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Full-Text Articles in Engineering

Analysis Of Bombyx Mori Silk And Polyimide Nanofibers, Sabrina Leseul Nov 2023

Analysis Of Bombyx Mori Silk And Polyimide Nanofibers, Sabrina Leseul

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

This thesis presents a study on the properties of Bombyx Mori silk nanofibers and polyimide (PI) nanofibers. Firstly, a Bombyx Mori silk solution has been created with degummed silkworm cocoons in order to separate the fibroin and the sericin, the two main proteins of the silk. The fibroin was then centrifuged to remove insoluble particles and stored and 4°C before mixing with hexafluoroisopropanol (HFIP). On the second part, a polyimide solution, made with shavings of polyimide and N,N-dimethylformamide (DMF). Both solutions are then electrospun. Electrospinning parameters are studied. In this way, a part of my thesis has been dedicated to …


Characterization Of Ground Albedo Materials For Bifacial Solar Farms, Fernanda De Los Angeles Garcia, Benny Tam, Jean Lee, James Vance Oct 2023

Characterization Of Ground Albedo Materials For Bifacial Solar Farms, Fernanda De Los Angeles Garcia, Benny Tam, Jean Lee, James Vance

College of Engineering Summer Undergraduate Research Program

Bifacial photovoltaics can collect solar energy from both sides, unlike regular one-sided solar panels. With the ability to collect energy from both sides, the energy production of bifacial photovoltaic farms is about 2-6% more efficient than typical solar farms. However, the increase in efficiency is highly dependent on the reflectivity of the ground material. This project explores six different materials to determine which material would be best to implement as a ground material for a bifacial photovoltaic farm, based on their mechanical properties and albedo value. Albedo refers to the ratio between the reflected solar radiation to the incident solar …


A Strong And Ductile Cobalt-Free Solid-Solution Fe30ni30mn30cr10 Multi-Principal Element Alloy From Hot Rolling, Hans Pommerenke, Jiaqi Duan, Nathan Curtis, Victor Delibera, Adam Bratten, Andrew Hoffman, Mario F. Buchely, Ronald J. O'Malley, Haiming Wen Jul 2023

A Strong And Ductile Cobalt-Free Solid-Solution Fe30ni30mn30cr10 Multi-Principal Element Alloy From Hot Rolling, Hans Pommerenke, Jiaqi Duan, Nathan Curtis, Victor Delibera, Adam Bratten, Andrew Hoffman, Mario F. Buchely, Ronald J. O'Malley, Haiming Wen

Materials Science and Engineering Faculty Research & Creative Works

Most of the Face-Centered Cubic (FCC) Multi-Principal Element Alloys (MPEAs) Developed Thus Far Contain Cobalt. for Many Applications, it is Either required or Beneficial to Avoid Cobalt, Since Cobalt Has Long-Term Activation Issue (For Nuclear Applications), is Expensive, and is Considered a Critical Material. in Addition, FCC Structured Solid-Solution MPEAs Tend to Have Relatively Low Strength. a FCC Solid-Solution Fe30Ni30Mn30Cr10 (At %) MPEA Was Fabricated Via Arc Melting, Followed by Homogenization at 1100 °C for 12 H. the Alloy Was Hot Rolled at 1100 °C with a Total Reduction of Up to 97 %. the Microstructure Was Characterized and Mechanical …


Nanoclays‑Containing Bio‑Based Packaging Materials: Properties, Applications, Safety, And Regulatory Issues, Kalpani Y. Perera, Maille Hopkins, Amit K. Jaiswal Dr, Swarna Jaiswal Feb 2023

Nanoclays‑Containing Bio‑Based Packaging Materials: Properties, Applications, Safety, And Regulatory Issues, Kalpani Y. Perera, Maille Hopkins, Amit K. Jaiswal Dr, Swarna Jaiswal

Articles

Food packaging is an important concept for consumer satisfaction and the increased shelf life of food products. The introduction of novel food packaging materials has become an emerging trend in recent years, which could be mainly due to environmental pollution caused by plastic packaging and to reduce food waste. Recently, numerous studies have been carried out on nanoclays or nanolayered silicate to be used in packaging material development as reinforcing filler composites. Different types of nanoclays have been used as food packaging materials, while montmorillonite (MMT), halloysite, bentonite (BT), Cloisite, and organically modified nanoclays have become of great interest. The …


Mechanical Properties Of Zrb2 Ceramics Determined By Two Laboratories, Jeffrey J. Swab, Jecee Jarman, William Fahrenholtz, Jeremy Lee Watts Jan 2023

Mechanical Properties Of Zrb2 Ceramics Determined By Two Laboratories, Jeffrey J. Swab, Jecee Jarman, William Fahrenholtz, Jeremy Lee Watts

Materials Science and Engineering Faculty Research & Creative Works

The mechanical properties for zirconium diboride (ZrB2) were measured at two laboratories and compared. Two billets of ZrB2 were prepared by hot-pressing commercial powder. The relative densities of the billets were >99% and with an average grain size of 5.9 ± 4.5 µm. Both laboratories prepared American Society for Testing and Materials (ASTM) C1161 B-bars for strength and ASTM C1421 bars with notch configuration A for fracture toughness. Specimens were machined by diamond grinding at the Army Research Laboratory (ARL) and electrical discharge machining (EDM) at Missouri S&T. Strength bars tested at Missouri S&T were polished to a.25 μm finish …


Effect Of Mechanical Activation On Carbothermal Synthesis And Densification Of Zrc, Nina Obradović, Lun Feng, Suzana Filipović, Miljana Mirković, Darko Kosanović, Jelena Rogan, William Fahrenholtz Jan 2023

Effect Of Mechanical Activation On Carbothermal Synthesis And Densification Of Zrc, Nina Obradović, Lun Feng, Suzana Filipović, Miljana Mirković, Darko Kosanović, Jelena Rogan, William Fahrenholtz

Materials Science and Engineering Faculty Research & Creative Works

Zirconium carbide ceramics were prepared by carbothermal reduction of ZrO2 and C that were mixed by high-energy ball milling. Powders were milled for times from 0 to 120 min in air. As milling time increased, the surface area of the powders increased, indicating significant particle size reduction. Milled powders were reacted at 1600 °C and then densified by spark plasma sintering at 2000 °C, which was sufficient to convert the starting powders to zirconium carbide. Unmilled powders did not reach full density. Milled powders reached full density, but ZrO2 impurities were found for specimens prepared from powders milled …


Strength Retention Of Single-Phase High-Entropy Diboride Ceramics Up To 2000°C, Lun Feng, William Fahrenholtz, Gregory E. Hilmas, Yue Zhou, Jincheng Bai Jan 2023

Strength Retention Of Single-Phase High-Entropy Diboride Ceramics Up To 2000°C, Lun Feng, William Fahrenholtz, Gregory E. Hilmas, Yue Zhou, Jincheng Bai

Materials Science and Engineering Faculty Research & Creative Works

The mechanical properties of single-phase (Hf0.2,Nb0.2,Ta0.2,Ti0.2,Zr0.2)B2 ceramics with high purity were investigated. The resulting ceramics had relative density greater than 99%, and an average grain size of 4.3 ± 1.6 μm. At room temperature (RT), the Vickers hardness was 25.2 ± 0.6 GPa at a load of 0.49 N, Young's modulus was 551 ± 7 GPa, fracture toughness was 4.5 ± 0.4 MPa m1/2, and flexural strength was 507 ± 10 MPa. Flexural strength increased by more than 50% from 507 ± 10 MPa at RT to 776 ± …


Processing And Mechanical Properties Of Hot-Pressed Zirconium Diboride – Zirconium Carbide Ceramics, Eric W. Neuman, William Fahrenholtz, Gregory E. Hilmas Sep 2022

Processing And Mechanical Properties Of Hot-Pressed Zirconium Diboride – Zirconium Carbide Ceramics, Eric W. Neuman, William Fahrenholtz, Gregory E. Hilmas

Materials Science and Engineering Faculty Research & Creative Works

ZrB2 was mixed with 0.5 wt% carbon and up to 10 vol% ZrC and densified by hot-pressing at 2000 °C. All compositions were > 99.8% dense following hot-pressing. The dense ceramics contained 1–1.5 vol% less ZrC than the nominal ZrC addition and had between 0.5 and 1 vol% residual carbon. Grain sizes for the ZrB2 phase decreased from 10.1 µm for 2.5 vol% ZrC to 4.2 µm for 10 vol% ZrC, while the ZrC cluster size increased from 1.3 µm to 2.2 µm over the same composition range. Elastic modulus was ~505 GPa and toughness was ~2.6 MPa·m½ for all compositions. …


Room-Temperature Mechanical Properties Of A High-Entropy Diboride, Alec C. Murchie, Jeremy Lee Watts, William Fahrenholtz, Gregory E. Hilmas Jul 2022

Room-Temperature Mechanical Properties Of A High-Entropy Diboride, Alec C. Murchie, Jeremy Lee Watts, William Fahrenholtz, Gregory E. Hilmas

Materials Science and Engineering Faculty Research & Creative Works

The mechanical properties of a (Hf,Mo,Nb,Ta,W,Zr)B2 high-entropy ceramic were measured at room temperature. A two-step synthesis process was utilized to produce the (Hf,Mo,Nb,Ta,W,Zr)B2 ceramics. The process consisted of a boro/carbothermal reduction reaction followed by solid solution formation and densification through spark plasma sintering. Nominally, phase pure (Hf,Mo,Nb,Ta,W,Zr)B2 was sintered to near full density (8.98 g/cm3) at 2000°C. The mean grain size was 6 ± 2 µm with a maximum grain size of 17 µm. Flexural strength was 528 ± 53 MPa, Young's modulus was 520 ± 12 GPa, fracture toughness was 3.9 ± 1.2 MPa·m1/2, and hardness (HV0.2) was 33.1 …


The Effect Of Green Biobased Binder On Structural, Mechanical, Liquid Absorption And Wetting Properties Of Coated Papers, Bilge N. Altay, Charles Klass, Ting Chen, Alexandar Fleck, Cem Aydemir, Arif Karademir, Paul D. Fleming Dec 2021

The Effect Of Green Biobased Binder On Structural, Mechanical, Liquid Absorption And Wetting Properties Of Coated Papers, Bilge N. Altay, Charles Klass, Ting Chen, Alexandar Fleck, Cem Aydemir, Arif Karademir, Paul D. Fleming

Articles

Synthetic styrene-butadiene (SB) and styrene-acrylic (SA) latex binders used in paper coating formulations are common and based on unsustainable petroleum sources. Today's papermaking industry turns towards sustainable substitutes that do not compromise quality, and reduce carbon emission, toxic substance release and waste disposal concerns related to fossil fuel sources. In this study, colloidal starch-based latex nanoparticles that do not require cooking were used for pigment coating and coated on the paper surfaces. The effects of these new biobased binders on the structural and mechanical strength properties, liquid absorption, wetting and surface topography of the paper were investigated and compared with …


Enhancement Of Asphalt Performance By Graphene-Based Bitumen Nanocomposites, Sara Moghtadernejad, Ehsan Barjasteh, Ren Nagata, Haia Malabeh Jun 2021

Enhancement Of Asphalt Performance By Graphene-Based Bitumen Nanocomposites, Sara Moghtadernejad, Ehsan Barjasteh, Ren Nagata, Haia Malabeh

Mineta Transportation Institute Publications

As the State of California continues to grow, demand for enhanced infrastructure such as roadways and highways escalates. In view of the current average highway lifespan of 15–20 years, the improvement of asphalt binders leads to material sustainability by decreasing required maintenance and increasing the lifespan of roadways. In the present investigation, enhancement of asphalt binder properties was achieved by different methods of mixing varying compositions of graphene nanoparticles with an SBS polymer and asphalt binder. Additionally, experimental evaluation and comparison of the rheological and mechanical properties of each specimen is presented. Graphene nanoparticles have attracted great curiosity in the …


Microstructure Evolution And Mechanical Property Response Of Tc11 Titanium Alloy Under Electroshock Treatment, Chang Liu, Lechun Xie, Dongsheng Qian, Lin Hua, Liqiang Wang, Lai-Chang Zhang Jan 2021

Microstructure Evolution And Mechanical Property Response Of Tc11 Titanium Alloy Under Electroshock Treatment, Chang Liu, Lechun Xie, Dongsheng Qian, Lin Hua, Liqiang Wang, Lai-Chang Zhang

Research outputs 2014 to 2021

© 2020 The Authors This work investigated the effects of electroshock treatment (EST) on the microstructure variation and mechanical properties of TC11 alloy. The average hardness of the specimens decreased from 358 HV to 328 HV after EST of 0.04 s, then increased to 396 HV after EST of 0.06 s. After EST, the yield strength of specimen declined from 959 MPa to 797 MPa after EST of 0.04 s, and then increased to 1265 MPa after EST of 0.06 s, but the fracture strain decreased continuously. The variation in mechanical properties was closely related to the phase transition from …


Properties And Performance Of The Basalt-Fiber Reinforced Texture Roof Tiles, Parinya Chakartnarodom, Wichit Prakaypan, Pitcharat Ineure, Nutthita Chuankrerkkul, Edward A. Laitila, Nuntaporn Kongkajun Dec 2020

Properties And Performance Of The Basalt-Fiber Reinforced Texture Roof Tiles, Parinya Chakartnarodom, Wichit Prakaypan, Pitcharat Ineure, Nutthita Chuankrerkkul, Edward A. Laitila, Nuntaporn Kongkajun

Michigan Tech Publications

The mechanical and the physical properties, and the performance of texture roof tiles reinforced with the basalt fibers were observed. The samples of the basalt-fiber reinforced texture roof tiles were produced on the industrial scale by using filter pressing method. After forming, the as-molded samples were air cured and characterized based on ASTM C1185 standard for their mechanical properties and physical properties. In addition, the roof-tile installation test was also performed. The results showed that the samples of the basalt-fiber reinforced texture roof tile (BFRT) could be produced on the industrial scale by using the common setting of the forming …


Aerosol Jet Printed Capacitive Strain Gauge For Soft Structural Materials, Kiyo T. Fujimoto, Jennifer K. Watkins, Timothy Phero, Takoda Bingham, Kshama Lakshmi Ranganatha, Benjamin C. Johnson, Zhangxian Deng, Brian Jaques, David Estrada Nov 2020

Aerosol Jet Printed Capacitive Strain Gauge For Soft Structural Materials, Kiyo T. Fujimoto, Jennifer K. Watkins, Timothy Phero, Takoda Bingham, Kshama Lakshmi Ranganatha, Benjamin C. Johnson, Zhangxian Deng, Brian Jaques, David Estrada

Materials Science and Engineering Faculty Publications and Presentations

Soft structural textiles, or softgoods, are used within the space industry for inflatable habitats, parachutes and decelerator systems. Evaluating the safety and structural integrity of these systems occurs through structural health monitoring systems (SHM), which integrate non-invasive/non-destructive testing methods to detect, diagnose, and locate damage. Strain/load monitoring of these systems is limited while utilizing traditional strain gauges as these gauges are typically stiff, operate at low temperatures, and fail when subjected to high strain that is a result of high loading classifying them as unsuitable for SHM of soft structural textiles. For this work, a capacitance based strain gauge (CSG) …


Boron Nitride Nanotube Based Lightweight Metal Matrix Composites: Microstructure Engineering And Stress-Transfer Mechanics, Pranjal Nautiyal Jun 2020

Boron Nitride Nanotube Based Lightweight Metal Matrix Composites: Microstructure Engineering And Stress-Transfer Mechanics, Pranjal Nautiyal

FIU Electronic Theses and Dissertations

Lightweight metals, such as Aluminum, Magnesium and Titanium, are receiving widespread attention for manufacturing agile structures. However, the mechanical strength of these metals and their alloys fall short of structural steels, curtailing their applicability in engineering applications where superior load-bearing ability is required. There is a need to effectively augment the deformation- and failure-resistance of these metals without compromising their density advantage.

This dissertation explores the mechanical reinforcement of the aforementioned lightweight metal matrices by utilizing Boron Nitride Nanotube (BNNT), a 1D nanomaterial with extraordinary mechanical properties. The nanotubes are found to resist thermo-oxidative transformations up to ~750°C, establishing their …


Aging Response And Precipitation Behavior After 5% Pre-Deformation Of An Al-Mg-Si-Cu Alloy, Shuoxun Jin, Tungwai Ngai, Liejun Li, Shian Jia, Tongguang Zhai, Dongjie Ke Aug 2018

Aging Response And Precipitation Behavior After 5% Pre-Deformation Of An Al-Mg-Si-Cu Alloy, Shuoxun Jin, Tungwai Ngai, Liejun Li, Shian Jia, Tongguang Zhai, Dongjie Ke

Chemical and Materials Engineering Faculty Publications

In this study, Al-1.00 Mg-0.65 Si-0.24 Cu alloy was solution heat-treated, water-quenched, and then pre-deformed for 5% before aging. The peak hardness and yield strength of the pre-deformed sample with subsequent artificial aging were similar to that of a T6 condition sample. It was also found that the pre-deformation treatment could inhibit the negative influence of natural aging to some degree. After seven days of natural aging, the pre-deformed sample obtained better peak hardness and yield strength upon artificial aging than the sample without pre-deformation. In addition, the pre-deformation treatment could reduce 50% of the artificial aging time to reach …


Mechanical Characterization Of Parts Produced By Ceramic On‐Demand Extrusion Process, Amir Ghazanfari, Wenbin Li, Ming Leu, Gregory Hilmas Jan 2017

Mechanical Characterization Of Parts Produced By Ceramic On‐Demand Extrusion Process, Amir Ghazanfari, Wenbin Li, Ming Leu, Gregory Hilmas

Faculty Publications, Mechanical Engineering

Ceramic On‐Demand Extrusion (CODE) is an additive manufacturing process recently developed to produce dense three‐dimensional ceramic components. In this paper, the properties of parts produced using this freeform extrusion fabrication process are described. High solids loading (~60 vol%) alumina paste was prepared to fabricate parts and standard test methods were employed to examine their properties including the density, strength, Young's modulus, Weibull modulus, toughness, and hardness. Microstructural evaluation was also performed to measure the grain size and critical flaw size. The results indicate that the properties of parts surpass most other ceramic additive manufacturing processes and match conventional fabrication techniques.


Equiaxed Ti-Based Composites With High Strength And Large Plasticity Prepared By Sintering And Crystallizing Amorphous Powder, Lehua Liu, Chao Yang, L. M. Kang, Yan Long, Zhiyu Xiao, Peijie Li, Laichang Zhang Jan 2016

Equiaxed Ti-Based Composites With High Strength And Large Plasticity Prepared By Sintering And Crystallizing Amorphous Powder, Lehua Liu, Chao Yang, L. M. Kang, Yan Long, Zhiyu Xiao, Peijie Li, Laichang Zhang

Research outputs 2014 to 2021

High-performance titanium alloys with an equiaxed composite microstructure were achieved by sintering and crystallizing amorphous powder. By introducing a second phase in a β-Ti matrix, series of optimized Ti-Nb-Fe-Co-Al and Ti-Nb-Cu-Ni-Al composites, which have a microstructure composed of ultrafine-grained and equiaxed CoTi2 or (Cu,Ni)Ti2 precipitated phases surrounded by a ductile β-Ti matrix, were fabricated by sintering and crystallizing mechanically alloyed amorphous powder. The as-fabricated composites exhibit ultra-high ultimate compressive strength of 2585MPa and extremely large compressive plastic strain of around 40%, which are greater than the corresponding ones for most titanium alloys. In contrast, the alloy fabricated by …


Cellulose Nanofibers Networks For Structural Nanomaterials And Biocomposites With Multiple Functions, Lars Berglund Nov 2015

Cellulose Nanofibers Networks For Structural Nanomaterials And Biocomposites With Multiple Functions, Lars Berglund

Composites at Lake Louise (CALL 2015)

Cellulose-based composites offer interesting potential as environmentally friendly materials. Wood nanocellulose disintegrated from chemical pulp is an interesting component, which can be used in materials of increased structural, sophistication, extended property range and new functions [1]. The network forming character of cellulose nanofibers (CNF) makes it possible to form other types of nanomaterials than biocomposites such as nanopaper, aerogels, hydrogels, foams and honeycombs. The CNF can also be combined with inorganic nanoparticles to prepare organic/inorganic hybrid materials.

The structure of CNF is discussed and routes to improve the properties of the CNF are suggested. For the purpose of nanomaterials preparation, …


High Temperature Nanoindentation Testing Of Amorphous Silicon Carbonitride Thin Films, Radim Ctvrtlik, Marwan Al-Haik, Valeriy Kilikovsky Oct 2015

High Temperature Nanoindentation Testing Of Amorphous Silicon Carbonitride Thin Films, Radim Ctvrtlik, Marwan Al-Haik, Valeriy Kilikovsky

Nanomechanical Testing in Materials Research and Development V

The mechanical properties of amorphous silicon carbonitride (SiCxNy) films with various nitrogen content (y = 0-40 at.%) were investigated in-situ at elevated temperatures up to 650 °C in inert atmosphere. The hardness and elastic modulus were evaluated using depth sensing nanoindentation with cubic boron nitride Berkovich indenter. Both the sample and indenter were separately heated during the experiments to temperatures 300, 500 and 650 °C. Short duration high temperature creep (1200 s) of the films was also investigated. The results revealed that the room temperature hardness and elastic modulus decline with the increase of the nitrogen …


Elastic And Electronic Properties Of Ti2al(Cxn1−X) Solid Solutions, Sitaram Aryal, Ridwan Sakidja, Lizhi Ouyang, Wai-Yim Ching Apr 2015

Elastic And Electronic Properties Of Ti2al(Cxn1−X) Solid Solutions, Sitaram Aryal, Ridwan Sakidja, Lizhi Ouyang, Wai-Yim Ching

Mathematical Sciences Faculty Research

The elastic coefficients and mechanical properties (bulk modulus, shear modulus, Young's modulus and Poisson's ratio) of Ti2Al(CxN1−x) continuous solid solutions for x from 0 to 1 are calculated using ab initio DFT methods on 4×4×1 supercell models. It is shown that the properties of these solid solutions do not vary linearly with x. Although the lattice constant c is almost constant for x≤0.5, a increases linearly. For x>0.5, c starts to increase with x while the rate of increase in a slows down. For x between 0.5 and 0.85, the elastic coefficients and the mechanical parameters show interesting dependence …


An Investigation Of The Effect Of Direct Metal Deposition Parameters On The Characteristics Of The Deposited Layers, Tarak A. Amine, Joseph William Newkirk, Frank W. Liou Jul 2014

An Investigation Of The Effect Of Direct Metal Deposition Parameters On The Characteristics Of The Deposited Layers, Tarak A. Amine, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

Multilayer direct laser deposition (DLD) is a fabrication process through which parts are fabricated by creating a molten pool into which metal powder is injected as particles. During fabrication, complex thermal activity occurs in different regions of the build; for example, newly deposited layers will reheat previously deposited layers. The objective of this study was to provide insight into the thermal activity that occurs during the DLD process. This work focused on the effect of the laser parameters of newly deposited layers on the microstructure and mechanical properties of the previously deposited layers in order to characterize these effects to …


A Tensile Deformation Model For In-Situ Dendrite/Metallic Glass Matrix Composites, J. W. Qiao, T. Zhang, Fuqian Yang, P. K. Liaw, S. Pauly, B. S. Xu Oct 2013

A Tensile Deformation Model For In-Situ Dendrite/Metallic Glass Matrix Composites, J. W. Qiao, T. Zhang, Fuqian Yang, P. K. Liaw, S. Pauly, B. S. Xu

Chemical and Materials Engineering Faculty Publications

In-situ dendrite/metallic glass matrix composites (MGMCs) with a composition of Ti₄₆Zr₂₀V₁₂Cu₅Be₁₇ exhibit ultimate tensile strength of 1510 MPa and fracture strain of about 7.6%. A tensile deformation model is established, based on the five-stage classification: (1) elastic-elastic, (2) elastic-plastic, (3) plastic-plastic (yield platform), (4) plastic-plastic (work hardening), and (5) plastic-plastic (softening) stages, analogous to the tensile behavior of common carbon steels. The constitutive relations strongly elucidate the tensile deformation mechanism. In parallel, the simulation results by a finite-element method (FEM) are in good agreement with the experimental findings and theoretical calculations. The present study gives a mathematical model to clarify …


Effect Of Architecture And Porosity On Mechanical Properties Of Borate Glass Scaffolds Made By Selective Laser Sintering, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Taylor Comte Aug 2013

Effect Of Architecture And Porosity On Mechanical Properties Of Borate Glass Scaffolds Made By Selective Laser Sintering, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Taylor Comte

Mechanical and Aerospace Engineering Faculty Research & Creative Works

The porosity and architecture of bone scaffolds, intended for use in bone repair or replacement, are two of the most important parameters in the field of bone tissue engineering. The two parameters not only affect the mechanical properties of the scaffolds but also aid in determining the amount of bone regeneration after implantation. Scaffolds with five different architectures and four porosity levels were fabricated using borate bioactive glass (13-93B3) using the selective laser sintering (SLS) process. The pore size of the scaffolds varied from 400 to 1300 μm. The compressive strength of the scaffolds varied from 1.7 to 15.5 MPa …


Freeze-Form Extrusion Fabrication Of Functionally Graded Material Composites Using Zirconium Carbide And Tungsten, Ang Li, Aaron S. Thornton, Bradley K. Deuser, Jeremy Lee Watts, Ming-Chuan Leu, Greg Hilmas, Robert G. Landers Aug 2012

Freeze-Form Extrusion Fabrication Of Functionally Graded Material Composites Using Zirconium Carbide And Tungsten, Ang Li, Aaron S. Thornton, Bradley K. Deuser, Jeremy Lee Watts, Ming-Chuan Leu, Greg Hilmas, Robert G. Landers

Materials Science and Engineering Faculty Research & Creative Works

Ultra-high-temperature ceramics are being investigated for future use in aerospace applications due to their superior thermo-mechanical properties, as well as their oxidation resistance, at temperatures above 2000⁰C. However, their brittleness makes them susceptible to thermal shock failure. As graded composites, components fabricated as functionally-graded materials (FGMs) can combine the superior properties of ceramics with the toughness of an underlying refractory metal. This paper discusses the grading of two materials through the use of a Freeze-form Extrusion Fabrication (FEF) system to build FGM parts consisting of zirconium carbide (ZrC) and tungsten (W). Aqueous-based colloidal suspensions of ZrC and W were developed …


The Influence Of Heterogeneous Meninges On The Brain Mechanics Under Primary Blast Loading, Linxia Gu, Mehdi S. Chafi, Shailesh Ganpule, Namas Chandra Apr 2012

The Influence Of Heterogeneous Meninges On The Brain Mechanics Under Primary Blast Loading, Linxia Gu, Mehdi S. Chafi, Shailesh Ganpule, Namas Chandra

Department of Mechanical and Materials Engineering: Faculty Publications

In the modeling of brain mechanics subjected to primary blast waves, there is currently no consensus on how many biological components to be used in the brain–meninges–skull complex, and what type of constitutive models to be adopted. The objective of this study is to determine the role of layered meninges in damping the dynamic response of the brain under primary blast loadings. A composite structures composed of eight solid relevant layers (including the pia, cerebrospinal fluid (CSF), dura maters) with different mechanical properties are constructed to mimic the heterogeneous human head. A hyper-viscoelastic material model is developed to better represent …


Effect Of Particle Size, Binder Content And Heat Treatment On Mechanical Properties Of 13-93 Bioactive Glass Scaffolds, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Mariano Garcia Velez Aug 2011

Effect Of Particle Size, Binder Content And Heat Treatment On Mechanical Properties Of 13-93 Bioactive Glass Scaffolds, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas, Mariano Garcia Velez

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Particle size, binder content and the post-processing schedule are important parameters that affect the microstructure, and, hence, the mechanical properties of parts produced using the indirect selective laser sintering process. 13-93 bioactive glass, with mean particle sizes ranging from 10 μm to 44 μm, is mixed with different amounts of stearic acid binder to fabricate green scaffolds. Through the design of the post-processing schedule, the time required for postprocessing the green scaffolds is reduced from the initial 80 hrs to 12 hrs. The compressive strength varies from 41 MPa for a part with~60% porosity to 157 MPa for a part …


Freeze Extrusion Fabrication Of 13-93 Bioactive Glass Scaffolds For Bone Repair, Tieshu Huang, Nikhil D. Doiphode, M. N. Rahaman, Ming-Chuan Leu, B. Sonny Bal, D. E. Day Aug 2010

Freeze Extrusion Fabrication Of 13-93 Bioactive Glass Scaffolds For Bone Repair, Tieshu Huang, Nikhil D. Doiphode, M. N. Rahaman, Ming-Chuan Leu, B. Sonny Bal, D. E. Day

Materials Science and Engineering Faculty Research & Creative Works

There is an increasing demand for synthetic scaffolds with the requisite biocompatibility, internal architecture, and mechanical properties for the bone repair and regeneration. In this work, scaffolds of a silicate bioactive glass (13-93) were prepared by a freeze extrusion fabrication (FEF) method and evaluated in vitro for potential applications in bone repair and regeneration. The process parameters for FEF production of scaffolds with the requisite microstructural characteristics, as well as the mechanical and cell culture response of the scaffolds were evaluated. After binder burnout and sintering (60 min at 700°C), the scaffolds consisted of a dense glass network with interpenetrating …


Freeform Fabrication Of Zirconium Diboride Parts Using Selective Laser Sintering, Ming-Chuan Leu, Erik B. Adamek, Tieshu Huang, Greg Hilmas, Fatih Dogan Aug 2008

Freeform Fabrication Of Zirconium Diboride Parts Using Selective Laser Sintering, Ming-Chuan Leu, Erik B. Adamek, Tieshu Huang, Greg Hilmas, Fatih Dogan

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Using the Selective Laser Sintering (SLS) process, both flexural test bars and 3D fuel injector components have been fabricated with zirconium diboride (ZrB2) powder. Stearic acid was selected as the binder. Values of SLS process parameters were chosen such that the green parts could be built with sharp geometrical features and that the sintered parts could have good mechanical properties. After binder burnout and sintering, the SLS fabricated ZrB2 test bars achieved 80% theoretical density, and the average flexural strength of the sintered samples was 195 MPa. These values demonstrate the feasibility of the SLS process for …


Titanium Alloyed With Boron, Seshacharyulu Tamirisakandala, Daniel B. Miracle, Raghavan Srinivasan, Jay S. Gunasekera Dec 2006

Titanium Alloyed With Boron, Seshacharyulu Tamirisakandala, Daniel B. Miracle, Raghavan Srinivasan, Jay S. Gunasekera

Mechanical and Materials Engineering Faculty Publications

Small additions of boron to conventional titanium alloys have been found to produce significant changes to the microstructures and associated properties. Grain refinement and improved strength and stiffness are first-order effects, which lead to possibilities for developing novel and affordable processing methodologies and to enhance performance over conventional titanium alloys. In this article, we introduce this new class of titanium alloys and describe unique formability benefits achieved via engineering microstructures.