Application In Chemical Vapor Sensing, Nicholas Alexander Engel
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Chemical/biological sensors serve many purposes in protecting machinery, the environment, and human life/wellness. Graphene, a two-dimensional (2-D) material made up of carbon atoms in a honeycomb-like lattice, is promising for applications to chemical/biological sensing due to its unique properties. Functionalization of graphene by surface decorating with nanoparticles and increasing interior adsorption sites can tailor its catalytic activity and electrical properties, and hence, important for detecting and distinguishing trace hazardous gases. This research introduces two different approaches to functionalize graphene towards enhanced sensitivity and selectivity of graphene-based sensors. The morphologies, structures, and electrical properties of the functionalized graphene are systematically characterized. …
Optical Flow Method For Blood Flow Velocimetry Based On Digital X-Ray Subtraction Angiography: A Brief Review, Zifeng Yang
Optical Flow Method For Blood Flow Velocimetry Based On Digital X-Ray Subtraction Angiography: A Brief Review, Zifeng Yang
Mechanical and Materials Engineering Faculty Publications
Detailed blood flow information has been recognized as the key information for diagnosis of vascular diseases, such as vascular stenosis and aneurysms. Optical flow method (OFM) is an emergent technique as a tool to analyze the digital x-ray subtraction angiographic images of blood vessels to obtain the detailed blood flow distribution in vascular systems. A brief review isconstructed to discuss the status, applicability, accuracy and future direction of the optical flow technique in the physical study of vascular flow.
Tracking Characteristics Of Tracer Particles For Piv Measurements In Supersonic Flows, Fang Chen, Hong Liu, Zifeng Yang, Hui Hu
Tracking Characteristics Of Tracer Particles For Piv Measurements In Supersonic Flows, Fang Chen, Hong Liu, Zifeng Yang, Hui Hu
Mechanical and Materials Engineering Faculty Publications
The tracking characteristics of tracer particles for particle image velocimetry (PIV) measurements in supersonic flows were investigated. The experimental tests were conducted at Mach number 4 in Multi-Mach Wind Tunnel (MMWT) of Shanghai Jiao Tong University. The motion of tracer particles carried by the supersonic flow across shockwaves was theoretically modelled, and then their aerodynamic characteristics with compressibility and rarefaction effects were evaluated. According to the proposed selection criterion of tracer particles, the PIV measured results clearly identified that the shockwave amplitude is in good agreement with theory and Schlieren visualizations. For the tracer particles in nanoscales, their effective aerodynamic …
Friction Stir Welding Between Similar And Dissimilar Materials, Khaled Yousif Ali
Friction Stir Welding Between Similar And Dissimilar Materials, Khaled Yousif Ali
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This thesis focuses on the friction stir welding (FSW) between similar and dissimilar alloys. FSW is a solid state joining process that welds the work-pieces through a combination of heat generated by friction and mechanical stirring of the metals in the region of the joint. Being a solid state process, FSW can be used to weld alloys with significantly different melting points. This provides a significant benefit over traditional fusion welding process in a variety of applications in automotive, biomedical, aerospace, nuclear and petroleum industries. Two materials - an aluminum alloy (6061-T6, m.p. 582 - 652°C) and a steel (SAE …
Processing Of Ultra-Thin Film Of Un Modified C60 Fullerene Using The Langmuir-Blodgett Technique. Effect Of Structure On Stiffness And Optoelectric Properties, Hasanain Basim Altalebi
Processing Of Ultra-Thin Film Of Un Modified C60 Fullerene Using The Langmuir-Blodgett Technique. Effect Of Structure On Stiffness And Optoelectric Properties, Hasanain Basim Altalebi
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Monolayer films of C60 fullerene were for the first time produced successfully by using the Langmuir-Blodgett technique. The processing parameters were optimized and the structure of these films has been investigated using Scanning Tunneling Microscopy (STM) and Atomic Force Microscopy (AFM). Film stiffness was measured to be in the range of 15 MPa to 32 MPa depending on the nature of the solvent used to process the films. Optical transparency and electrical performance have been measured and correlated to the film structure. While 100% transparent, the film measured conductivity was in the range of 1013 S/m, that is orders of …
An Experimental Investigation Of Residual Stress Development During Selective Laser Melting Of Ti-6al-4v, Nathan Charles Levkulich
An Experimental Investigation Of Residual Stress Development During Selective Laser Melting Of Ti-6al-4v, Nathan Charles Levkulich
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Selective laser melting (SLM) is an additive manufacturing (AM) process that gives rise to large thermal gradients and rapid cooling rates that lead to the development of undesirable residual stress and distortion. In this work, a number of different techniques (i.e., x-ray-diffraction, hole-drilling, layer-removal, and contour) were utilized to establish the effect of process parameters on residual stress development during SLM of Ti-6Al-4V. The measurements indicated that higher laser power, slower scan speed, smaller stripe width, reduced substrate overhang, and reduced build plan area each reduce the level of residual stress. In addition, the correlation between microstructure, crystallographic texture, and …
Studies Of Ionic Liquid Hybrids: Characteristics And Their Potential Application To Li-Ion Batteries And Li-Ion Capacitors, Mengxin Liu
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Ionic liquids (ILs) have attracted much attention in electrochemical energy storage systems for their advantageous properties over traditional lithium salt/carbonate solvent electrolyte in terms of higher electrochemical potential windows, comparable ionic conductivity, negative vapor pressure and non-flammability. Ionic liquids can be used as the solvent-free electrolyte in electrochemical double layer capacitors (EDLCs) or can act as the important additives to the carbonate electrolyte in lithium ion batteries (LIBs). Recently, lithium ion capacitors (LICs) have emerge as a novel energy storage system to satisfy the demands for higher energy density and higher power density in portable and transportation systems. This Master …
Synthesis And Characterizations Of Lithium Aluminum Titanium Phosphate (Li1+Xalxti2-X(Po4)3) Solid Electrolytes For All-Solid-State Li-Ion Batteries, Jianping Yang
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New-generation low-emission transportation systems demand high-performance lithium ion (Li-ion) batteries with high safety insurance at broad operable temperatures. Highly conductive solid electrolyte is one of the key components for such applications. The objective of this thesis is to synthesize and characterize aluminum doped lithium titanium phosphate, i.e. Li1+xAlxTi2-x(PO4)3 (LATP), one of the solid-state electrolytes for potential applications to all solid-state lithium-ion batteries. In this research, sol-gel method and one step solid-state reaction approaches were explored and critical processes were optimized towards maximizing lithium ion conductivities at room temperature. The impacts of the processing conditions on the structures, morphologies, compositions of …
Investigation Of Residual Stresses In Melt Infiltrated Sic/Sic Ceramic Matrix Composites Using Raman Spectroscopy, Kaitlin Noelle Kollins
Investigation Of Residual Stresses In Melt Infiltrated Sic/Sic Ceramic Matrix Composites Using Raman Spectroscopy, Kaitlin Noelle Kollins
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Ceramic matric composites (CMCs) are being developed for use in extreme operating conditions. Specifically, there is interest to replace superalloys with Silicon Carbide/Silicon Carbide (SiC/SiC) CMCs in the hot section of gas turbine engines because of their lower densities, high temperature performance, and oxidation resistance. Residual stresses in SiC/SiC CMCs are a direct result of the high temperature processing conditions, a mismatch in the coefficients of thermal expansion between composite constituents, and silicon crystallization expansion upon cooldown. Understanding the residual stress state and magnitudes of these stresses will enable better prediction of behavior and life performance in application environments. This …
Experimental Investigation On Flow Characteristics Of A Four-Wing Micro Air Vehicle, Lisong Shi, Chunkit Uy, Shih K. Huang, Zifeng Yang, George P.G. Huang, Chihyung Wen
Experimental Investigation On Flow Characteristics Of A Four-Wing Micro Air Vehicle, Lisong Shi, Chunkit Uy, Shih K. Huang, Zifeng Yang, George P.G. Huang, Chihyung Wen
Mechanical and Materials Engineering Faculty Publications
The aim of current research work on micro air vehicles is to realize their autonomous control, i.e. building a library for a lookup table that would apply to micro electronics. In doing so, comprehensive flight tests need to be carried out. In this study, a four-wing flapping MAV is built and a multi-discipline approach is used to design the MAV model. Precision manufacturing technology is introduced here. The finished micro air vehicle has a weight of 8 g and is tested for flight by remote control. The micro air vehicle can perform both hovering and forward flight with high maneuverability. …
Quantifying Amorphous Content Of Commercially Available Silicon Carbide Fibers, Ian Mark Wolford
Quantifying Amorphous Content Of Commercially Available Silicon Carbide Fibers, Ian Mark Wolford
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SiC/SiC ceramic matrix composites (CMCs) with potential applications at =2700°F (1482°C) are of significant interest to the Air Force. The high temperature performance of SiC fibers used within these composites is greatly affected by the presence of amorphous SiOC and free carbon in the fibers. Therefore quantification of this non SiC material in commercially available SiC fibers is extremely important. In this work Hi Nicalon, Hi-Nicalon Type-S, Tyranno-SA3, Cef-NITE, and Sylramic SiC fibers were studied. Changes in mass, grain size, and amorphous content were measured as a function of processing temperature and time. The amorphous material in each fiber was …
Computational Fluid Dynamics Simulation Of Intracranial Aneurysms - Comparing Size And Shape, Zifeng Yang, Hongtao Yu, George P. Huang, Ryan Schwieterman, Bryan Ludwig
Computational Fluid Dynamics Simulation Of Intracranial Aneurysms - Comparing Size And Shape, Zifeng Yang, Hongtao Yu, George P. Huang, Ryan Schwieterman, Bryan Ludwig
Mechanical and Materials Engineering Faculty Publications
Objective: To study the hemodynamics of an anatomic internal carotid artery aneurysm derived from a patient-specific model and then manipulate into two phantom morphologies: one growing uniformly by size and the other changing shape unevenly. Methods: The computational model of the saccular, internal carotid artery, aneurysm was constructed from 3D rotational, digitally subtracted, catheter angiography images. Computational fluid dynamics simulations were performed under pulsatile cardiac flow conditions. Velocity vectors, streamlines, pressure, and wall shear stress (WSS) and its variance distributions were quantitatively visualized. Results: The maximum pressure and WSS from the time-averaged distribution on the inside saccular surface of the …
Experimental Validation Of The Calphad Approach Applied To Multi-Principle Element Alloys, Nathan J. Bryant
Experimental Validation Of The Calphad Approach Applied To Multi-Principle Element Alloys, Nathan J. Bryant
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High entropy alloys (HEAs) are a recent area of research in materials science. Their namesake is because their high entropy of mixing due to multiple metallic elements in a near equimolar ratio. The high entropy of mixing is supposed to suppress unwanted, brittle, ordered intermetallic phases, and form a single, randomly mixed solid solution phase. This phenomena makes HEAs a good candidate for structural applications. However, this entropy of mixing may not be enough to suppress all intermetallic phases. For this reason, the CALculation of PHAse Diagrams (CALPHAD) approach is being explored to predict phase equilibrium in HEAs. This study …
Numerical Study Of Crossflow Enhanced Microfiltration Of Oil-In-Water Emulsions, Nikolai Priezjev, Tohid Darvishzadeh, Volodymyr Tarabara
Numerical Study Of Crossflow Enhanced Microfiltration Of Oil-In-Water Emulsions, Nikolai Priezjev, Tohid Darvishzadeh, Volodymyr Tarabara
Mechanical and Materials Engineering Faculty Publications
No abstract provided.
Analysis Of Laser Induced Spallation Of Electron Beam Physical Vapor Deposited (Eb-Pvd) Thermal Barrier Coatings, David Allen Beeler
Analysis Of Laser Induced Spallation Of Electron Beam Physical Vapor Deposited (Eb-Pvd) Thermal Barrier Coatings, David Allen Beeler
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The use of thermal barrier coatings (TBCs) has been an important factor in the efficiency improvements of jet engines due to their ability to withstand the extreme environments within the engine. With this improved resistance, TBCs have also become more difficult to remove without damaging the substrate. Mound Laser & Photonics Center, Inc. (MLPC) has developed an innovative, laser based technique to spall this coating. The intention of this work was to investigate and better understand the removal mechanism. Through experimentation and analysis (such as high speed video, Scanning Electron Microscopy and Energy Dispersive Spectroscopy, semi-logarithmic analysis, and a numerical …