Engineering Commons^™

Efficient Uncertainty Quantification In Aerospace Analysis And Design, Yi Zhang

Doctoral Dissertations

"The main purpose of this study is to apply a computationally efficient uncertainty quantification approach, Non-Intrusive Polynomial Chaos (NIPC) based stochastic expansions, to robust aerospace analysis and design under mixed (aleatory and epistemic) uncertainties and demonstrate this technique on model problems and robust aerodynamic optimization. The proposed optimization approach utilizes stochastic response surfaces obtained with NIPC methods to approximate the objective function and the constraints in the optimization formulation. The objective function includes the stochastic measures which are minimized simultaneously to ensure the robustness of the final design to both aleatory and epistemic uncertainties. For model problems with mixed uncertainties, …

Heat Transfer And Bubble Dynamics In Bubble And Slurry Bubble Columns With Internals For Fischer-Tropsch Synthesis Of Clean Alternative Fuels And Chemicals, Moses Odongo O. Kagumba

Doctoral Dissertations

"Synthesis gas, a mixture of CO and H₂ obtained from coal, natural gas and biomass are increasingly becoming reliable sources of clean synthetic fuels and chemicals and via Fischer-Tropsch (F-T) synthesis process. Slurry bubble column reactor is the reactor of choice for the commercialization of the F-T synthesis. Even though the slurry bubble column reactors and contactors are simple in structures, their design, scale-up, operation, and performance prediction are still challenging and not well understood due to complex interaction of phases. All the studies of heat transfer have been performed without simultaneously investigating the bubble dynamics adjacent to the heat …

Inverter Design And Analysis Using Multiple Reference Frame Theory, Luke Dale Watson

Doctoral Dissertations

"Multiple reference frame theory allows for periodically time varying signals to be represented as a set of dc signals. In other words, every periodic signal can be expanded into a Fourier series representation. By modeling an inverter connected to a boost maximum power point tracker (MPPT) in this manner, frequency transfer properties can be preserved and harmonics throughout the system can be predicted. A state space model taking into account the dc and fundamental grid frequency is presented and used to optimize the controller gains of the system. Using information from the dq-axis values of the measured grid current and …

New Microarray Image Segmentation Using Segmentation Based Contours Method, Yuan Cheng

Doctoral Dissertations

The goal of the research developed in this dissertation is to develop a more accurate segmentation method for Affymetrix microarray images. The Affymetrix microarray biotechnologies have become increasingly important in the biomedical research field. Affymetrix microarray images are widely used in disease diagnostics and disease control. They are capable of monitoring the expression levels of thousands of genes simultaneously. Hence, scientists can get a deep understanding on genomic regulation, interaction and expression by using such tools.

We also introduce a novel Affymetrix microarray image simulation model and how the Affymetrix microarray image is simulated by using this model. This simulation …

Microfluidic Devices Applied On Enriching Post –Translational Modified Proteins For Proteomics, Hui Xia

Doctoral Dissertations

In this work, microfluidic devices were developed for enriching post-translational modified proteins. Post-translational modifications (PTM) of proteins play essential roles in cellular physiology and disease. The identification of protein substrates and detection of modification site helps understand PTM-mediated regulation in essential biological pathways and functions in various diseases. However, PTM proteins are typically present only at trace levels, making them difficult to identify in mass spectrometry based proteomics. This work study is about the design, fabrication and testing of the microfluidic device for the enrichment of abundant amount of PTMs. Carbonylated protein is used as a representative PTM to illustrate …

Rheological Study Of Asphalt Binders With A Wax-Based Warm Mix Additive And Its Relationships To Mix Compaction And Rutting, Rajan Saha

Doctoral Dissertations

Although the energy saving Warm Mix Asphalt (WMA) technology that produces asphalt mixes at lower temperatures are around for about a decade, there still exist some concerns that are hindering its wide spread implementation. The overall objective of this study is to investigate if the viscosity reductions at higher temperatures have any impacts on asphalt mix compaction and rutting performances. This study reveals that there exists a critical temperature for each asphalt binder below which viscosity will increase with addition of Sasobit®. Therefore, compaction below the critical temperature can negatively impact density.

For PG 64-22, the critical temperature is 104 …

Ultrasonication Assisted Layer-By-Layer Technology For The Preparation Of Multi-Functional Anticancer Drugs Paclitaxel And Lapatinib, Xingcai Zhang

Doctoral Dissertations

In this dissertation, ultrasonication assisted Layer-by-Layer (LbL) technology for the preparation of multifunctional poorly water-soluble anticancer drug nanoparticles, paclitaxel and lapatinib, has been developed. Many FDA approved drugs are very low soluble in water; therefore, it is very difficult to load and control their release and targeting efficiently, which greatly confines their application. The development of this method will pave the way for the development and application of those low soluble anticancer drugs.

In the first part of this dissertation, the first approach for powerful ultrasonication, the top-down approach (sonicating bulk drug crystals in polyelectrolyte solution), was successfully applied for …

Using Power-Law Properties Of Social Groups For Cloud Defense And Community Detection, Justin L. Rice

Doctoral Dissertations

The power-law distribution can be used to describe various aspects of social group behavior. For mussels, sociobiological research has shown that the Lévy walk best describes their self-organizing movement strategy. A mussel's step length is drawn from a power-law distribution, and its direction is drawn from a uniform distribution. In the area of social networks, theories such as preferential attachment seek to explain why the degree distribution tends to be scale-free. The aim of this dissertation is to glean insight from these works to help solve problems in two domains: cloud computing systems and community detection.

Privacy and security are …

Engineering Microenvironments To Modulate Calcium Information Processing In Neuronal Cells, Kinsey Cotton Kelly

Doctoral Dissertations

Tissue engineered microenvironments were constructed to test the effects glial cells have on calcium information processing, and to mimic conditions in vivo for tumor invasion and residual cancer after resection of tumor. Submaximal, nM, glutamate (GLU) stimuli were applied to the engineered environments, and the resulting calcium dynamic behavior of neuronal cells was measured to help predict and interpret chaotic systems in the experimental realm. Calcium is a key signaling ion which signals through the N-methyl-D-aspartate (NMDA) glutamate receptor on the neuronal membrane. GLU binding to the NMDA receptor (NMDAR) causes a large and dynamic increase in neuronal intracellular calcium. …

Integration Of Nanoporous Zeolite With Optical Fiber Devices For Chemical Sensing, Xinwei Lan

Doctoral Dissertations

"Label-free optical fiber chemical sensors have provoked significant research interest in recent years due to their unique advantages of small size, low cost, potential for distributed sensing, capability of in situ and remote operation, and tolerance to harsh environments. However, existing optical fiber chemical sensors lack the desired sensitivity and specificity for many applications such as chemical and biological analysis, industrial process control, environmental monitoring, and national security.

The dissertation summarizes our research efforts and results in functional integration of nanoporous zeolites with optical fiber devices for development of label-free optical fiber chemical sensors with high sensitivity and selectivity. Fundamental …

Processing, Microstructural Evolution And Electrochemical Performance Relationships In Solid Oxide Fuel Cells, Ayhan Sarikaya

Doctoral Dissertations

"The relationships between the processing parameters, microstructures and electrochemical performance of solid oxide fuel cell (SOFC) components were investigated. The operating regimes (i.e., reducing vs. oxidizing) as well as the elevated temperatures (e.g. 800°C) for their operation introduce several material challenges. Therefore, composite materials are employed to withstand operating conditions while providing sufficient electrochemical performance for fuel cell operation. Analyses on lanthanum-strontium manganite (LSM) - yttria stabilized zirconia (YSZ) compositions (45 vol%-55 vol%) by impedance spectroscopy demonstrated that two competing polarization mechanisms (i.e. charge-exchange and surface adsorption-diffusion of oxygen) limit performance. Optimization of microstructures resulted in total resistances as low …

Infiltrated Composite Electrodes For Solid Oxide Fuel Cells, Aligul Buyukaksoy

Doctoral Dissertations

"Solid oxide fuel cells (SOFCs) are electrochemical devices which can convert chemical energy to electrical energy with efficiencies up to 60%. In order for SOFCs to be favorable energy conversion devices, the power obtained from a unit volume should be improved. This corresponds to minimized resistances from SOFC components (composite electrodes and electrolyte). Stability of the generated power is another important issue. Degradation of SOFCs with time due to microstructural processes or chemical reactions that occur at operating conditions; and due to reduction/oxidation cycles caused by the changes in the anode has been an important obstacle that has prevented the …

Numerical Modeling Of Heat Transfer And Fluid Flow In Laser Metal Deposition By Powder Injection, Zhiqiang Fan

Doctoral Dissertations

"Laser metal deposition is an additive manufacturing technique which allows quick fabrication of fully-dense metallic components directly from Computer Aided Design (CAD) solid models. A self-consistent three-dimensional model was developed for the laser metal deposition process by powder injection, which simulates heat transfer, phase changes, and fluid flow in the melt pool, The governing equations for solid, liquid and gas phases in the calculation domain have been formulated using the continuum model. The free surface in the melt pool has been tracked by the Volume of Fluid (VOF) method, while the VOF transport equation was solved using the Piecewise Linear …

On The Effect Of Silicon And Phosphorus During The Precipitation Of Κ-Carbide In Fe-Mn-Al-C Alloys, Laura Bartlett

Doctoral Dissertations

"Implementation of lightweight high manganese and aluminum steels for use in high energy absorbing applications requires a detailed knowledge of how alloying additions and impurities affect age hardening and high strain rate fracture properties. Dynamic fracture toughness is an important design criterion but has not been reported previously in these alloys. In addition, previous studies have shown that silicon and phosphorus increased the strength and aged hardness; however, the mechanism was unknown. This research mainly focuses on the effect of silicon and phosphorus on the precipitation of Κ-carbide and alloy partitioning during aging. Short range ordering, SRO, of Fe-Al-C into …

Phytoforensics On Energetics: Novel Plant Tissue Measure Approach And Modeling, Yuan Yuan

Doctoral Dissertations

"Explosives and energetics are common soil and groundwater pollutions. This research was to develop novel phytoforensics approaches on energetics. Four different plants species, including woody perennial trees and monocot grasses, were planted both in soil and sand reactors with continuous exposure to a mixture of explosives in the greenhouse. Time dependent assessments were carried out to determine kinetic mechanisms of uptake, transport and accumulation. Plant concentrations were analyzed by both traditional solvent extraction and novel sap analysis methods. A dynamic soil-plant system model was developed to quantify the relationship between tissue concentration and soil pore water concentration for non-volatile organic …

Optimized Techniques For Real-Time Microwave And Millimeter Wave Sar Imaging, Joseph T. Case

Doctoral Dissertations

"Microwave and millimeter wave synthetic aperture radar (SAR)-based imaging techniques, used for nondestructive evaluation (NDE), have shown tremendous usefulness for the inspection of a wide variety of complex composite materials and structures. Studies were performed for the optimization of uniform and nonuniform sampling (i.e., measurement positions) since existing formulations of SAR resolution and sampling criteria do not account for all of the physical characteristics of a measurement (e.g., 2D limited-size aperture, electric field decreasing with distance from the measuring antenna, etc.) and nonuniform sampling criteria supports sampling below the Nyquist rate. The results of these studies demonstrate optimum sampling given …

Risk Analysis: Comparative Study Of Various Techniques, Hanan Mohammad Altabbakh

Doctoral Dissertations

"Researchers in the safety field are facing more challenges everyday with the expanding modern socio-technical systems. Safety analysis such as hazard analysis, accident causation analysis, and risk assessment are being revisited to overcome the shortcoming of the conventional safety analysis. With increasingly complex human system interaction in today's modern systems, new safety challenges are being faced that needed to be assessed and addressed. Managers and engineers face the challenge to choose from the vast amount of techniques available and utilize the correct one. Indeed, new or improved risk assessment tools that can address these complexities are needed. One of the …

Recycling Of Electronic Waste: Printed Wiring Boards, Alex Luyima

Doctoral Dissertations

"Pyrolysis and leaching are the dominant techniques applied in the recycling of waste printed wiring boards (PWBs). Waste PWB pyrolysis is a highly polluting technology and produces brominated pyrolysis oils in addition to hydrogen bromide (HBr) gas. Moreover, leaching as a treatment process of waste PWBs is not well investigated. In this work, the pyrolysis of waste PWBs has been studied with the aim of reducing the amount of brominated oils and HBr gas evolved. The effects of powder inorganic chemicals (CaO, CaCO₃, Fe₂O₃, Al₂O₃, Y-Zeolite, and ZSM-5) additions on the pyrolysis of waste PWBs has been studied through experiments …

Scaleup And Hydrodynamics Study Of Gas-Solid Spouted Beds, Shreekanta Basavaraj Aradhya

Doctoral Dissertations

"A thorough understanding of the complex flow structure of gas-solid spouted bed is crucial for design, scale-up and performance. Advanced gas-solid optical probes were developed and used to evaluate different hydrodynamic parameters of spouted beds. These optical probes measure solids concentration, velocity and their time series fluctuations. Since solids concentration needs to be converted to solids holdup through calibration, for meaningful interpretation of results, a novel calibration method was proposed (which is inexpensive and reliable compared to the current reported methods) and validated in the present study. The reported dimensionless groups approach of spouted bed scale-up was assessed and was …

Shear And Fracture Behavior Of High Performance Concretes, Mahdi Arezoumandi

Doctoral Dissertations

"Concrete is the most widely used man-made material in the world. Like other materials, it has been improved over time. Nowadays, with continued development of science and technology, a new generation of concretes is produced and is termed high performance concretes. A review of previously published work indicates that very few studies (in some cases none) have addressed the structural behavior of full-scale, high performance concrete elements. This study investigated the shear and fracture behavior of two types of high performance concrete - high-volume fly ash concrete (HVFAC) and self-consolidating concrete (SCC). The HVFAC incorporates up to 70% cement replacement …

The Role Of Face-To-Face Interactions In The Success Of Virtual Project Teams, Lawrence Raymond Blenke

Doctoral Dissertations

"This dissertation examines the importance of in-person Face-To-Face (FTF) interactions in virtual engineering development projects. The basis for this investigation will be the hypothesis that FTF interactions increase the effectiveness, quality of communication, and the trust between participants beyond that achieved with purely computer mediated communication. Through a combination of a literature review and empirical research, this dissertation addresses the following questions: * How important is FTF interaction in virtual development work? * Do various functional areas and age groups rate the importance of FTF interactions differently? * How does FTF interaction affect the levels of trust and communication within …

Data Fusion Techniques For Nondestructive Evaluation And Medical Image Analysis, Soumya De

Doctoral Dissertations

"Data fusion is a technique for combining data obtained from multiple sources for an enhanced detection or decision. Fusion of data can be done at the raw-data level, feature level or decision level. Applications of data fusion include defense (such as battlefield surveillance and autonomous vehicle control), medical diagnosis and structural health monitoring. Techniques for data fusion have been drawn from areas such as statistics, image processing, pattern recognition and computational intelligence. This dissertation includes investigation and development of methods to perform data fusion for nondestructive evaluation (NDE) and medical imaging applications. The general framework for these applications includes region-of-interest …

Establishing Well Operability Limits For Frac Pack Sandface Well Completions Using A Screen Erosion Model And Well Completion Score Card, Rickey Hendrix

Doctoral Dissertations

"Completion quality has a direct impact upon the maximum production rate at which a frac pack well should be operated. Best practices for frac pack well completions ensure the highest possible quality for the well completion. A novel frac pack well completion score card was developed based on best practices for frac pack well completions identified through consultation with industry experts. The score card systematically combines and assesses completions data readily available standard completion reports. The outcome of the score card process is a numerical completion quality rating, which combines all well design and frac pack operations information.

The completion …

Bioactive Glass Scaffolds For The Regeneration Of Load-Bearing Bone, Xin Liu

Doctoral Dissertations

"Biocompatible scaffolds that replicate the structure and function of bone would be ideal bone substitutes for structural bone loss, provided they have the requisite mechanical properties for reliable long-term loading. In this dissertation, strong porous scaffolds of silicate 13-93 bioactive glass, created with two different microstructures, were evaluated to determine their mechanical properties and their capacity to regenerate bone in a rat calvarial defect model. Scaffolds with an oriented microstructure of columnar pores were prepared by unidirectional freezing of camphene-based suspensions, followed by thermal annealing and sintering. By optimizing the freezing conditions, annealing time, and sintering temperature, constructs (porosity = …

Two Essays On Dynamic Programming And Reinforcement Learning, Shuva Ghosh

Doctoral Dissertations

"The semi-Markov decision process (SMDP) is a variant of the Markov decision process (MOP). This dissertation work focuses on the application of SMDPs to disaster response management and to maintenance management. Average and discounted reward are two popular performance metrics for MDPs/SMDPs. While both dynamic programming (DP) methods, i.e., value iteration and policy iteration, are commonly used to solve MDPs/SMDPs, value iteration is easier to apply than policy iteration. The existing value iteration algorithms for average reward SMDPs have some noteworthy limitations, which are sought to be overcome in this work. Reinforcement learning (RL) techniques, which are also studied in …

Nanoscale Metal Oxide And Supported Metal Catalysts For Li-Air Battery, Kan Huang

Doctoral Dissertations

"The dissertation work focuses on research and development of durable nanoscale catalysts and supports for rechargeable Li-air batteries that use aqueous catholytes. Transition metal oxides, TiO₂ and Nb₂O₅ in particular, were prepared from a sol-gel process in the form of nanocoatings (5~50 nm) on carbon nanotubes (CNTs) and studied as catalyst supports. Carbon doping in the oxides and post annealing significantly increased their electronic conductivity. Pt catalyst on the support with TiO₂ (Pt/c-TiO₂/CNTs) showed a much better oxygen reduction reaction (ORR) activity than a commercial Pt on carbon black (Pt/C). Negligible loss ( …

Approximate Dynamic Programming Based Solutions For Fixed-Final-Time Optimal Control And Optimal Switching, Ali Heydari

Doctoral Dissertations

"Optimal solutions with neural networks (NN) based on an approximate dynamic programming (ADP) framework for new classes of engineering and non-engineering problems and associated difficulties and challenges are investigated in this dissertation. In the enclosed eight papers, the ADP framework is utilized for solving fixed-final-time problems (also called terminal control problems) and problems with switching nature. An ADP based algorithm is proposed in Paper 1 for solving fixed-final-time problems with soft terminal constraint, in which, a single neural network with a single set of weights is utilized. Paper 2 investigates fixed-final-time problems with hard terminal constraints. The optimality analysis of …

Real Options Modeling And Valuation Of Price Adjustment Flexibility With An Application To The Leasing Industry, Ahmed A. A. Al Sharif

Doctoral Dissertations

"Uncertainty poses not only threats but also opportunities. This study sought to build the scientific foundation for introducing a real options (ROs) methodology for price risk management to the leasing industry. A price risk management that allows for both coping with threats and taking advantage of opportunities. In the leasing industry, fixed rate long-term lease contracts help contract parties stabilize cash flows within volatile markets. The contract's term, however, may be extended long enough that prevent capturing the opportunities of gaining greater profits or reducing expenses. Therefore, the flexibility that enables participants to take advantage of favorable market price is …

Coupled Geomechanical Reservoir Simulation, Amin Amirlatifi

Doctoral Dissertations

"Founded by Department Of Energy, the Plains CO₂ Reduction (PCOR) Partnership is investigating the Williston Basin as a candidate for sequestering CO₂ emissions from power plants. The State of Missouri, a member of PCOR, lies at the outermost point on the proposed transportation route and consequently faces the highest CO₂ compression and transportation costs. In order to minimize the cost of CO₂ sequestration, it is desirable to find a storage site within the state. The Lamotte sandstone is identified as a suitable sequestration aquifer formation in Missouri with acceptable permeability, porosity, extension, rock strength and water salinity. Using the finite …

Detecting And Locating Electronic Devices Using Their Unintended Electromagnetic Emissions, Colin Stagner

Doctoral Dissertations

"Electronically-initiated explosives can have unintended electromagnetic emissions which propagate through walls and sealed containers. These emissions, if properly characterized, enable the prompt and accurate detection of explosive threats. The following dissertation develops and evaluates techniques for detecting and locating common electronic initiators. The unintended emissions of radio receivers and microcontrollers are analyzed. These emissions are low-power radio signals that result from the device's normal operation. In the first section, it is demonstrated that arbitrary signals can be injected into a radio receiver's unintended emissions using a relatively weak stimulation signal. This effect is called stimulated emissions. The performance of stimulated …