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Full-Text Articles in Materials Chemistry
Preparation Of Pbo 2/Ti Plate Electrode, Zhigang Shao, Baolian Yi, Xinge Zhang, Enjun Zhang
Preparation Of Pbo 2/Ti Plate Electrode, Zhigang Shao, Baolian Yi, Xinge Zhang, Enjun Zhang
Journal of Electrochemistry
The perchlorate was made up of a lead dioxide plate elcetrode and an oxygen cathode. By measuring the flow capacity of cell gas in the cell, and by means of CV、SEM、XRD, the performances of the lead dioxide plate electrodes are evaluated. The influence of changes in the concentrations of electroplating solutions (F 、HNO 3、Bi 3+ 、Ni 2+ 、Fe 3+ and surface active agent) is investigated. The results show that the concentrations of Fe 3+ in the solutions must be lower 0.01 g/l, and the concentrations of HNO 3 in the solutions are about 20 g/l, in order to get better …
Studies On The Cathodic Current Efficiency In The Electrodeposition Ni Psz Gradient Coating, Jun Li, Dianlong Wang, Li Chen, Xinguo Hu
Studies On The Cathodic Current Efficiency In The Electrodeposition Ni Psz Gradient Coating, Jun Li, Dianlong Wang, Li Chen, Xinguo Hu
Journal of Electrochemistry
The cathodic current efficiency and the electrochemical behavior in electrodeposition Ni PSZ gradient coating were investigated by various electrochemical techniques and scanning electron microscope. The results showed that the Ni PSZ composite coatings can accelerate evolution of hydrogen with the increase of PSZ content. The overpotential of nickel reduction will be increased and that of hydrogen reaction will be reduced in the presence of PSZ particles in electrolyte. The effect of PSZ particles on nickel electrodeposition was preferentially to catalyze the formation of H ads . These all contributed to the lower current efficiency.