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Articles 121 - 123 of 123
Full-Text Articles in Chemical Engineering
Electrochemical Reduction Of Molybdenum(Vi) Compounds In Molten Lithium Chloride-Potassium Chloride Eutectic, Branko N. Popov, H. A. Laitinen
Electrochemical Reduction Of Molybdenum(Vi) Compounds In Molten Lithium Chloride-Potassium Chloride Eutectic, Branko N. Popov, H. A. Laitinen
Faculty Publications
Molybdenum (VI) oxide reacts with molten LiCl-KCl eutectic at 450° to form MoO2CI2, which probably is present as an anion MoO2Cl4=, and pyromolybdate, Mo2O7=. Both of these species are electrochemically reduced to MoO2, which can be reoxidized to MoO2Cl2 by current reversal. A second reduction step, observed whether MoO3 or Mo2O72− is added to the melt, can be attributed to the reduction of MoO4−−, formed as a secondary reaction product in the first …
Electrochemical Reduction Of Chromate In The Presence Of Nickel Chloride In Molten Lithium Chloride-Potassium Chloride Eutectic, Branko N. Popov, H. A. Laitinen
Electrochemical Reduction Of Chromate In The Presence Of Nickel Chloride In Molten Lithium Chloride-Potassium Chloride Eutectic, Branko N. Popov, H. A. Laitinen
Faculty Publications
Chronopotentiometry of chromate in the presence of NiCl2 in molten LiCl-KCl eutectic reveals a diffusion controlled, three electron reduction step. In the presence of excess NiCl2, chromate is reduced at −0.35V vs. Pt(II)/Pt reference electrode and the electroactive species responsible for the chrono-potentiometric wave is estimated to have a diffusion coefficient of 1.06 · 10−5 cm2 sec−1 at 450°C. The stoichiometry of the reduction product depends mainly on the temperature at which the deposit is formed. At 500°C the deposit approaches the composition LiNi2CrO4. X-ray powder diffraction shows the deposit …
Electrodeposition Of Cellulose And Carboxy-Methylcellulose, Charles Edward Driesens Jr.
Electrodeposition Of Cellulose And Carboxy-Methylcellulose, Charles Edward Driesens Jr.
Theses
The previous work done by Frank Cozzarelli on the eleotrodeposition of cellulose from a sodium zincate-urea-cellulose system has been verified, except that zinc was found to deposit on the cathode at all voltages and current densities within the range of the optimum conditions for deposition. The optimum conditions are: voltage - 1.10 to 1.28 volts; current density 0.13 to 1.10 amperes/square foot; electrode material - copper. Current efficiencies range from 0.80 to 5.53%.
A chelate-like complex formed from the sodium zincate and urea which couples with the cellulose has been proposed as a possible explaination of the mechanism governing the …