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The Effect Of The Rolling Load On The Micro-Structure Of Low Carbon Sheet Steel, Jerry Lee Cadden

Masters Theses

"A Stanat 315, two high-four high, combination rolling mill is used to cold roll annealed, low carbon steel strips. A method of measuring the rolling load was presented. The method consisted of constructing a load cell using SR-4 strain gages attached to a steel column. The load cell was placed under the hold down screw of the rolling mill and a known load was applied. The stresses from this load were transferred to the mill housing where another SR-4 strain gage was located. The strain in the mill housing was recorded at the corresponding applied load. During rolling, the strain …

Experimental Stress Analysis Of Bolts In A Flange Coupling, Vijay Rastogi

Masters Theses

"In this investigation an attempt has been made to determine simple formulae leading to a better, more useful and much safer design of flange coupling bolts. The bolts were tested under tensile loading and bending and hence the results obtained apply for bolts under these modes of loading only.

The behavior of flange bolts under different initial tightening torques was studied by measuring strains in a bolt on which strain gages had been attached* . From this, the load producing separation of flanges, under different tightening torques, was determined and used in deriving formulae for prediction of the load for …

Neutron Flux Mapping Of The Msm Reactor, Cary Chow-Yuen Chen

Masters Theses

"This investigation presents a mean to determine thermal neutron flux of a reactor by irradiating copper wires inside the fuel elements. The activity recorded after decay correction, is the relative thermal neutron density. Thermal neutron flux is a measure of the neutron density at thermal energy, 0.025 ev.

Gold foils irradiated at National Bureau of Standards were used as the absolute neutron flux calibration standards. The average flux of the reactor with water as the reflector ranges from 7.24 x 10¹⁰ neutrons/cm² - sec. to 7.87 x 10¹⁰ neutrons/cm² - sec. as obtained from the calculations. …

A Determination Of Vapor Pressure Of Barium In The Thermal Production Of Barium Metal, Thomas A. Theobald

Masters Theses

The Knudsen effusion method was used to find the equilibrium reaction pressure of barium for the following reactions:
4BaO + 2Al - 3Ba + BaO·Al₂O₃ (l)
4BaO + Si - 2Ba + 2BaO·SiO₂ (2).
The resulting barium pressure for reaction (l) ranged from 0.27 mm. Hg to 1.77 mm. Hg in a temperature range of 940°C to 1086°C. The barium pressures for reaction (2) varied from 0.38 mm. Hg to 1.94 mm. Hg in a temperature range of 1000°C to 1086°C. The free energies of formation of BaO·Al₂O₃ and 2BaO·SiO₂ at 1087°C …

Thermal Conductometer For Liquids, Yuan-Kai Chang

Masters Theses

"The published data pertaining to the thermal conductivity of liquids are of such a character that it is very difficult to determine from them the correct value, or the temperature coefficient for any liquid.

Most of the published values of thermal conductivity for liquids are evaluated at one particular temperature. It is the purpose of this investigation to design, construct and calibrate a thermal conductometer for liquids over a temperature range of 30°F to 200°F.

Since water and glycerol were the only liquids found by this investigator with published data on their conductivities as a function of temperature, they were …

A Study Of The Chemical Kinetics, Activation Energy And Difference Effect On Beryllium Dissolving In Mineral Acids, Daniel Santhamurthi Gnanamuthu

Masters Theses

"The rate of dissolution of polycrystalline beryllium was studied in hydrofluoric, hydrochloric and sulfuric acids. Two samples of beryllium containing different amounts of beryllium oxide were used. The experiments were performed at temperatures ranging from 20 to 50°C, and at various acid concentrations. The kinetics of these heterogeneous processes conformed to a reaction order of approximately one in all the cases. Since the conditions of the surface were complex during dissolution, these might complicate the reaction. This might be due to the oxide layer, which is present as impurity.

The difference effect was determined at various acid concentrations at 25°C …

A Study Of The Colloidal Properties Of Zirconium And Promethium By Electrodialysis And Liquid-Liquid Extraction, James N. Click

Masters Theses

"The purpose of this investigation was to study the solution chemistry of zirconium by investigating the colloidal behavior of natural zirconium and zirconium-95, utilizing electrodialysis and liquid-liquid extraction techniques. Also incorporated into this study was the investigation of optimum conditions for the extraction of the natural zirconium and zirconium-95 with thenoyl trifluoracetone. A limited amount of work was done on the colloidal nature of promethium-147"--Introduction, pages 2-3.

A Study Of Several Commercial Steels In The Red Short Range, Jorge Alberto Espana

Masters Theses

"The red short phenomenon present in steel, was studied by means of torsion tests at temperatures between 800 and 1200⁰C. Cold drawn bars of different compositions of steels were tested, and the number of turns to failure and maximum twisting torque were plotted versus temperature.

All the steels tested, exhibited to have a certain degree of red shortness. By comparing the curves and the respective chemical analyses, the detrimental effect of sulphur and lead and the beneficial effect of manganese, was established.

Microscopic examinations revealed the intergranular nature of the cracks in the red short range. Sulphur and oxide distribution …

A Study Of Heat Transfer Coefficients On Cylindrical Pipe In Turbulent Flow, Dennie Lee Adkins

Masters Theses

"This thesis represents a study of the effects of turbulent motion on heat transfer coefficients on cylindrical pipe.

The turbulent motion was created by cutting transverse slots in a spiral configuration along the pipe length.

An induction heater was used for the heat source and water as the cooling medium. The water was conducted over the pipe surface and through the slots.

This caused the laminar layer along the pipe surface to be broken up and an increase in the heat transfer coefficient was experienced.

The main objective of this test was to find if a relation existed between the …

Circular Arch Analysis, Aylmer Pao-Sheng Cheng

Masters Theses

"This work presents an analysis of a two-hinged circular arch by both the elastic theory and the deflection theory. The basic assumption made in this analysis was that the moment of inertia of the arch rib and the normal force vary as the secant of the angle with respect to the crown. The increase of maximum moment as found by the deflection theory was in the range of 30%"--Abstract, page 2.

Syntheses And X-Ray Investigations Within The System Fes₂-Cos₂, Samuel Shu Mou Chan

Masters Theses

"Pyrite (FeS₂), cattierite (CoS₂), and various transitional members of the solid solution compounds were prepared. The methods used are as follows:

First, sulfides of cobalt, iron, or cobalt-iron were obtained by precipitation from a mixture of the cobalt chloride and/or ferrous sulfate in an aqueous solution. The dried precipitates were then mixed with an equal weight amount of sulfur and placed into silica glass tubes. After evacuation, they were filled with hydrogen gas of 3/4 of atmospheric pressure and sealed. The samples were then heated up to 500°C (for FeS₂), 650°C (for FeS_{2 …}

A Survey Of The Influence Of Selected Sulfides On The Thermal Decomposition Rate Of Zinc Sulfate, L. G. Twidwell

Masters Theses

"The influence which ZnS, CdS, Cu₂S, PbS, and FeS has on the thermal decomposition rate of ZnSO₄ was studied by measuring the SO₂ gas evolved per unit of time for various ZnSO₄-MeS mixtures at 600°C, and analyzing the solid phases by means of X-ray diffraction patterns.

The SO₂ gas evolved upon heating the pellets was analyzed as a function of time by absorbing the gas in a solution of distilled water, H₂O₂, and NaOH, and measuring the time required for the SO₂ to neutralize the NaOH. The gas …

The Experimental Determination And Prediction Of Ternary-Liquid Equilibria Data, Risdon William Hankinson

Masters Theses

"Although the field of liquid extraction is of increasing importance in today's chemical industry, the ternary-liquid data so necessary to the design and study of extraction operations are available in the literature only to a limited extent. During the twentieth century, approximately 120 ternary-liquid systems have been studied. However, limiting solubility data have been reported for approximately one-third of these systems, and about 30 per cent of the equilibria data reported for the remainder of these systems are incomplete or inaccurate.

Within limits, liquid equilibria data may be calculated for a ternary system from the properties of its constituents which …

Model Analysis By The Moiré Method, David D. Kick

Masters Theses

"This study presents the use of Moiré fringes for model analysis of deflections and strains. Deflection of a beam, strain in a disk, and an Influence diagram for a frame are presented as examples of uses of the Moiré method. The necessary equations for the determination of strain using the Moiré method are also derived and presented in this work"--Abstract, page v.

A Study Of A Second-Order Predictive Control System, Tarkeshwar Singh

Masters Theses

"The purpose of this thesis is the study of a predictive control system by simulating it on an analog computer. Logic criteria for step reference inputs are derived by the phase- plane technique, and tie corresponding logic network designed to bring the error and error rate of the controlled system toward zero in the least possible time.

The responses of the predictive control system for step, ramp, sinusoidal and exponential reference inputs are investigated with primary emphasis placed on the rise time and overshoot for several values of step inputs of the reference.

Finally, recommendations are made for further investigations …

A Study Of The Behavior Of Zirconium In Aqueous Solutions And The Separation Of Radioactive Zirconium By Electrodialysis, Charles William Brauer Jr.

Masters Theses

"Nuclear reactor installations designed for power production must of necessity operate at higher energy levels than their experimental precursors. As these facilities increase in number, better solutions must be found for both technical and economic problems.

The disposal of waste materials is of primary importance and will require greater effort if satisfactory disposal methods are to keep pace with the increase of waste materials, produced by the increasing number of new nuclear facilities. The radioactive materials present in this waste material may constitute a valuable by-product from these operations if suitable and economic recovery procedures are developed. If the development …

An Evaluation Of State Mineral Taxation In Missouri, Jerry Wayne Huffman

Masters Theses

"A study was made to evaluate the present taxes levied on the mineral industry in the State of Missouri. The corporate income tax, corporate franchise tax, and general property taxes were examined, in addition to the mine inspection fees and methods of local assessment of mineral properties.

It is suggested that the State of Missouri revise the method of application of the general property tax to mineral properties. Utilization of the principle of taxation of future profits and employment of qualified appraisers would provide a more equitable application of the general property tax.

It is recommended that the present mine …

Investigation And Development Of Ground Water Of Chalone Creek, (Pinnacles National Monument, California), Donald Lee Brown

Masters Theses

"The Pinnacles National Monument is located in San Benito and Monterey Counties about 130 highway miles south of San Francisco, California. Because of unusual patterns in volcanic rocks, the Monument was set aside as a recreation area on January 16, 1908, by President Theodore Roosevelt. It encompasses an area of approximately 12,818 acres.

Water quality and supply problems were experienced at the Monument in the few years prior to 1961. In 1961, a collection trench system was installed to alleviate the water supply condition. A horizontal trench system, 215 feet long and four feet below the dry season water table, …

A Correlation Of Heat Transfer Coefficients Using An Induction Heater, Charles Maurice Martin

Masters Theses

"This thesis represents a study of the following problems. (1) Determination of techniques and equipment which would give satisfactory correlation of experimental heat transfer coefficients with those obtained from acceptable heat transfer equations when using an induction heater as the heat source. (2) Determination of depth of energy deposition in a thick-walled tube due to induction heating.

Techniques were developed that gave a correlation between experimental and calculated coefficients that were within -5% for minimum flow and +8% for maximum flow.

Because of difficulties in positioning thermocouples, the depth of energy deposition could not be accurately determined. However, two surface …

Development Of A Simple Bar Method Thermal Conductivity Test, V. J. Flanigan

Masters Theses

"A linear flow bar method type apparatus was set up for finding thermal conductivities by comparison techniques. Comparison technique consist of using a standard specimen where the thermal conductivity is known and comparing it to the unknown specimens to find their conductivity. Apparatus of this type usually uses thermocouples for the required temperature measurements, but thermistors were used in this experiment. The thermistors used required calibration to measure accurate temperatures and this was accomplished by using the known temperatures of the changes of state of some common materials. Five alloys were used to evaluate the method: SAE 1020 steel, gray …

Velocity Distribution Induced By Free Jet Impact On A Stilling Basin, Sedat Özkol

Masters Theses

"At present, the use of the free jet impacting on a stilling basin as an energy dissipator is not very common, as there is very little information available concerning this particular field. However, if conditions are favorable, this type of energy dissipator will be quite economical to construct.

In this paper it was found that the hydraulic behavior of the free jet impacting on a stilling basin can be determined to a degree which may be considered accurate for practical purposes. It was also shown that given the free jet velocity, the magnitudes of the velocities at the critical points …

Transpiration Cooling Of A Porous Plate, Stephan A. Sayegh

Masters Theses

"Transpiration cooling has long been known as an effective way of removing heat from porous materials. This thesis is a new approach to one of the problems of transpiration cooling in the steady state.

The specific problem considered here is that of a uniform porous plate through which a liquid is forced. This liquid vaporizes at a short distance from the surface through which it is forced and leaves the porous plate at the other surface which is exposed to hot gases. It also protects the hot surface by forming an insulating layer between that surface and the hot gases. …

Analysis Of Flat Plates By Reaction Distribution Method, David D. W. Yang

Masters Theses

"This study was made to analyze rectangular flat plates by the method of Reaction Distribution and to compare results obtained by this method with that of other methods. The basic approach is to divide the plate into an equivalent grid system and introduce temporary supports at the intersecting joints. The results from this study shows that the Reaction Distribution method is useful in a qualitative analysis of the behavior in a plate but is less satisfactory in obtaining reliable quantitative results"--Abstract, page 2.

A Study Of The Permeability And Separation Of Carbon Dioxide And Hydrogen By Gaseous Diffusion Employing Barriers Of Polystyrene, Carl J. Wallace

Masters Theses

"The purpose of this investigation was to study the permeability and separation of carbon dioxide and hydrogen by gaseous diffusion employing barriers of polystyrene. The offset of temperature and barrier thickness on the permeability and separation of carbon dioxide and hydrogen wore Investigated for barriers of one, three, and five-mil thicknesses and for temperatures of 26, 35, 45, and 50 degrees centigrade.

With an increase in barrier thickness of one to five- mils, the permeability of carbon dioxide decreased to one-fourth of its value at the one-mil thickness. The hydrogen permeability decreased to approximately two- thirds of its value at …

A Study Of Placer Tin Materials From Southern Thailand, Somkiat Ganthavee

Masters Theses

"This thesis deals with a series of investigations of placer tin samples from a Chinteik's Tin-dredge, Gnaw District, Ranong Province, and the Tin-Pet mine, Phang-gna Province, in southern Thailand.

A brief summary of the geography and geology of Thailand as a whole has been given as a general introduction to the source of the materials studied in this thesis.

The results of sieve analyses have shown that the sluice boxes do not effectively concentrate the cassiterite grain below 0.147 mm. from the rough concentrate treated in the tin-dressing shed.

It has been found that roundness and shape determinations of quartz …

Transpiration Cooling Of A Heat Generating Porous Plate, M. K. A. Hameed

Masters Theses

"This investigation is a continuation of a thesis by T. S. Purewal. Several of the simplifying assumptions made by the above author are either ignored or the justifiability of such assumptions is probed into in order to obtain a more rigorous solution. Effects of the assorted grain size, non-Newtonian cooling, direction of coolant flow, thickness of the porous heat generating plate, specific heat of the coolant, and compressibility of the coolant are investigated in this thesis. Variation of maximum temperature of both coolant and the solid material for different types of heat source distribution are also studied.

As the grain …

Statistical Analysis Of Fracture Stresses Of Triaxial Porcelain Bodies, Robert E. Moore

Doctoral Dissertations

"Triaxial porcelain bodies containing various forms of silica, quartz, cristobalite and fused silica, were strength tested in bending. Significance tests were employed to discern real differences in the strength sample statistics caused by the various forms of silica. Firings were performed at three temperature levels. The differences in strength sample statistics were correlated to the microstructures of these silica porcelains.

A triaxial alumina porcelain body was employed as a model brittle solid for a study of the effect of flaw density on mean fracture stress. The flaws were introduced in the form of large diameter (d̄ = 115 microns) rounded …

An Investigation Of The Deformation Textures Of Cobalt, Roy Carl Wilcox

Doctoral Dissertations

"Deformation textures of various cobalt structures as a result of cold rolling together with some annealing textures were studied. The textures of cobalt were determined using a modification of the Schulz-Decker Geiger counter technique. Pole figures of the (1011), (0001) and (1010) planes were constructed. Also, a study of the microhardness of cobalt was made.

Microhardness tests were performed on various cobalt structures, in both the cold rolled and unworked conditions. The microhardness was found to vary with the source of the cobalt, the crystal orientation, and the amount of deformation and twinning. Deformation lines about the hardness impressions diffused …

Lattice Parameters, Densities And Imperfections In Indium And Indium-Cadmium Alloys Rich In Indium, Paluri Bhimeswara Rao

Doctoral Dissertations

"An investigation of perfection of the structure of the indium-cadmium system was suggested by the interesting properties of indium and its cadmium alloys. The lattice of indium, though tetragonal, may be considered as distorted cubic, its axial ratio being 1.0767 at 20°C. Furthermore earlier studies have revealed a transformation of the tetragonal structure to cubic in the presence of cadmium.

To determine the perfection or soundness of the indium and indium-cadmium alloys rich in indium, pure indium (99.999 per cent purity) and eight samples of the indium-cadmium alloys ranging in composition from 2.977 to 10.015 per cent by weight of …

The Geology Of The Eldorado Mining District, Clark County, Nevada, Spenst M. Hansen

Doctoral Dissertations

The rocks of the Eldorado mining district, Clark County, Nevada, are of Precambrian, Tertiary and Quaternary age. Precambrian rocks include a heterogeneous series of gneisses and schists, younger garnetiferous granite gneiss and a youngest group of pegmatites. Paleozoic and Mesozoic rocks present in surrounding areas are absent in the district and Tertiary volcanics lie directly on the Pre- cambrian basement. Tertiary rocks consist of middle to late Tertiary flows and pyroclastic beds of andesite, basalt and rhyolite. These are assigned to three volcanic formations: the Patsy Mine volcanics; the Golden Door volcanics; and the Mount Davis volcanics. The Patsy Mine …