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Analytical Chemistry Commons

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Spectroscopy

Governors State University

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Full-Text Articles in Analytical Chemistry

Quantitative Analysis Of Acetylsalicylic Acid By Q-Nmr (Quantitative-Nuclear Magnetic Resonance Spectroscopy), Charles Flemming Jr. Oct 2016

Quantitative Analysis Of Acetylsalicylic Acid By Q-Nmr (Quantitative-Nuclear Magnetic Resonance Spectroscopy), Charles Flemming Jr.

All Student Theses

Quantitative analysis is an important step during pharmaceutical drug development. Currently, the pharmaceutical industry uses high performance liquid chromatography (HPLC) for quantitative analysis of organic compounds as the preferred technique. The proton nuclear magnetic resonance (NMR) technique has an inherent ability to quantify a given analyte and may be used to quantify organic compounds. Quantitative nuclear magnetic resonance spectroscopy (q-NMR) of acetylsalicylic acid (ASA) was conducted using tert-butyl alcohol (tert-butanol) as the internal standard and deuterated chloroform (CDCl3) as the solvent. Preparations of ASA solutions in low and high concentration ranges, 1.0 mM – 10.1 …


Study And Identification Of Environmental Nanoparticles In Governors State University (Gsu's) Agricultural Fields, Ekta Desai Apr 2013

Study And Identification Of Environmental Nanoparticles In Governors State University (Gsu's) Agricultural Fields, Ekta Desai

All Capstone Projects

Main purpose of this project is to study nanoparticles in Governors State University’s agricultural field and design experimental protocol for the same. Nanoparticles have one dimension that measures between 1 - 100 nanometers or less. Nanoparticles are widely used in day to day life such as in medicines, textiles, manufacturing and cosmetics. Due to their wide use, they can enter environment through many ways such as accidental spills during handling. Waste water treatment plant disposal serves as a main source of their entrance into the environment. Analysis of nanoparticles in environmental samples presents a number of challenges, including separation and …