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A New And Convenient Method Of Generating Alkyl Isocyanates From Alcohols, Thiols, And Trimethylsilyl Ethers Using A 2,4,6-Trichloro[1,3,5] Triazine/N-Bu_4nocn, Batool Akhlaghinia, Sima Samiei
A New And Convenient Method Of Generating Alkyl Isocyanates From Alcohols, Thiols, And Trimethylsilyl Ethers Using A 2,4,6-Trichloro[1,3,5] Triazine/N-Bu_4nocn, Batool Akhlaghinia, Sima Samiei
Turkish Journal of Chemistry
Alkyl isocyanates are prepared in good to excellent yields by treatment of alcohols, thiols, and trimethylsilyl ethers with 2,4,6-trichloro[1,3,5] triazine/n-Bu_4NOCN in acetonitrile. This method is highly selective for conversion of 1° alcohols to alkyl isocyanates in the presence of 2° and 3° alcohols, thiols, and trimethylsilyl ethers.
Efficient Method For Tetrahydropyranylation Of Phenols And Alcohols Using 2,4,6-Trichloro[1,3,5]Triazine, Batool Akhlaghinia, Elham Roohi
Efficient Method For Tetrahydropyranylation Of Phenols And Alcohols Using 2,4,6-Trichloro[1,3,5]Triazine, Batool Akhlaghinia, Elham Roohi
Turkish Journal of Chemistry
Alcohols and phenols were tetrahydropyranylated in the presence of 2,4,6-trichloro[1,3,5]triazine in good to excellent yields in acetonitrile.