Engineering Commons^™

Low Pressure Chemical Vapor Deposition Of Silicon Dioxide And Phosphosilicate Glass Thin Films, Vijayalakshmi Venkatesan

Theses

Silicon dioxide thin films were synthesized on silicon and quartz wafers using Ditertiarybutylsilane(DTBS) and oxygen as precursors. Trimethylphosphite (TMP) was injected to obtain phosphosilicate glass. The films were processed at different temperatures between 700°C and 850°C at a constant pressure, and at different flow ratios of the precursors. The films deposited were uniform, amorphous and the composition of the films varied with deposition temperature and precursor flow ratios. The deposition rate increased with increasing temperature and with increasing TMP flow rate. The stresses were very low tensile in the case of undoped silicon dioxide film and tended towards being less …

Real-Time Implementation Of An Adaptive Control System For A 3-Zone Rapid Thermal Processing Station, David Hur

Theses

In this thesis, the implementation details of a real time adaptive control system for a TI 3-zone RTP station, as well as the simulation and the experimental results are presented. Extensive simulation of the system is performed in order to ensure proper operation of the system. The experimental results are used to verify proper operation of the closed loop control system. Initial experiments were conducted using two thermocouples. Further experiments were conducted using one thermocouple for the purpose of testing the performance of the system using Extended Kalman Filter as the state estimator.

The implementation of the control system is …

Development Of A Gel Content Analysis Protocol For Ultra High Molecular Weight Polyethylene, Max Harold Jeanty

Theses

A modified procedure based upon ASTM (D 2765 - 90) to determine the gel content of crosslinked polyethylene plastics was developed. The new procedure was applied to ram extruded Ultra High Molecular Weight (UHMWPE) implant components processed under different manufacturing conditions. This new evaluation tool provides consistent results with greater accuracy and consistency compared to the American Society for the Testing of Materials (ASTM) method. Using the same tool, several relationships between the UHMWPE processing conditions and gel content were established. The amount of gel content is related to the crosslinked material. It has been shown that the more crosslinking …

Solidification/Stabilization Of Petroleum Contaminated Soils With Cold Mix Asphalt Concrete, Nazhat Aboobaker

Theses

In this research Petroleum Contaminated Soils (PCSs) are recycled in Cold Mix Asphalt (CMA), to produce a useful product that can control potential environmental threats. The stability, durability, and hydraulic conductivity are three important engineering parameters that need to be considered when using petroleum contaminated soils (PCSs) in cold mix asphalt (CMA). In this research, stability, durability, and hydraulic conductivity due to the addition of six different PCSs into CMA is investigated. The stability test were performed to determine if cold mix asphalt made with petroleum contaminated soil can withstand heavy traffic. The freeze-thaw, and wet-dry tests were performed to …

Removal Of Gasoline-Based Hydrocarbons By Vapor Permeation Membranes, Shivashanker Bagavandoss

Theses

Removal and recovery of evaporated lighter gasoline fractions can be effectively implemented by selectively permeating the hydrocarbons (HCs) and other volatile organic compounds (VOCs) from the vented air streams through nonporous hydrophobic polymeric membranes subjected to vacuum on the permeate side and then condensing these organics from the permeate. Such a vapor permeation process employing spiral-wound membranes has already been commercialized for VOCs. In this study, attention has been focused on removal of hydrocarbons from nitrogen flowing through the bore of microporous hydrophobic hollow fibers with a specially engineered nonporous silicone coating on the outside surface with a view to …

Synthesis And Characterization Of Silicon Dioxide Thin Films By Low Pressure Chemical Vapor Deposition Using Ditertiarybutylsilane And Oxygen, Sung-Jun Lee

Theses

This study is focused on the synthesis and characterization of silicon dioxide thin films deposited on silicon wafers by Low Pressure Chemical Vapor Deposition (LPCVD), using ditertiarybutylsilane (DTBS) as a precursor and oxygen as the oxidant. The dependence of film growth rate on various process parameters were studied. The growth rate was found to follow an Arrhenius curve with the variation in the temperature with an activation energy of 12.6 kcal/mol. The growth rate was found to be inversely proportional to the temperature in the range 550-750 °C. The refractive index and density were observed to be close to 1.47 …

Fuel-Rich Combustion Of Ethylene And Air In A Two Stage Turbulent Flow Reactor, Tara Byrnes Salem

Theses

This thesis presents experimental and modeling results from the combustion of ethylene and air in a two stage turbulent flow reactor. This work is motivated by the continuing concern over combustion by-products. The first half of the research effort focused on the validation of the reactor as a perfectly stirred reactor and a plug flow reactor (PSR+PFR) sequence. Using four detailed reaction mechanisms, measured concentrations of carbon oxides, oxygen, and light hydrocarbon concentrations were modeled. Within the accuracy of the data, the mechanism of Mao (1995) yielded the best results. However, it was observed that the success of the reactor …

Residual Stress Analysis Of Sputtered Tantalum Silicide Thin Film, Young Joo Song

Theses

The influence of different argon pressures on the residual stress, microstructure, and resisitivity of sputtered tantalum silicide thin films has been investigated. TaSi₂ films were deposited onto Si wafers by dc magnetron sputtering. The deposition temperature was assumed to be 300°C. The thickness was about 0.5 μm. The residual stresses in the films deposited at different argon pressures were determined by curvature measurement method. The compressive intrinsic stress of 1033.4MPa was measured at P_Ar = 0.5 mTorr. The intrinsic stress in the films seemed to change from compression to tension as P_Ar increased above 8mTorr. A maximum …

Implementation Of Fortran Finite Element Analysis Source Code With Application : Particle Deposition In A 90 Degree Duct Bend, Pantaleo Loiacono

Theses

Two FORTRAN 77 finite element analysis source codes, by 1.N. Reddy, were input into a PC, debugged, executed, and tested successfully. These programs are available to students interested in implementing a good finite element analysis source code on a PC or on a workstation in one or two dimensions. The programs can solve problems relating to heat transfer, stresses, beam analysis, frames, trusses, plane elasticity, plate bending, and laminar viscous incompressible fluids with various node and element combinations.

The two-dimensional program was used to obtain the velocity distributions in a 90 degree duct bend with incoming and exiting fully developed …

Relationship Between Precipitation, Surface Runoff, And Shallow Water-Table, Manoj Patel

Theses

In this study, a model was developed to describe the relationship between precipitation, surface runoff, and shallow groundwater table in a watershed that is subjected to groundwater extraction and urbanization. Regression analysis of fourteen years (1976-1989) of time series data for precipitation, stream discharge, ground water elevation, and groundwater extraction yielded good correlation between these parameters.

Analysis of the data associated with groundwater recharge and discharge events that occurred in the watershed from 1976 to 1989 yielded a high correlation between the above cited parameters. Regression analysis utilized to predict monthly variations in groundwater elevations showed a fair correlation between …

Study Of Stress In Microelectronic Materials By Photoelasticity, Hancheng Liang

Dissertations

The study of stress is playing an important role in microelectronic technology. In comparison with other techniques, the photoelasticity technique has the advantages of having high spatial resolution and high sensitivity. It can be used in qualitative observation in real-time and quantitative determination of stress distribution in the microelectronic materials and devices.

This dissertation presents a systematic study of photoelastic stress analysis in microelectronic materials and devices, ranged from theoretical study to practical system setup, from measurement methods to their applications. At first, based on the detailed survey on the piezo-optic properties of the crystals used in microelectronics, we apply …

Reaction Kinetics Of Methanol And Mtbe Oxidation And Pyrolysis, Wen-Chiun Ing

Dissertations

This study presents experimental data on the decomposition of methanol in several different reaction environments - fuel lean to stoichiometric at a temperature range of 873 and 1073 K and a pressure range of I and 5 atm. Methane fuel is also added in several of the systems studied in order to provide experimental data to understand the methanol addition effect on the methane oxidation.

Computer codes: ThermCal, ThermSrt and ThermCvt have been developed for the thermal property calculations of stable molecules by the Benson group additivity method and of radicals by the NJIT hydrogen bond increment method.

Pressure dependent …

Experimental And Analytical Investigation Of Waterjet Cleaning Process, Ping Meng

Dissertations

This doctoral dissertation is concerned with the development of water based cleaning technology required by industry which may substitute the traditional approach based upon the use of various chemical cleansers.

The experimental study involves the waterjet removal of various coatings (rust, oil and epoxy based paints, etc.). Cleaning was carried out under a wide range of operational and geometrical conditions (standoff distance, travel speed, water pressure, diameters of sapphire nozzle and focusing tube, nozzle body type). A new designed spiral nozzle body was tested in this work. The use of surfactant was also investigated. Microscope and SEM surface were used …

Characterization And Fabrication Of A (6h)-Sic As A Piezoresistive Pressure Sensor For High Temperature Applications, Robert Sylvester Okojie

Dissertations

A prototype monolithic 6H-SiC pressure sensor operational up to 350°C, with potential to operate up to 600°C, was batch fabricated and tested. At temperatures higher than 450°C, silicon diaphragms creep under minimal load. To operate beyond 450°C, therefore, the use of 6H-SiC was proposed. However, three key technological issues - fabrication, high temperature metallization, and gage factor characterization - had to be resolved. Since conventional fabrication technology is not applicable to SiC due to its near inert chemistry, photoconductive selectivity techniques to etch the piezoresistors were developed. Techniques to wet etch the cavities in a dark current mode were developed, …

Experimental And Numerical Investigation Of Abrasive Waterjet Polishing Technology, Fenggang Li

Dissertations

The objective of this investigation is the development of the abrasive waterjet (AWJ) based polishing technology. The result of the investigation will assist the implementation of AWJ polishing for manufacturing processes and procedures.

Experimental exploration of AWl polishing involving processing of difficultmachine materials such as Alumina ceramic and stainless steel. Surface improvement due to this processing is evaluated by measuring the roughness of the generated surfaces and examining the microhardness and micro-topography of the surfaces using Scanning Electronic Microscopy (SEM). The surface roughness of 0.3 micron was obtained at samples of ceramic and metal alloys at a reasonable rate using …

The Constant Fracture Angle Model For Cementitious Materials, Suk Ki Kim

Dissertations

Fracture mechanics of concrete has been investigated for the past two decades using linear elastic and nonlinear fracture mechanics concepts. The models proposed so far remain questionable largely due to specimen dependency of the proposed fracture parameters.

In this study, a new approach for modeling the fracture characteristics of concrete and fiber reinforced concrete is proposed. The model depends on the load CMOD relationship rather than the traditional load-deflection principle. Although energy consumed during fracture is definitely a direct function of the load displacement response, it was observed that traditional displacement measurement included an extraneous and erratic portion due to …

Emulsion Liquid Membrane Removal Of Arsenic And Strontium From Wastewater : An Experimental And Theoretical Study, Ding-Wei Zhou

Dissertations

The emulsion liquid membrane (ELM) technique has been successfully applied on the removal of arsenic (As) from metallurgical wastewater and the removal of strontium (Sr) horn radioactive wastewater. This study consisted of experimental work and mathematical modeling.

Extraction of arsenic by an emulsion liquid membrane was firstly investigated. The liquid membrane used was composed of 2-ethylhexyl alcohol (2EHA) as the extractant, ECA436OJ as the surfactant, and Exxsol D-8O solvent (or heptane) the diluent. The sulfuric acid and sodium hydroxide solutions were use I as the external and internal phases, respectively. The arsenic removal efficiency reached 92% within 15 minutes in …

Explicit Congestion Control Algorithms For Available Bit Rate Services In Asynchronous Transfer Mode Networks, Ambalavanar Arulambalam

Dissertations

Congestion control of available bit rate (ABR) services in asynchronous transfer mode (ATM) networks has been the recent focus of the ATM Forum. The focus of this dissertation is to study the impact of queueing disciplines on ABR service congestion control, and to develop an explicit rate control algorithm.

Two queueing disciplines, namely, First-In-First-Out (FIFO) and per-VC (virtual connection) queueing, are examined. Performance in terms of fairness, throughput, cell loss rate, buffer size and network utilization are benchmarked via extensive simulations. Implementation complexity analysis and trade-offs associated with each queueing implementation are addressed. Contrary to the common belief, our investigation …

Design, Process And Performance Simulation Of A 360x360-Element Very High Frame Rate Burst-Image Sensor, Guang Yang

Dissertations

A process was developed for fabrication of 360x360-element Very High Frame Rate (VHFR) burst-image sensor on the bases of one-dimensional (1-D) and two-dimensional (2-D) device and process simulations using SUPREM III, SUPREM IV, PISCES IIB and ISE-TCAD software, and the process data provided by the David Sarnoff Research Center. This process includes SiO₂-Si₃N₄ gate dielectric, four-levels of polysilicon, three-levels of metal, eight implants, and requires twenty-one mask levels. The imagers with a 2-cmx2-cm chip size were fabricated at the David Sarnoff Research Center. The VHFR burst-image sensor is capable of capturing images at frame rates …

Global Fuzzy Control Based On Cell Mapping, Tea-Quin Kim

Dissertations

Cell mapping methods can generate global optimal controls for nonlinear dynamic systems. However, the implementation of this approach for on-line control is difficult due to its use of a table-based controller which requires a large amount of memory.

In this dissertation, a cell mapping based systematic method is developed to construct a fuzzy controller to replace the table-based controller for global optimal control of dynamic systems. The method consists of four steps: 1) An optimal control table is generated using a cell mapping algorithm. 2) The cells are linked into trajectories to characterize the optimal dynamic evolution of various cell. …

Development Of A Traffic Safety Index For Urban Intersections, Jae-Hong Kang

Dissertations

Conventional safety analysis focuses on the accident environment at specific locations or a limited segment of highways or arterials, and attempts to identify the effects of accident contributing factors. The development of a safety index in the past was based on a statistical summary for county or statewide areas, using general indicators such as population, number of registered vehicles, vehicle miles traveled and so on. This research effort presents a state-of-the-art procedural analytical approach for the safety analysis of Manhattan intersections that are exposed to a unique urban environment. The computed index provides safety ratings that can identify potential safety …

Development Of A Multivariate Qsar Model To Predict Desorption Of Halogenated Aliphatic Hydrocarbons From Activated Sludge Solids, Sudhi Ranjan Mukherjee

Dissertations

Data collected from different wastewater treatment processes have provided statistically significant evidence that many toxic organic contaminants on EPA's list of priority pollutants concentrate several orders of magnitude greater than influent concentrations in industrial and municipal wastewater sludges. Because of the reversibility of sorption processes, it is possible for sorbed organic compounds to desorb at a later time, hence making disposal of these sludges a potential problem. Although a number of models have been developed to predict sorption parameters, they have all been based on empirically derived descriptors whose validity is seriously compromised by the variation in available data for …

A Full Wave Method For Rough Surface Scattering Using Fictitious Current Distributions, Anthony A. Triolo

Dissertations

Rough surface scattering is a current topic of interest in many diverse fields. But, despite its importance, the two most widely used solution methods, the Kirchhoff and first order perturbation methods, are valid only for a restricted range of surface types. There is a large range of surface statistics for which neither of these theories is valid. There are purely numerical solutions to the problem, i.e., the integral equation technique and FDTD method, but these methods require a prohibitively large amount of computer time and storage space for use in practical applications. A full wave method has been introduced by …

Reduction Of Inertia-Induced Forces In A General Spatial Mechanism, Sahidur Rahman

Dissertations

A computer-aided design procedure has been developed for minimizing the adverse effects of the inertia-induced forces by optimum mass redistribution amongst the links of high speed general spatial linkages. The evaluation of an optimality criterion for the mass redistribution of the mechanism will be carried out with the aid of a quadratic programming technique. This has been found to be successful in minimizing inertia induced forces and torques. The validity of the optimization procedure will be demonstrated by application to one kind of spatial linkage.

No literature has been found on the balancing of a general spatial mechanism, since its …

Discrete Element Modeling Of Dry Granular Material Using A Massively Parallel Supercomputer, David W. Washington

Dissertations

It is the state-of -the-art within Geotechnical Engineering to model soils as systems of particles rather than using the traditional continuum approach. Simulating these systems of particles for geotechnical boundary value problems results in systems which are of necessity large, motivating the application of massively parallel supercomputers. This thesis pursues such an approach.

The following work describes numerical experiments using a Discrete Element Method (DEM) paradigm for soils (Trubal) together with massively parallel computers with Single Instruction Multiple Data (SIMD) architecture. The discrete element method describes the behavior of granular assemblies using the classical mechanics of discrete bodies. The computational …

Relay Ladder Logic And Petri Nets For Discrete Event Control Design : A Comparative Study, Edward Twiss

Theses

In the 1960's and earlier discrete event systems (DES) were controlled by hardwired electromechanical relay systems. In 1969 an electronic programmable logic controller (PLC) was introduced. PLC's have been programmed utilizing relay ladder logic (RLL). RLL is a graphical programming language with software "devices" used to emulate electromechanical devices. RLL programs, however, often become large and difficult to understand because its graphical representation of physical switching devices obscures the discrete event dynamics inherent in the process to be controlled. Petri nets are a methodology for modeling discrete event systems (DES). Using a Petri net based controller, a control strategy could …

Simple Fast Vector Quantization Of The Line Spectral Frequencies, Jin Zhou

Theses

Speech coding has been of interest to communication specialists for years. A number of technologies for describing and transmitting the speech spectral envelope have been studied. Among them, the Vector Quantization (VQ) of Line Spectral Frequencies (LSF) is receiving more attention because of its good rate-distortion performance. Typically, about 30 bits are assigned to code 10-dimensional LSF vectors with a resulting spectral distortion of less than ldB. However, 30-bit full-search VQ is totally impractical in terms of both computational complexity and memory space. Various standard suboptimal, low-complexity VQ techniques have been used for coding the LSF's in the literature. The …

A Mathematical Model Of Cardiovascular System With Feedback Control, Jiayu Gu

Theses

A mathematical model of human cardiovascular system is presented in this study. The closed-loop model is composed of twenty compartments which includes the left and right ventricles, and the systemic and pulmonary circulations. Two physiologic feedback control mechanisms, autoregulation of blood flow and baroreceptor reflex regulation of arterial pressure, are incorporated in the model. Autoregulation acts by changing local resistance to blood flow through metabolic and myogenic mechanisms, thereby insuring a match between oxygen supply and demand for any tissue or organ. Baroreceptors act through neural pathways to alter heart rate, contractility and peripheral resistance in order to return sudden …

Measurement Of The Electroencephalogram (Eeg) Coherence, Atmospheric Noise, And Schumann Resonances In Group Meditation, Douglas A. Newandee

Theses

Electrical activity in the human body was investigated using EEG and ECG measurements while subjects remained with eyes open, eyes closed and in a meditation state. During these measurements, additional antennas were attached to the equipment to record atmospheric noise and signal activity simultaneously. The obtained data was analyzed and various observations were made. Processed data based on antenna signals clearly showed the presence of man-made signals, having narrow spectral widths that could be treated as atmospheric noise in the frequency range up to 50 Hz. In addition, signals clustered around 7.8, 14.1, 20.3, 26.4, and 32.5 Hz were observed …

Comparison Of Different Signal Processing Algorithms To Extract The Respiration Waveform From The Ecg, David J. Caggiano

Theses

Power spectral analysis of heart rate variability is a powerful tool to measure the activity of the parasympathetic division of the autonomic nervous system noninvasively. To determine the parasympathetic activity, the frequency of respiration must be known. However, during ambulatory studies, the frequency of respiration is not acquired. To alleviate this problem, methods have been proposed in the past to derive the respiration from the ECG. Unfortunately, these previous methods are unreliable if the subject's breathing rate is uncontrolled. In this study, four methods to derive the respiration waveform from the electrocardiogram (ECG) were developed. Two leads of ECG and …