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The Twiggs Clay: Mineralogy, Origin, And Industrial Properties Of An Upper Eocene Opaline Claystone In The Coastal Plain Province Of Georgia, U.S., Lori G. Eversull Jan 2005

The Twiggs Clay: Mineralogy, Origin, And Industrial Properties Of An Upper Eocene Opaline Claystone In The Coastal Plain Province Of Georgia, U.S., Lori G. Eversull

LSU Doctoral Dissertations

The Twiggs Clay is an upper Eocene claystone found as discontinuous deposits downdip of the Fall Line in the Coastal Plain Province of eastern and central Georgia. A distinctive facies of the Twiggs is found in two lenses near the town of Wrens. The nature, origin, and potential commercial application of this resource are examined. Four strata and two mineralogic assemblages are recognized in the Wrens deposit. The lower three strata are near white in color and very low in density. These strata are mineralogically similar and are composed predominantly of disordered silica and smectite. The smectite is dioctahedral, and …

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Sulfur And Oxygen Isotope Characterization Of An Eocene Playa Deposit, Northern High Plains, And Rainwater Sulfate, Baton Rouge, Usa, Kathryn Ann Jenkins Jan 2005

Sulfur And Oxygen Isotope Characterization Of An Eocene Playa Deposit, Northern High Plains, And Rainwater Sulfate, Baton Rouge, Usa, Kathryn Ann Jenkins

LSU Master's Theses

This thesis is composed of two independent chapters which are linked through the application of multiple stable isotope measurements of sulfate. Chapter 1 compares two Cenozoic playa deposits in the northern High Plains. Anomalous playa sulfate was discovered at Scotts Bluff which is speculated to have originated via the oxidation of volcanically emitted reduced sulfur gases. A question arises, then, is a volcanic origin of sulfate common for other Cenozoic playa deposits in the region. A complete stable isotope characterization was performed on the gypsum sulfate collected at Wolf Butte (nearby apparent playa setting) to determine if the sulfate has …

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Simulation Study For Wireless Sensor Networks And Load Sharing Routing Protocol To Increase Network Life And Connectivity, Ankur Suri Jan 2005

Simulation Study For Wireless Sensor Networks And Load Sharing Routing Protocol To Increase Network Life And Connectivity, Ankur Suri

LSU Master's Theses

LSU SensorSimulator is a framework for simulating wireless sensor networks. It is a customizable and extendible simulator, which allows testing and analyzing software for wireless sensor networks. The users can subclass the framework classes and customize the behavior of various network layers. This subclassing gives a way to the developers an opportunity to analyze and investigate, phenomenological, networking, robustness and scaling issues, to explore arbitrary algorithms for distributed sensors, independent of hardware constraint. The results are compared against the simulation results for ns-2 for routing protocols Directed Diffusion and GEAR. Through the comparison of results for scalability, performance and memory …

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Musculoskeletal Disorders In Dentistry, Frank Maurice Pitts Jan 2005

Musculoskeletal Disorders In Dentistry, Frank Maurice Pitts

LSU Master's Theses

Because of the common occurrence of pain experienced by dental professionals during the course of a workday and throughout their career, an epidemiological and a field study were performed in an effort to contribute to the prevention of musculoskeletal disorders in dentistry. The aim of the thesis is two fold: to assess the perception of occupational pain and discomfort felt by dentists through a perception based survey and to assess the muscle behavior of dentists during isotonic postures while performing various dental procedures on their first and last patients in a given work day. One hundred (100) dentists participated in …

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Environmental Benefits Realized From Eradication Of The Non-Indigenous Insect Anthonomus Grandis Boheman, The Cotton Boll Weevil, Marc Stephen Bordelon Jan 2005

Environmental Benefits Realized From Eradication Of The Non-Indigenous Insect Anthonomus Grandis Boheman, The Cotton Boll Weevil, Marc Stephen Bordelon

LSU Master's Theses

At least one third of the insecticide used in agriculture has been used to control the boll weevil in cotton. Historically, these insecticides have been toxic to humans and harsh on the environment. In addition, the intensive use of chemical insecticides to control the boll weevil results in the disruption of naturally occurring biological control factors that regulate other insect pest populations causing a chain reaction of secondary pest populations that require treatment followed by resurgence and repeat treatment. This situation has resulted in the development of resistance to insecticides, high control costs and unacceptable levels of chemical insecticide contamination …

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An Analysis Of The Variables That Influence A Country's Decision To Ratify The Stockholm Convention On Persistent Organic Pollutants, Tokesha Marie Collins Jan 2005

An Analysis Of The Variables That Influence A Country's Decision To Ratify The Stockholm Convention On Persistent Organic Pollutants, Tokesha Marie Collins

LSU Master's Theses

The objective of this thesis is to identify key factors that influence a country to ratify the Persistent Organic Pollutants (POPs) Treaty. The POPs treaty seeks to eliminate or reduce the emissions of 12 POPs. I will examine the links between the countries that have ratified the POPs treaty in an effort to identify variables that may have influenced a country's decision to ratify the treaty. For each of the 165 nations in my dataset, I will examine economic, social, geographic, health, and political indicators and history of malaria and determine if a relationship exists between these variables and treaty …

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Diagenesis Of Mudstones, Offshore Texas And Southwestern Louisiana, Maria Antonieta Pacheco Jan 2005

Diagenesis Of Mudstones, Offshore Texas And Southwestern Louisiana, Maria Antonieta Pacheco

LSU Master's Theses

Predicting the effects of mudstone diagenesis on reservoir quality is an important component of successful petroleum exploration and production programs. A regional study using chemical analyses from mudstone core cuttings and SP logs from 15 wells from the western Gulf of Mexico, including the Matagorda, Brazos, Mustang offshore areas, indicates that chemical changes with depth such as overall depletion of quartz and calcite; the illite-smectite conversion; and K2O enrichment occur in the mudstone Miocene interval of the study area. Mixing of depositional sources has been suggested to be the cause of similar chemical and mineralogical changes observed in Paleocene-Eocene and …

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Quasicontinuous Derivatives And Viscosity Functions, Rodica Cazacu Jan 2005

Quasicontinuous Derivatives And Viscosity Functions, Rodica Cazacu

LSU Doctoral Dissertations

In this work we demonstrate how the continuous domain theory can be applied to the theory of nonlinear optimization, particularly to the theory of viscosity solutions. We consider finding the viscosity solution for the Hamilton-Jacobi equation H(x, y) = g(x), with continuous hamiltonian, but with possibly discontinuous right-hand side. We begin by finding a new function space Q(X,L), the space of equivalence classes of quasicontinuous functions from a locally compact set X to a bicontinuous lattice L and we will define on Q(X,L) the qo-topology, which is a variant of classical order topology defined on complete lattices. On this …

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Interference Suppression And Parameter Estimation In Wireless Communication Systems Over Time-Varing Multipath Fading Channels, Jianqiang He Jan 2005

Interference Suppression And Parameter Estimation In Wireless Communication Systems Over Time-Varing Multipath Fading Channels, Jianqiang He

LSU Doctoral Dissertations

This dissertation focuses on providing solutions to two of the most important problems in wireless communication systems design, namely, 1) the interference suppression, and 2) the channel parameter estimation in wireless communication systems over time-varying multipath fading channels. We first study the interference suppression problem in various communication systems under a unified multirate transmultiplexer model. A state-space approach that achieves the optimal realizable equalization (suppression of inter-symbol interference) is proposed, where the Kalman filter is applied to obtain the minimum mean squared error estimate of the transmitted symbols. The properties of the optimal realizable equalizer are analyzed. Its relations with …

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Toward A Construct Validation Of The Louisiana School Analysis Model Instructional Staff Questionnaire, Nikki Bray Clark Jan 2005

Toward A Construct Validation Of The Louisiana School Analysis Model Instructional Staff Questionnaire, Nikki Bray Clark

LSU Doctoral Dissertations

This study assessed the construct validity of the School Analysis Model (SAM) Instructional Staff Questionnaire. Construct validation was necessary for several reasons. First, it has not been possible to obtain evidence of the latent factor structure of this key component of the School Analysis Model (SAM). A factor analysis using data collected with the questionnaire was conducted to assess and identify the underlying factor structure of the instrument. Second, there is no evidence that the constructs measured by the SAM are associated with attributes of school performance further empirical analysis was done to determine if latent constructs contained within the …

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A Conductor's Analysis Of Amaral Vieira's Stabat Mater, Op.240: An Approach Between Music And Rhetoric, Vladimir A. Pereira Silva Jan 2005

A Conductor's Analysis Of Amaral Vieira's Stabat Mater, Op.240: An Approach Between Music And Rhetoric, Vladimir A. Pereira Silva

LSU Doctoral Dissertations

Choral music is one of the most common musical activities in Brazil. However, the lack of biographical studies, music publication, and theoretical works which discuss stylistic and interpretative aspects of choral performance creates problems for conductors. The primary goal of this study is to consider Amaral Vieira’s Stabat Mater, op. 240 specifically from a conductor’s point of view, focusing on biographical, analytical, stylistic, and interpretative issues. The document is divided into three chapters; chapter one discusses twentieth-century Brazilian choral music, Amaral Vieira’s life and music, history and overview of the Stabat Mater, op. 240, and textual aspects. Chapter two presents …

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Economic Valuation Of Natural Resource Management: A Case Study Of The Benuaq Dayak Tribe In Kalimantan, Indonesia, Indah D. Kusuma Jan 2005

Economic Valuation Of Natural Resource Management: A Case Study Of The Benuaq Dayak Tribe In Kalimantan, Indonesia, Indah D. Kusuma

LSU Doctoral Dissertations

The unavailability of total economic values of indigenous people in Indonesia, both in the short and long term, has created the rejection of their existences in the forest area. The purpose of this study is to estimate the total economic value of sustainable forest management conducted by indigenous tribes in Indonesia using total economic value concepts. The tribe’s total economic value is expressed by estimating the use value, indirect use value and non-use value. The study used benefit transfer and survey methods using questionnaires to estimate the tribe’s total economic value. The estimated total economic value of the Benuaq Dayak …

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Comparing Calf Sex Ratio And Semen Sex Ratio Determined By Conventional Pcr, Tara Marie Taylor Jan 2005

Comparing Calf Sex Ratio And Semen Sex Ratio Determined By Conventional Pcr, Tara Marie Taylor

LSU Master's Theses

Thirty-nine ejaculates from 8 Holstein bulls were collected. Straws of semen (n=750) were distributed among dairies in three states. Ten straws per ejaculate were sent to Louisiana State University (LSU) Dairy Improvement Center for conventional polymerase chain reaction (PCR) analysis. Spermatozoal DNA was extracted and PCR analysis was done using one primer set amplifying a single copy 125 base pair (bp) section of the Bos taurus factor IX (Christmas factor) precursor (found on the X chromosome) and another primer set amplifying a single copy section of the Bos taurus sex determining region Y protein (SRY) gene (found on the Y …

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Analysis Of Alternative Well Control Methods For Dual Density Deepwater Drilling, Mikolaj Stanislawek Jan 2005

Analysis Of Alternative Well Control Methods For Dual Density Deepwater Drilling, Mikolaj Stanislawek

LSU Master's Theses

The recent push into deepwater is currently limited by high drilling costs resulting from conventional well designs. As a result, dual gradient drilling methods have been proposed. This research investigates riser gas-lift as a potential means to implement a dual gradient system. A primary concern is well control in a system containing so many different density fluids and different flow paths. The specific concerns addressed in this study were kick detection, cessation of formation feed-in, removal of kick fluids, and re-establishing hydrostatic control with a constant bottom hole pressure method. These concerns were studied using a transient, multiphase simulator whose …

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The Influence Of Solo Performance Opportunities On Self-Reported Levels Of Musical Performance Anxiety Among Undergraduate College Music Majors, Carol W. Larsen Jan 2005

The Influence Of Solo Performance Opportunities On Self-Reported Levels Of Musical Performance Anxiety Among Undergraduate College Music Majors, Carol W. Larsen

LSU Master's Theses

Musical performance anxiety (MPA) is a concern for most college age musicians. While low to moderate levels of MPA may enhance performances for some musicians, too much “stage fright” can seriously hinder the quality of solo performances. Musicians use several techniques to manage MPA. One of these, desensitization, involves repeated exposure to solo performance opportunities. The purpose of this study was to determine if a relationship existed between the number and type of public solo performances completed and the level of self-reported performance anxiety among students pursuing baccalaureate degrees in music at a research extensive university in the southern United …

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Seasonal Space Use, Habitat Preference And Survival Of Female Wild Turkeys In A Louisiana Bottomland Hardwood Forest, Walker Blake Wilson Jan 2005

Seasonal Space Use, Habitat Preference And Survival Of Female Wild Turkeys In A Louisiana Bottomland Hardwood Forest, Walker Blake Wilson

LSU Master's Theses

Female wild turkeys (Meleagris gallopavo) were captured and radio-marked in a bottomland hardwood forest in south-central Louisiana. Turkeys were monitored using radio telemetry from fixed points on Sherburne Wildlife Management Area, Atchafalaya National Wildlife Refuge, and Bayou des Ourses to observe seasonal patterns of space use, habitat preference and survival from 2002-04. The largest mean seasonal home range of 902.87 ha occurred during preincubation (15 Feb – 9 Apr; n = 24) when females typically search for suitable nest sites, and the smallest mean seasonal home range was 434.12 ha, during brood-rearing (1 Jun – 30 Sep; n = 32) …

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Designation Of The Southwest National Wildlife Refuge Complex As Wetlands Of International Importance Under Ramsar, Convention On Wetlands Of International Importance, Mitchell Ward Coffman Jan 2005

Designation Of The Southwest National Wildlife Refuge Complex As Wetlands Of International Importance Under Ramsar, Convention On Wetlands Of International Importance, Mitchell Ward Coffman

LSU Master's Theses


The historical loss and continued threat of loss of Louisiana wetlands is a major environmental concern for the United States and the world. In 1971, the Ramsar Convention, an international environmental treaty was ratified to specifically address conservation planning and land use management issues involving wetlands of the world. Ramsar provides an international designation award called, the Wetlands of International Importance List, which formally acknowledges globally important wetland landscapes. Ramsar outlines specific criterion nominated wetland sites must possess for consideration of this listing.

The Southwest Louisiana National Wildlife Refuge Complex is an excellent candidate for nomination to the Ramsar Convention …

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Geologic Variability And Holocene Sedimentary Record On The Northern Gulf Of Mexico Inner To Mid-Continental Shelf, Triniti A. Dufrene Jan 2005

Geologic Variability And Holocene Sedimentary Record On The Northern Gulf Of Mexico Inner To Mid-Continental Shelf, Triniti A. Dufrene

LSU Master's Theses

Sidescan Sonar, chirp sonar sub-bottom profiles, and grab samples were collected on the north-central Gulf of Mexico continental shelf as part of an interdisciplinary study mapping juvenile red snapper habitat. Demarcation of essential fish habitat for juvenile red snapper (Lutjanus campechansis) in the Gulf of Mexico is considered critical for effective management of this valuable species. The first goal of this study was to map and describe the geology of this region. The second goal was to attempt to relate variations in geology to juvenile red snapper abundance and distribution. Sidescan mosaics were created for ten polygons, ranging in size …

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Molecular Recognition And Its Underlying Mechanisms In Molecularly Imprinted Polymers, Ryan Simon Jan 2005

Molecular Recognition And Its Underlying Mechanisms In Molecularly Imprinted Polymers, Ryan Simon

LSU Doctoral Dissertations

Molecular recognition in molecularly imprinting polymers (MIPs) is governed by two mechanisms: pre-organization of functional groups and shape specificity of the binding site. While pre-organization of functional groups has been studied extensively, shape specificity of the binding site has not been rigorously explored. The goal of this research is to determine the influence of shape specificity on molecular recognition in MIPs (Chapter 2). Once shape selectivity was proven to play a vital role in molecular recognition, it was important to determine if pre-organization of functional groups or shape specificity was the dominating factor in determining molecular recognition in the binding …

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Komatiites Of The Weltevreden Formation, Barberton Greenstone Belt, South Africa: Implications For The Chemistry And Temperature Of The Archean Mantle, Keena Kareem Jan 2005

Komatiites Of The Weltevreden Formation, Barberton Greenstone Belt, South Africa: Implications For The Chemistry And Temperature Of The Archean Mantle, Keena Kareem

LSU Doctoral Dissertations

The komatiites of the 3.29 Ga Weltevreden Formation, Barberton Greenstone Belt, South Africa represent extremely magnesian lavas derived from the Archean mantle. Three related papers are presented on aspects of the temperature and composition of the Archean mantle, and surface alteration processes. Petrographical and geochemical analyses confirm that olivines from the komatiites retain much of their original igneous character, containing fresh olivines, pyroxenes, and chromites. The olivines from the Weltevreden Formation are extremely magnesian, with Fo contents up to 95.6. Primitive mantle normalized Gd/Yb values near 1, and Al2O3/TiO3 values of 26-33 for these rocks …

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Hydrophobic Guar Gum Derivatives Prepared By Controlled Grafting Processes For Hydraulic Facturing Applications, Ahmad Bahamdan Jan 2005

Hydrophobic Guar Gum Derivatives Prepared By Controlled Grafting Processes For Hydraulic Facturing Applications, Ahmad Bahamdan

LSU Doctoral Dissertations

The synthesis of new water soluble guar gum derivatives is described. Introduction of polyalkoxyalkyleneamide grafts to guar gum or hydroxyopropyl guar was achieved in a three step process: carboxymethylation with sodium chloroacetate, esterification with dimethyl sulfate and amidation with a series of polyalkoxyalkylene-amines. The process steps were followed using infrared spectroscopy; the grafted guar derivatives were characterized using FT-IR and 1H NMR. A series of hydroxypropyl guar derivatives with degrees of carboxymethylations ranging from 0.15-0.25 were modified with polyalkoxyalkyleneamines with molecular weights ranging from 300-3000. The ratio of oxypropylene to oxoethylene units in the polyalkoxyalkyleneamines was varied from 9/1 …

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Using The Biodatamation Strategy To Learn Introductory College Biology: Value-Added Effects On Selected Students' Conceptual Understanding And Conceptual Integration Of The Processes Of Photosynthesis And Celluar Respiration, Jewel Jurovich Reuter Jan 2005

Using The Biodatamation Strategy To Learn Introductory College Biology: Value-Added Effects On Selected Students' Conceptual Understanding And Conceptual Integration Of The Processes Of Photosynthesis And Celluar Respiration, Jewel Jurovich Reuter

LSU Doctoral Dissertations

The purpose of this exploratory research was to study how students learn photosynthesis and cellular respiration and to determine the value added to the student's learning by each of the three technology-scaffolded learning strategy components (animated concept presentations and WebQuest-style activities, data collection, and student-constructed animations) of the BioDatamation™ (BDM) Program. BDM learning strategies utilized the Theory of Interacting Visual Fields™ (TIVF) (Reuter & Wandersee, 2002a, 2002b; 2003a, 2003b) which holds that meaningful knowledge is hierarchically constructed using the past, present, and future visual fields, with visual metacognitive components that are derived from the principles of Visual Behavior (Jones,1995), Human …

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An Empirical Study Of Imputation Techniques For Software Data Sets, Sumanth Yenduri Jan 2005

An Empirical Study Of Imputation Techniques For Software Data Sets, Sumanth Yenduri

LSU Doctoral Dissertations

Software Project Effort/Cost/Time Estimation has been one of the hot topics of research in the current software engineering industry. Solutions for effort/cost/time estimation are in great demand. Knowledge of accurate effort/cost/time estimates early in the software project life cycle enables project managers manage and exploit resources efficiently. The constraints of cost and time can also be met. To this day, most companies rely on their historical database of past project data sets to predict estimates for future projects. Like other data sets, software project data sets also suffer from numerous problems. The most important problem is they contain missing/incomplete data. …

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Comparative Studies Of Sperm Cryopreservation Of Diploid And Tetraploid Pacific Oysters, Qiaoxiang Dong Jan 2005

Comparative Studies Of Sperm Cryopreservation Of Diploid And Tetraploid Pacific Oysters, Qiaoxiang Dong

LSU Doctoral Dissertations

This dissertation addressed comparative studies of sperm cryopreservation of diploid and tetraploid Pacific oysters, Crassostrea gigas, with an emphasis on the development of standardized and optimized protocols. This includes comparative ultrastructural differences between sperm from diploid and tetraploid oysters, methods for the rapid estimation of sperm concentration, optimization of cryopreservation, and evaluation of the mechanisms for sperm agglutination (formation of clumps or elongated "noodles") in thawed samples. Currently, cryopreserved sperm has not been commercialized in any aquatic species, and standardization and optimization could greatly benefit the potential commercialization of its use. In oysters specifically, cryopreserved sperm from tetraploids would facilitate …

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Nitrate Reduction And Methane Formation As Influenced By Iron-Centered Intermediate Redox Processes In Rice Soils, Bin Huang Jan 2005

Nitrate Reduction And Methane Formation As Influenced By Iron-Centered Intermediate Redox Processes In Rice Soils, Bin Huang

LSU Doctoral Dissertations

Rice fields are a major source of the greenhouse gases methane (CH4) and nitrous oxide (N2O) and contribute to nitrate (NO3-) pollution in waters. Ferric iron (Fe3+) and manganic manganese (Mn4+) are two intermediate alternative electron acceptors (AEAs) capable of regeneration in freshwater soils. In this investigation, the influences of iron-centered intermediate redox processes on NO3- reduction and CH4 formation in rice soils were studied using soil slurries, soil columns, and potted rice. Reduction of Fe3+-centered intermediate AEAs was mainly mediated by obligate anaerobes …

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Characterization Of A Modified Poly(Propylene Imine) Dendrimer Host System, Amy D. Morara Jan 2005

Characterization Of A Modified Poly(Propylene Imine) Dendrimer Host System, Amy D. Morara

LSU Doctoral Dissertations

The research in this dissertation focuses on the design of a novel redox-responsive host system that has the ability to encapsulate guest molecules. The host at hand is a tri(ethylene oxide), TEO, pyrrole-terminated PPI dendrimer that possesses water-solubility as a result of the presence of the TEO chains on the pyrrole groups and redox-responsive activity from the pyrrole groups after their oligomerization. The pyrrole moieties at the periphery of the dendrimer exhibit the ability to be oligomerized by oxidation chemistry, and this is shown to aid in the retention and egress of guest molecules located within the dendrimer interior. These …

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Population Dynamics Of Clausocalanus Furcatus (Copepoda, Calanoida) In The Northern Gulf Of Mexico, Hongsheng Bi Jan 2005

Population Dynamics Of Clausocalanus Furcatus (Copepoda, Calanoida) In The Northern Gulf Of Mexico, Hongsheng Bi

LSU Doctoral Dissertations

Copepods are important components of marine ecosystems. Understanding copepod population dynamics can help interpret variations in both primary producers and higher trophic levels. Egg production, stage duration, and stage-specific mortality rates are key parameters describing copepod population dynamics. Estimation of stage-specific mortality is complicated due to a complex life history, patchiness, and sampling biases. This study was undertaken to quantify the population dynamics of the copepod Clausocalanus furcatus in the northern Gulf of Mexico and to assess the utility of available mortality estimation methods in a highly advective environment. Zooplankton samples were taken every 12h from March 18-April 6, and …

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Two Dimensional Sediment Transport Model Using Parallel Computers, Vikas Singh Jan 2005

Two Dimensional Sediment Transport Model Using Parallel Computers, Vikas Singh

LSU Master's Theses

Management and development of water bodies is vital for meeting domestic, agricultural, energy and industrial needs. To that end, dams, artificial channels, lakes and other water structures have been constructed. Management and development of these structures encounter problems of land erosion, reservoir silting, and degradation and aggradation of channel beds, which need to be addressed. Fundamental to these problems are sediment transport, erosion and deposition. Numerical modeling of sediment transport is the best tool to simulate sediment transport in a water body. This study develops a vertically integrated two-dimensional numerical sediment transport model. Sediment transport is simulated in two parts …

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Hydrodynamic Analysis Of Compliant Journal Bearings, Amith Hanumappa Reddy Jan 2005

Hydrodynamic Analysis Of Compliant Journal Bearings, Amith Hanumappa Reddy

LSU Master's Theses

Compliant journal bearings are commonly used to support radial loads at extreme operating speeds and conditions where conventional bearings cannot operate. The journal and bearing system are supported by a thin lubricant film (gas) due to the hydrodynamic pressure distribution. To predict the bearing performance parameters, the compressible Reynolds equation is solved based on Infinitely Long Approximation (ILA), Finite Analysis (FA) and a new Modified Parabolic Approximation (MPA). The MPA method reduces the classical Reynolds equation to an ordinary differential equation. Appropriate equations and numerical solution are developed for treating a compressible Reynolds equation using MPA. A series of parametric …

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Linear Versus Cyclic Inorganic/Organic Hybrid Oligomeric Molecules, Christopher Roland Sparrow Jan 2005

Linear Versus Cyclic Inorganic/Organic Hybrid Oligomeric Molecules, Christopher Roland Sparrow

LSU Master's Theses

The synthesis of the new aryl bis(β-diketone) ligand m-phenylenebis(acetylacetone) (m-pbaH2) allowed for complexation with copper(II) to form a 4-membered ring Cu4(m-pba)4. An alternate route, via a phospholene adduct, was implemented after difficulties in preparing the ligand via an azo sulfide conversion from m-phenylenediamine. The connection of two m-pba ligands coordinated to a Cu(II) metal ion causes a distortion along the axial position of the metal center. The pore has a diameter of (Cu-----Cu = 14.317 Å) when viewing opposite metal centers. An open coordination site along Cu(II) axial position may facilitate host-guest binding interactions. The concave shape of the host …

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