Engineering Commons^™

A Study Of The Deleading Of Zinc Sulfide Concentrates, Larry Leroy Gidley

Masters Theses

"The object of this research was to study the basic principles and optimum conditions for the deleading of commercial zinc sulfide concentrates by sublimation of the lead in the form of a sulfide. Present commercial practice conducts this sublimation in hearth roasters. This research considered only the variables affecting sublimation of the lead sulfide, not the types of applicable equipment, or other possible processes. However, the laboratory conditions were at least partially similar to those that could be obtained in commercial practice"--Object, page 1.

Development Of Large Hole Burn Cut Drift Rounds, Joseph J. Yancik Jr.

Masters Theses

"A decided change in the attitudes of mining management toward the need for mine research has taken place during the past decade. More emphasis is being placed not only on the improvement of existing mining methods, but also on the adaptation of new ideas. As the depletion of the high grade ore deposits in this country becomes a reality, the need for reducing the costs of mining is pressing. The successful exploitation of low grade ore bodies will depend upon the continued advancement in the science of mining.

The methods used today in driving a small drift or tunnel in …

Physical Properties Of Concrete At Early Ages, Peter G. Hansen

Masters Theses

"One of the principal types of heavy duty pavements in use in Missouri and in many other states is that known as rigid type portland cement concrete.

There have been two major trends in this type of pavement design. One of these trends is the use of short slabs, i.e., 15 to 25 feet, with no reinforcement. Another trend consists of concrete slabs containing distributed reinforcement such as wire mesh or reinforcing bars with joints occurring at fairly large intervals of 50 to 100 feet. As loads on the highways have increased the designers have increased the slab thicknesses and …

Further Studies Of Vapor-Liquid Equilibria Of Methanol-Ethylene Glycol-Water, Herbert Benjamin Sachs

Masters Theses

"The freezing points of the ternary system methanol-glycol-water have been investigated by Conrad, Hill and Ballman. The vapor-liquid equilibria of the same system was studied by Sjoberg. These investigations were carried out to determine the properties of the system relative to its possible use as an antifreeze mixture.

Since Sjoberg's work in 1948, the improved Othmer equilibrium still has been introduced for vapor-liquid experimental determinations. It is therefore the purpose of the present investigation to evaluate the use of this still, compare results with those obtained by Sjoberg, and analyze ternary mixtures for the entire range of glycol concentrations.

The …

Mechanical Vibration Of Vacuum Tubes, Jerry Dale Swearingen

Masters Theses

"Since the beginning of the art of vacuum tube building, vacuum tube engineers have been faced with many mechanical problems as well as electrical problems.

Early mechanical problems were comparatively small because most of the tubes were used in stationary apparatus where little or no vibration was envolved.

As time went on, vacuum tubes were placed in portable equipment and this useage established the need for a tube that was mechanically strong enough to give reliable electrical behavior where the tube was subjected to considerable vibration….

Recently it has been shown that vacuum tubes operating in the instrument cabins of …

A Study Of Titanium Diffusion Coatings By X-Ray Fluorescent Methods, Alan Bernard Burgess

Masters Theses

"As the only previous determinations of the chemical composition of the titanium coatings had been analyses of the average composition of the entire coating, the determination of the variation in chemical composition throughout the coating was suggested. From this information, it was proposed that a better insight might be gained as to the extent and mechanism of diffusion in the coatings. It was also hoped to correlate the results with concurrent work being done on the phases present in the titanium coatings. From this correlation, it might be possible to show which phases are responsible for the desirable properties of …

Deposition Of Titanium By Gaseous Reaction, Louis John Reitsma Jr.

Masters Theses

"Previous investigations undertaken at the Missouri School of Mines and Metallurgy on the deposition of titanium involved the use of fused salt baths, aqueous solutions, and cementation processes. The fused salt baths produced satisfactory coatings on small metal parts. Some difficulty was encountered however, when the coating of large articles was attempted.

For this reason, it was decided to investigate the possibility of titanium deposition by the reaction of a volatile titanium compound with a metal surface. Two different compounds were proposed for investigation, (1) a lower chloride of titanium and (2) an iodide of titanium. The reaction with the …

A Study Of Tunnel Demolition By Hasty Methods, Richard Lee Bullock

Masters Theses

"The use of explosives to construct obstacles which impede the enemy or close his routes of communication has long been employed by our armies. They have developed fairly effective methods for destroying bridges, setting up road craters and constructing abatis. However, one phase of obstacle construction, that of tunnel demolition, has been neglected in that no procedures or methods have been formulated which will aid in the proper destruction of tunnels.

At the present time, under the auspices of the Department of the Army, The Missouri School of Mines and Metallurgy is conducting a research program on tunnel demolition. The …

The Preparation Of Titanium Tetrachloride From Rutile, Nalin Sen

Masters Theses

"In recent years, considerable interest has been shown in the manufacture of titanium metal because of its outstanding properties both physical and chemical. The commercial process for the preparation of metallic titanium, known as the Kroll process, consists essentially of the reduction of titanium tetrachloride with magnesium in an inert atmosphere to produce titanium metal with magnesium chloride as a by-product.

Since, titanium tetrachloride is the basic compound from which to prepare metallic titanium by the Kroll process, much thought has been given to the preparation of titanium tetrachloride from titanium ores such as rutile or ilmenite.

The present work …

A Study Of The Structure Of Titanium Diffusion Coatings On Iron And Steel, Pao-Jen Chao

Masters Theses

"The Problem of the Thesis: A series of experiments have been made in the Metallurgical. Engineering Department of the Missouri School of Mines and Metallurgy for the investigation of titanium diffusion coatings. The technique of applying the titanium diffusion coatings on iron and steel is still in the experimental stage. A few of the physical properties and chemical compositions of such coatings have been determined, but the structures have not yet been extensively studied. As the correlations of the structures and the desirable properties are valuable for improving the quality or titanium diffusion coatings on iron and steel, an investigation …

The Closure Of Thin Wall Pressure Vessels, Archie W. Culp Jr.

Masters Theses

"The object of this thesis is to find various methods of closing thin wall aluminum cylinders. Such a closure must be strong enough, that when internal pressure is applied, ultimate failure will occur along a longitudinal element of the cylinder and not at the closure. Moreover, such a method must not only be mechanically sound, but it must be readily adaptable to mass production"--Introduction.

Investigation Of Soil Bricks As A Building Material, Ahmet Ilter

Masters Theses

"The need of a cheap construction material for small village farm construction in Turkey makes soil-cement a most desirable material. What is more, as far as the author knows, soil-cement has not found any application in farm house construction in Turkey as yet. So the author, being acquainted with his native country's house construction problem, and seeing the suitable application soil-cement have on such construction, came to the decision that he should investigate this problem thoroughly.

The main objective of the tests run in this investigation will be to find the strength of different samples of soil-cement. The stabilizer used …

A Fundamental Study Of Clay Drying Using Ware Of Large Cross Section, Robert F. Grady Iii

Masters Theses

"The drying of clay has been studied extensively in the past by many investigators, some of whom attempted to relate this information to the structure of clay and thereby develop a more vivid picture, while others studied the mechanism of drying in its own right in order to present a useable theory that would allow improvements in the drying operation.

At present the literature is unable to present a theory of the mechanism of drying that is sufficiently general to cover the observed aspects of clay drying. Many and varied mechanisms are presented, but correlation is seldom completely evident between …

The Use Of A Steady State Flow Reactor In The Study Of Rapid Gas Phase Reactions, Ormond Kennedy Lay

Masters Theses

"The demonstration of the feasibility of rocket propelled devices for various purposes within the past few years has initiated an intensive search for suitable reactants for use as rocket fuels. Consequently, the investigation of the properties of chemical reactions which rapidly liberate large quantities of energy has assumed major importance. In order that such reactions may be adapted to practical use as rocket propellants knowledge of the characteristics of these reactions is required. Properties such as+ the mechanism of the reaction, the speed of the reaction under varied conditions of temperature, pressure and concentrations, the conditions required for the initiation …

An Investigation Of Continuous Steel Beams In The Plastic Range, Robert Adams Shoolbred

Masters Theses

"The purpose of this thesis is to investigate the action of beams in the plastic range. The test specimen will be a 4WF 13 structural shape continuous over three supports having equal span lengths of seven feet. Three types of loading were chosen. The first loading will be concentrated in the center of each span. The second loading will be a concentrated load in the center of one span only. The third loading will be the settlement of the two end supports until a plastic hinge forms at the center support, then the two spans will be loaded with concentrated …

Horizontal Pressures On Retaining Walls Due To Line Surface Loads, John B. Heagler

Masters Theses

"Among the oldest types of structures with which engineers have had to deal are those which serve to laterally restrain masses of earth, or to prevent earth embankments from assuming their natural angle of repose. This is necessary where space is limited or the natural slope would encroach upon other property. These structures, usually called retaining walls, are subjected to forces, both lateral and vertical due to the pressures exerted by the backfill material and any loads imposed on the backfill material. The first step in the design of the retaining wall is to determine the magnitude, position, and line …

Testing Of Missouri Shales For Light Weight Aggregate Production, Jerry D. Plunkett

Masters Theses

"The original objective of this investigation was to determine by testing those clays, shales, and loesses occuring in Missouri in large deposits (over 15 feet in thickness with little overburden), which would be suitable for the production of light weight aggregate. The second objective was to investigate the mechanism of bloating as related to the physical and chemical properties of the above materials, and by using these relationships cause clays which do not naturally bloat, to bloat using some addition. The use of additives would permit the economical use of material closer to the market in many instances.

After the …

The Design And Construction Of An Electronic D-C Analog Computer, Frederick R. Wagner, William A. Paar

Masters Theses

"To make this project realizable with the funds available and in the time allowed, and to set forth some definite goals, the following objectives were adopted:

1. Design, construct, and place in working order a d-c electronic analog computer capable of solving 4th order linear differential equations with constant coefficients.
2. Include in the design provisions for real time computation, and also fast, repetitive operation.
3. Provide for later expansion of the computer installation.
4. Limit expenditures to $700"--Introduction, page 4.

Heat Flow In A Two-Dimensional Steady-Flow System Without Radial Symmetry, George H. Parharoglu

Masters Theses

"As the extent of the science of heat conduction depends on the multiplicity of the boundary conditions that can be applied to the basic differential equation, a particular case in which the use of one set boundary conditions for the development of the general equation for the temperature distribution as well as the the amount of heat flow in a steady-state, two-dimensional heat flow system with a source of heat plased at the center of or along the axis of a cylinder, and without radial symmetry has been the object of this problem. Radial symmetry means the variation of temperature …

Deposition Of Metallic Coatings From Fused Salt Baths, Andrew Hessler Larson

Masters Theses

"This thesis is the result of an investigation undertaken to study some of the important factors affecting the deposition of metallic diffusion coatings on other metals immersed in a fused salt bath….

There are many methods which have been devised to obtain diffusion coatings on various metals. One which is quite well known and used commercially is the process of “chromizing” which produces a diffusion layer if chromium on another metal. One method of “chromizing” consists of immersing the specimen to be coated in a mixed chloride fused bath containing chromium metal flakes. Another method consists of packing a low …

Effect Of Carbon Content In Steels Upon The Deposition Of Titanium From A Fused Salt Bath, Reinhard Paul Abendroth

Masters Theses

"STATEMENT OF PROBLEM Previous work done at the Missouri School of Mines and Metallurgy on the deposition of titanium upon various metals, especially iron and steel, bas shown that titanium can be deposited upon ingot iron and. low carbon steels with comparitive ease. Difficulty was encountered in attempts to deposit titanium upon steels of higher carbon content and upon cast irons.

For this reason, it was decided to investigate more thoroughly the relationship between the carbon content of various steels and the quality of titanium coatings deposited on these steels. Once this relationship had been established, a suitable theoretical explanation …

Corrosion Products Of Titanium In Fused Salt Baths, Kai-Chai Chiou

Masters Theses

"Titanium is gaining great interest in the modern metal industry because of its natural abundance and its desirable physical and chemical properties. Among them, its excellent corrosion resistance, such as the resistance to normal atmosphere attack, humid and saline atmosphere attack, sea water attack, and nitric acid attack, is the most prominent characteristic being welcomed by the engineers. The usefulness of titanium would be greatly increased if it were possible to plate titanium on other metals, thus increasing the corrosion resistance of these other metals.

Much concern, at present, has been given to the possibilities of the electrodeposition of titanium …

Mechanism And Measurement Of First Stage Graphitization In White Cast Iron, David S. Gould

Masters Theses

"The original object of this thesis was to ascertain if coercive force measurements could be used for the determination of degree of malleablization in malleable iron. Since first stage graphitization was involved, it was only natural that an interest in the mechanism of first stage graphitization developed. The investigation which resulted from this interest was done primarily for the edification of the author, however it was subsequently deemed of enough importance to be included in this thesis. For this reason the thesis may appear at times to deviate from the original objective"--Preface, page iii.

Tunnel Rehabilitation, Jay C. Dotson

Masters Theses

"This paper is an outgrowth of research conducted at Missouri School of Mines and Metallurgy over a two year period. The purpose of the study is to assemble into one volume information that is pertinent to the rehabilitation of tunnels. Notwithstanding the voluminous size of the paper, much descriptive material necessarily has been omitted because of the far-reaching scope of tunneling practices and of the specialized fields therein. An extensive bibliography has been prepared to supplement the material that has been selected for presentation. Through consultation with tunnel men of all ranks, observations in the field, and an intensive search …

The Bloating Of Missouri's Shales, Peter Kurtz Jr.

Masters Theses

"The first objective of this investigation was to determine which deposits of clays, shales, and loesses in Missouri are suitable for use in the production of lightweight aggregate by virtue of their expanding characteristics upon heating. The second objective was to determine, if possible, commercially feasible additions that will produce the bloating property in shales that do not naturally bloat.

There are two conditions which must be met in firing in order to bloat a clay or shale. First, a gas must be formed and evolved during firing. Second, enough glass of the proper viscosity must be formed to trap …

Crimp Method Of Closure Of Small Pressure Vessels, Zafiri Bersu

Masters Theses

"The object of this thesis is to design a means of closing the ends of thin aluminum alloy tubing in the 1” O.D. to 2” O.D. by .035 to .065 inch thick sizes, so that the closure will withstand internal hydrostatic pressure sufficient to burst the tube along the longitudinal element.

The aim is to approach the ultimate mechanical efficiency possible, and at the same time to keep actual production in mind.…

Summarizing the aims of this investigation, it can be said that the objectives of this investigation are:

1. To design ends for closed vessels.
2. To form the designs.
3. To …

The Lattice Constant And Coefficient Of Expansion Of Chromium, Chao-Ching Weng

Masters Theses

"The most important use of chromium, other than as an alloying element in the manufacture of stainless steel, is for electroplating; to form a coating on other metals for corrosion prevention in order to procure longer life, and to achieve a decorative effect.

The physical properties of chromium are important in the effectiveness of its uses, and its lattice constant, as well as coefficient of thermal expansion, seem worthy of exact determination.

A number of research workers, over a span of thirty years, have spent considerable effort in determining the aforementioned constants. However, their results do not check, and the …

An Investigation Of The Use Of Surface-Active Agents In The Secondary Recovery Of Oil By Water Flooding, Robert P. Schafer

Masters Theses

"The importance of producing oil cannot be emphasized enough in this modem world. Therefore, when primary methods of production seemingly exhaust the oil reservoirs, a secondary method of producing more oil is a necessity. At the present time, secondary methods of oil recovery have developed into a large industry. They are not a new development. The need of introducing compressed air or air-gas mixtures into the wells to increase production was quickly realized. Water flooding methods followed, and at first were restricted to the Eastern fields. Later, about 1935, systematic water flooding methods were developed and applied all over the …

Photoelastic Investigation Of The Stresses In A Capless Connecting Rod, Gerald Delaine Smith

Masters Theses

"For a great many years the primary method used to solve engineering problems was by the use of mathematics. However, rigorous and simple mathematical solutions are only possible if the geometry of the member and its loadings are relatively simple. When irregular shapes with complex loadings are encountered, rigorous mathematical solutions for stresses induced are either impossible or very cumbersome. In such cases, the engineer must resort to other methods which are available today.

This paper attempts to show the application of the photoelastic method to such a problem. Moreover, it will show the comparative ease with which the designer …

Effect Of Viscosity On The Cetane Number Of A Diesel Fuel, Moris Bolay

Masters Theses

"The object of this paper is to determine or rather experimentally establish the effect of a change in viscosity of a given diesel oil in regard to the ignition quality (cetane rating) of the oil.

The author did not attempt to prove why or find out how much the cetane number was affected. But, merely, tried to experimentally verify the fact that the cetane number of the fuel used underwent a change when its viscosity was decreased by preheating it.

Since his professional interests lie in the field of automotive engineering, several thesis problems were suggested to him by Dr. …