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2013

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Full-Text Articles in Physics

A Viscous Flow Analog To Prandtl’S Optimized Lifting Line Theory Utilizing Rotating Biquadratic Bodies Of Revolution, Mark Nathaniel Callender Dec 2013

A Viscous Flow Analog To Prandtl’S Optimized Lifting Line Theory Utilizing Rotating Biquadratic Bodies Of Revolution, Mark Nathaniel Callender

Doctoral Dissertations

Prandtl’s lifting line theory expanded the Kutta-Joukowski theorem to calculate the lift and induced drag of finite wings. The circulation distribution about a real wing was represented by a superposition of infinitesimal vortex filaments. From this theory, the optimum distribution of circulation was determined to be elliptical. A consequence of this theory led to the prediction that the elliptical chord distribution on a real fixed wing would provide the elliptical circulation distribution. The author applied the same line of reasoning to lift-producing rotating cylinders in order to determine the cylindrical geometry that would theoretically produce an elliptical circulation distribution. The …


Extracting The Structure And Conformations Of Biological Entities From Large Datasets, Ali Dashti Dec 2013

Extracting The Structure And Conformations Of Biological Entities From Large Datasets, Ali Dashti

Theses and Dissertations

In biology, structure determines function, which often proceeds via changes in conformation. Efficient means for determining structure exist, but mapping conformations continue to present a serious challenge. Single-particles approaches, such as cryogenic electron microscopy (cryo-EM) and emerging "diffract & destroy" X-ray techniques are, in principle, ideally positioned to overcome these challenges. But the algorithmic ability to extract information from large heterogeneous datasets consisting of "unsorted" snapshots - each emanating from an unknown orientation of an object in an unknown conformation - remains elusive.

It is the objective of this thesis to describe and validate a powerful suite of manifold-based algorithms …


Molecular Dynamics Model Of Carbon Nanotubes In Epon 862/Detda Polymer, Guttormur Arnar Ingvason Dec 2013

Molecular Dynamics Model Of Carbon Nanotubes In Epon 862/Detda Polymer, Guttormur Arnar Ingvason

Doctoral Dissertations and Master's Theses

The aerospace industry is interested in increasing the strength while reducing the weight of carbon fiber composite materials. Adding single walled carbon nanotubes (SWCNT) to a polymer matrix can achieve that goal by improving delamination properties of the composite. Due to the complexity of polymer molecules and the curing process, few 3-D Molecular Dynamics simulations of a polymer-SWCNT composite have been run. Our model runs on the Large-scale Atomic/Molecular Massively Parallel Simulator (LAMMPS), with a COMPASS (Condensed phase Optimized Molecular Potential for Atomistic Simulations Studies) potential to represent the interactions between the atoms of the polymer and the SWCNT. This …


Criticality And Characteristic Neutronic Analysis Of A Transient-State Shockwave In A Pulsed Spherical Gaseous Uranium-Hexafluoride Reactor, Jeremiah Boles Dec 2013

Criticality And Characteristic Neutronic Analysis Of A Transient-State Shockwave In A Pulsed Spherical Gaseous Uranium-Hexafluoride Reactor, Jeremiah Boles

UNLV Theses, Dissertations, Professional Papers, and Capstones

The purpose of this study is to analyze the theoretical criticality of a spherical uranium-hexafluoride reactor with a transient, pulsed shockwave emanating from the center of the sphere in an outward-radial direction. This novel nuclear reactor design, based upon pulsed fission in a spherical enclosure is proposed for possible use in direct energy conversion, where the energy from fission products is captured through the use of electrostatic fields or through induction. An analysis of the dynamic behavior of the shockwave in this reactor is the subject of this thesis. As a shockwave travels through a fluid medium, the characteristics of …


Design And Fabrication Of An Infrared Optical Pyrometer Asic As A Diagnostic For Shock Physics Experiments, Jared Gordon Dec 2013

Design And Fabrication Of An Infrared Optical Pyrometer Asic As A Diagnostic For Shock Physics Experiments, Jared Gordon

UNLV Theses, Dissertations, Professional Papers, and Capstones

Optical pyrometry is the sensing of thermal radiation emitted from an object using a photoconductive device to convert photons into electrons, and is an important diagnostic tool in shock physics experiments. Data obtained from an optical pyrometer can be used to generate a blackbody curve of the material prior to and after being shocked by a high speed projectile. The sensing element consists of an InGaAs photodiode array, biasing circuitry, and multiple transimpedance amplifiers to boost the weak photocurrent from the noisy dark current into a signal that can eventually be digitized. Once the circuit elements have been defined, more …


Optics And Spectroscopy In Massive Electrodynamic Theory, Adam Caccavano Oct 2013

Optics And Spectroscopy In Massive Electrodynamic Theory, Adam Caccavano

Dissertations and Theses

The kinematics and dynamics for plane wave optics are derived for a massive electrodynamic field by utilizing Proca's theory. Atomic spectroscopy is also examined, with the focus on the 21 cm radiation due to the hyperfine structure of hydrogen. The modifications to Snell's Law, the Fresnel formulas, and the 21 cm radiation are shown to reduce to the familiar expressions in the limit of zero photon mass.


Modeling The Atomic And Electronic Structure Of Metal-Metal, Metal-Semiconductor And Semiconductor-Oxide Interfaces, Ganesh Krishna Hegde Oct 2013

Modeling The Atomic And Electronic Structure Of Metal-Metal, Metal-Semiconductor And Semiconductor-Oxide Interfaces, Ganesh Krishna Hegde

Open Access Dissertations

The continuous downward scaling of electronic devices has renewed attention on the importance of the role of material interfaces in the functioning of key components in electronic technology in recent times. It has also brought into focus the utility of

atomistic modeling in providing insights from a materials design perspective. In this thesis, a combination of Semi Empirical Tight-Binding (TB), first-principles Density

Functional Theory and Reactive Molecular Dynamics (MD) modeling is used to study aspects of the electronic and atomic structure of three such 'canonical' material interfaces - Metal-Metal, Metal-Semiconductor and Semiconductor oxide interfaces.

An important contribution of this thesis …


Atomistic Simulation Of Plasma Interaction With Plasma Facing Components In Fusion Reactors, Xue Yang Oct 2013

Atomistic Simulation Of Plasma Interaction With Plasma Facing Components In Fusion Reactors, Xue Yang

Open Access Dissertations

The interaction between plasma and fusion relevant materials is one of the critical issues in successfully using those materials in Tokamak reactors. This research uses molecular dynamics, kinetic Monte Carlo and binary collision approximation methods to model fusion relevant material bombarded by energetic particles to investigate retention, deposition, sputtering, erosion, blistering effects, diffusion, and so on.

The deuterium bombardment of monocrystalline tungsten was modeled by LAMMPS code using Tersoff type interatomic potential. The deuterium trapping rate, implantation depth, and stopping time in 600-2000 K tungsten bombarded by 5-100 eV deuterium atoms were simulated. Irradiated monocrystalline tungsten became amorphous prior to …


Design And Assembly Of Nanostructured Complex Metal Oxide Materials For The Construction Of Batteries And Thermoelectric Devices, Gautam Ganapati Yadav Oct 2013

Design And Assembly Of Nanostructured Complex Metal Oxide Materials For The Construction Of Batteries And Thermoelectric Devices, Gautam Ganapati Yadav

Open Access Dissertations

Thermoelectric devices and lithium-ion batteries are among the fastest growing energy technologies. Thermoelectric devices generate energy from waste heat, whereas lithium-ion batteries store energy for use in commercial applications. Two different topics are bound with a common thread in this thesis - nanotechnology! In fact, nanostructuring is a more preferred term for the approach I have taken herein. Another commonality between these two topics is the material system I have used to prove my hypotheses - complex metal oxides.

Complex metal oxides can be used for both energy generation and storage as they are stable at high temperatures, are benign …


Altered Cholesterol Metabolism In Human Cancers Unraveled By Label-Free Spectroscopic Imaging, Shuhua Yue Oct 2013

Altered Cholesterol Metabolism In Human Cancers Unraveled By Label-Free Spectroscopic Imaging, Shuhua Yue

Open Access Dissertations

Despite tremendous scientific achievements, cancer remains the second leading cause of death in the United States. Metabolic reprogramming has been increasingly recognized as a core hallmark of cancer. My dissertation work identified novel diagnostic markers and therapeutic targets for human cancers through the study of cholesterol in cancer cells.

Enabled by label-free Raman spectromicroscopy, we performed the first quantitative analysis of lipogenesis at single cell level in human patient cancerous tissues. Our imaging data revealed an unexpected, aberrant accumulation of esterified cholesterol in lipid droplets of high-grade prostate cancer and metastases, but not in normal prostate, benign prostatic hyperplasia, or …


Applicability Of Continuum Fracture Mechanics In Atomistic Systems, Shao-Huan Cheng Oct 2013

Applicability Of Continuum Fracture Mechanics In Atomistic Systems, Shao-Huan Cheng

Open Access Dissertations

By quantitating the amplitude of the unbounded stress, the continuum fracture mechanics defines the stress intensity factor K to characterize the stress and displacement fields in the vicinity of the crack tip, thereby developing the relation between the stress singularity and surface energy (energy release rate G). This G-K relation, assigning physical meaning to the stress intensity factor, makes these two fracture parameters widely used in predicting the onset of crack propagation. However, due to the discrete nature of the atomistic structures without stress singularity, there might be discrepancy between the failure prediction and the reality of nanostructured materials. Defining …


Fabricating Cost-Effective Nanostructures For Biomedical Applications, Erden Ertorer Sep 2013

Fabricating Cost-Effective Nanostructures For Biomedical Applications, Erden Ertorer

Electronic Thesis and Dissertation Repository

In this thesis we described inexpensive alternatives to fabricate nanostructures on planar substrates and provided example applications to discuss the efficiency of fabricated nanostructures.

The first method we described is forming large area systematically changing multi-shape nanoscale structures on a chip by laser interference lithography. We analyzed the fabricated structures at different substrate positions with respect to exposure time, exposure angle and associated light intensity profile. We presented experimental details related to the fabrication of symmetric and biaxial periodic nanostructures on photoresist, silicon surfaces, and ion-milled glass substrates. Behavior of osteoblasts and osteoclasts on the nanostructures was investigated. These results …


Piv-Based Investigation Of Hemodynamic Factors In Diseased Carotid Artery Bifurcations With Varying Plaque Geometries, Sarah Kefayati Aug 2013

Piv-Based Investigation Of Hemodynamic Factors In Diseased Carotid Artery Bifurcations With Varying Plaque Geometries, Sarah Kefayati

Electronic Thesis and Dissertation Repository

Ischemic stroke is often a consequence of complications due to clot formation (i.e. thrombosis) at the site of an atherosclerotic plaque developed in the internal carotid artery. Hemodynamic factors, such as shear-stress forces and flow disturbances, can facilitate the key mechanisms of thrombosis. Atherosclerotic plaques can differ in the severity of stenosis (narrowing), in eccentricity (symmetry), as well as inclusion of ulceration (wall roughness). Therefore, in terms of clinical significance, it is important to investigate how the local hemodynamics of the carotid artery is mediated by the geometry of plaque. Knowledge of thrombosis-associated hemodynamics may provide a basis to introduce …


Optimization Of A Boundary Element Approach To Electromagnet Design With Application To A Host Of Current Problems In Magnetic Resonance Imaging, Chad T. Harris Aug 2013

Optimization Of A Boundary Element Approach To Electromagnet Design With Application To A Host Of Current Problems In Magnetic Resonance Imaging, Chad T. Harris

Electronic Thesis and Dissertation Repository

Magnetic resonance imaging (MRI) has proven to be a valuable methodological approach in both basic research and clinical practice. However, significant hardware advances are still needed in order to further improve and extend the applications of the technique. The present dissertation predominantly addresses gradient and shim coil design (sub-systems of the MR system).

A design study to investigate gradient performance over a set of surface geometries ranging in curvature from planar to a full cylinder using the boundary element (BE) method is presented. The results of this study serve as a guide for future planar and pseudo-planar gradient systems for …


Fully Coupled Fluid And Electrodynamic Modeling Of Plasmas: A Two-Fluid Isomorphism And A Strong Conservative Flux-Coupled Finite Volume Framework, Richard Joel Thompson Aug 2013

Fully Coupled Fluid And Electrodynamic Modeling Of Plasmas: A Two-Fluid Isomorphism And A Strong Conservative Flux-Coupled Finite Volume Framework, Richard Joel Thompson

Doctoral Dissertations

Ideal and resistive magnetohydrodynamics (MHD) have long served as the incumbent framework for modeling plasmas of engineering interest. However, new applications, such as hypersonic flight and propulsion, plasma propulsion, plasma instability in engineering devices, charge separation effects and electromagnetic wave interaction effects may demand a higher-fidelity physical model. For these cases, the two-fluid plasma model or its limiting case of a single bulk fluid, which results in a single-fluid coupled system of the Navier-Stokes and Maxwell equations, is necessary and permits a deeper physical study than the MHD framework. At present, major challenges are imposed on solving these physical models …


Investigation Of Time And Position Resolved Alpha Transducers For Multi-Modal Imaging With A D-T Neutron Generator, Joshua William Cates Aug 2013

Investigation Of Time And Position Resolved Alpha Transducers For Multi-Modal Imaging With A D-T Neutron Generator, Joshua William Cates

Doctoral Dissertations

Deuterium-Tritium (D-T) neutron generators have been used as an active interrogation source for associated particle imaging (API) techniques. The D-T reaction yields a 14.1 MeV neutron and a 3.5 MeV alpha (or assoicated) particle, projected nearly back-to-back. The kinetics of the reaction allow the direction and initial time of the neutron to be determined utilizing position sensitive detectors for both the alpha and neutron. This information facilitates multi-modal fast neutron imaging of inspection objects and closed containers to infer the geometry within them and the presence of special nuclear material (SNM). Since position and time of interaction of the alpha …


Structural Properties Of Ferroelectric Lead (Zirconium0.5,Titanium0.5)Oxygen3 Nanotube Array And Electronic Structure Of Lao Delta-Doped Strontium Titanate, Rajendra Prasad Adhikari Aug 2013

Structural Properties Of Ferroelectric Lead (Zirconium0.5,Titanium0.5)Oxygen3 Nanotube Array And Electronic Structure Of Lao Delta-Doped Strontium Titanate, Rajendra Prasad Adhikari

Graduate Theses and Dissertations

In this Dissertation we begin with two introductions on: 1) ferroelectricity and related phenomena, and 2) novel properties of Oxide electronics and the generation of two dimensional electron gas. We then give theoretical background of density functional theory (including LDA+U) and pseudopotentials. The first part of research work is about structural, polarization, and dielectric properties of ferroelectric Lead Zirconate Titanate (PZT) solid solution in the form of a nanotube array, embedded in a matrix medium of different ferroelectric strengths. We use the effective Hamiltonian derived from first-principles and finite-temperature Monte Carlo methods to determine the various properties. We revealed different …


High-Performance, Scalable Optical Network-On-Chip Architectures, Xianfang Tan Aug 2013

High-Performance, Scalable Optical Network-On-Chip Architectures, Xianfang Tan

UNLV Theses, Dissertations, Professional Papers, and Capstones

The rapid advance of technology enables a large number of processing cores to be integrated into a single chip which is called a Chip Multiprocessor (CMP) or a Multiprocessor System-on-Chip (MPSoC) design. The on-chip interconnection network, which is the communication infrastructure for these processing cores, plays a central role in a many-core system. With the continuously increasing complexity of many-core systems, traditional metallic wired electronic networks-on-chip (NoC) became a bottleneck because of the unbearable latency in data transmission and extremely high energy consumption on chip. Optical networks-on-chip (ONoC) has been proposed as a promising alternative paradigm for electronic NoC with …


Growth Of Zno Thin Films On Polar Oxide Surfaces By Atomic Layer Deposition, Kallol Pradhan Aug 2013

Growth Of Zno Thin Films On Polar Oxide Surfaces By Atomic Layer Deposition, Kallol Pradhan

Theses and Dissertations

Polar heterointerfaces of MgO(111) and the II-VI semiconductor ZnO are of technological interest for transparent conducting electrode applications. Growth and structure of thin films on polar surfaces can be different than on non-polar surfaces due to the large surface energy of polar surfaces. We have grown ZnO on unreconstructed MgO(111)-(1x1)-OH terminated and reconstructed MgO(111)-(√3x√3)R30° polar oxide surfaces using atomic layer deposition. A homemade UHV-interfaced viscous-flow atomic layer deposition (ALD) reactor with in-situ quartz crystal monitor was used to grow ZnO thin films on the MgO(111) substrates. Surface morphology studies revealed that the surface roughness increases with ZnO film thickness and …


Study Of A Non-Equilibrium Plasma Pinch With Application For Microwave Generation, Ahmad Al Agry Aug 2013

Study Of A Non-Equilibrium Plasma Pinch With Application For Microwave Generation, Ahmad Al Agry

UNLV Theses, Dissertations, Professional Papers, and Capstones

The Non-Equilibrium Plasma Pinch (NEPP), also known as the Dense Plasma Focus (DPF) is well known as a source of energetic ions, relativistic electrons and neutrons as well as electromagnetic radiation extending from the infrared to X-ray. In this dissertation, the operation of a 15 kJ, Mather type, NEPP machine is studied in detail. A large number of experiments are carried out to tune the machine parameters for best performance using helium and hydrogen as filling gases. The NEPP machine is modified to be able to extract the copious number of electrons generated at the pinch. A hollow anode with …


Multiscale Study Of Batio3 Nanostructures And Nanocomposites, Lydie Louis Louis Aug 2013

Multiscale Study Of Batio3 Nanostructures And Nanocomposites, Lydie Louis Louis

Graduate Theses and Dissertations

Advancements in integrated nanoelectronics will continue to require the use of unique materials or systems of materials with diverse functionalities in increasingly confined spaces.

Hence, research on finite-dimensional systems strive to unearth and expand the knowledge of fundamental physical properties in certain key materials which exhibit numerous concurrent and exploitable functions.

Correspondingly, ferroelectric nanostructures, which particularly display a plethora of complex phenomena, prevalent in countless fields of research, are noteworthy candidates. Presently, however, the assimilation of zero-(0D) and one-dimensional (1D) ferroelectric into micro- or nano-electronics has been lagging, in part due to a lack of applied and fundamental studies but …


Influence Of Microstructure On The Propagation Of Fatigue Cracks In Inconel 617, Benjiman Michael Albiston Jul 2013

Influence Of Microstructure On The Propagation Of Fatigue Cracks In Inconel 617, Benjiman Michael Albiston

Boise State University Theses and Dissertations

Inconel 617 is a candidate material for use in the intermediate heat exchanger of the Next Generation Nuclear Plant. Because of the high temperatures and the fluctuations in stress and temperature, the fatigue behavior of the material is important to understand. The goal of this study was to determine the influences of the microstructure during fatigue crack propagation. For this investigation, Inconel 617 compact tension samples, fatigue tested by Julian Benz at the Idaho National Laboratory, were obtained. The testing conditions included two environments at 650 °C (lab air and impure-He) and varied testing parameters including: loading waveform (triangular, trapezoidal), …


All-Optical Sigma-Delta Modulator For Analog-To-Digital Conversion, Bin Zhang Jul 2013

All-Optical Sigma-Delta Modulator For Analog-To-Digital Conversion, Bin Zhang

Graduate Theses - Physics and Optical Engineering

In this thesis, an all-optical sigma-delta (ΣΔ) modulator for analog-to-digital conversion (ADC) using a novel optical bistable switch, the SOA-PD device, is demonstrated. The presented all-optical ΣΔ modulator consists of a photonic leaky integrator, the SOA-PD optical comparator, and a positive feedback loop. The switching properties of the SOA-PD device are studied and experimentally tested to confirm its performance. Then the all-optical ΣΔ modulator is designed according to the switching performance of the SOA-PD device. It is demonstrated that the all-optical ΣΔ modulator is capable of producing an inverted non-return-to-zero (NRZ) type binary output for frequencies in the range of …


Field Emission Studies Toward Improving The Performance Of Dc High Voltage Photoelectron Guns, Mahzad Bastaninejad Jul 2013

Field Emission Studies Toward Improving The Performance Of Dc High Voltage Photoelectron Guns, Mahzad Bastaninejad

Mechanical & Aerospace Engineering Theses & Dissertations

Field emission is the main mechanism that prevents DC high voltage photoemission electron guns from operating at the very high bias voltages required to produce low emittance beams. Gas conditioning is shown to eliminate field emission from cathode electrodes used inside DC high voltage photoelectron guns. Measurements and simulation results indicate that gas conditioning eliminates field emission from cathode electrodes via two mechanisms: sputtering and implantation, with the benefits of implantation reversed by heating the electrode. The field emission characteristics of 5 stainless steel electrodes varied significantly upon the initial application of voltage but improved to nearly the same level …


Ramjet Combustion Chamber, Paul Cameron Stone Jun 2013

Ramjet Combustion Chamber, Paul Cameron Stone

Aerospace Engineering

A ramjet combustion chamber is designed and some initial assembly fabrication and test completed as a component of a ramjet graduate project for California Polytechnic State University, San Luis Obispo Supersonic Wind Tunnel. The combustor design is driven by a theoretical model created by a Cal Poly graduate student, Harrison Sykes. Temperature, pressure, and fuel flow will be measured.


Nbconvert Refactor, Jonathan Frederic Jun 2013

Nbconvert Refactor, Jonathan Frederic

Physics

IPython is an interactive Python computing environment. It provides an enhanced interactive Python shell. The IPython Notebook is a browser based interface distributed with IPython. It enables the creation of richly formatted notebooks that contain embedded IPython code. With nbconvert, notebooks can be exported to various formats including, but not limited to, LaTeX, reveal.js, RST, and HTML. This is important for users that want to be able to share their work outside of IPython. This senior project is the addition of a Sphinx LaTeX output format and the refactor of nbconvert.


Organic Solar Cells Based On High Dielectric Constant Materials: An Approach To Increase Efficiency, Khalil Jumah Tawfiq Hamam Jun 2013

Organic Solar Cells Based On High Dielectric Constant Materials: An Approach To Increase Efficiency, Khalil Jumah Tawfiq Hamam

Dissertations

The efficiency of organic solar cells still lags behind inorganic solar cells due to their low dielectric constant which results in a weakly screened columbic attraction between the photogenerated electron-hole system, therefore the probability of charge separating is low. Having an organic material with a high dielectric constant could be the solution to get separated charges or at least weakly bounded electron-hole pairs. Therefore, high dielectric constant materials have been investigated and studied by measuring modified metal-phthalocyanine (MePc) and polyaniline in pellets and thin films. The dielectric constant was investigated as a function of temperature and frequency in the range …


Novel Bimetallic Plasmonic Nanomaterials, Ritesh Sachan May 2013

Novel Bimetallic Plasmonic Nanomaterials, Ritesh Sachan

Doctoral Dissertations

Plasmonic nanomaterials have attracted a lot of attention recently due to their application in various fields such as chemical and biological sensing, catalysis, energy harvesting and optical devices. However, there is a need to address several outstanding issues with these materials, including cost-effective synthesis, tunability in plasmonic characteristics, and long term stability. In this thesis, we have focused on bimetallic nanoparticles (NPs) of Ag and Co due to their immiscibility as well as their individual properties. First, a pulsed laser induced dewetting route was used to synthesize Ag-Co bimetallic plasmonic NPs. An synthesis parameter space was derived to show the …


Femtosecond Laser Patterned Templates And Imprinted Polymer Structures, Deepak Rajput May 2013

Femtosecond Laser Patterned Templates And Imprinted Polymer Structures, Deepak Rajput

Doctoral Dissertations

Femtosecond laser machining is a direct-write lithography technique by which user-defined patterns are efficiently and rapidly generated at the surface or within the bulk of transparent materials. When femtosecond laser machining is performed with tightly focused amplified pulses in single-pulse mode, transparent substrates like fused silica can be surface patterned with high aspect ratio (>10:1) and deep (>10 μm) nanoholes. The main objective behind this dissertation is to develop single-pulse amplified femtosecond laser machining into a novel technique for the production of fused silica templates with user-defined patterns made of high aspect ratio nanoholes. The size of the …


Probing Bonding And Dynamics At Heterogeneous Adsorbate/Graphene Interfaces, Eric Charles Mattson May 2013

Probing Bonding And Dynamics At Heterogeneous Adsorbate/Graphene Interfaces, Eric Charles Mattson

Theses and Dissertations

Graphene-based materials are becoming an astoundingly promising choice for many relevant technological and environmental applications. Deriving graphene from the reduction of graphene oxide (GO) is becoming a popular and inexpensive route toward the synthesis of these materials. While the desired product from GO reduction is pristine graphene, defects and residual oxygen functional groups inherited from the parent GO render reduced graphene oxide (RGO) distinct from graphene. In this work, the structure and bonding for GO and RGO is investigated to the end of a working understanding of the composition and properties of these materials. In situ selected area electron diffraction …