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Dental Public Health and Education Commons

Open Access. Powered by Scholars. Published by Universities.®

SelectedWorks

2011

Microcapsules; micro-cracking; in situ polymerization; self-healing; material; polyurea microcapsules; encapsulation; composites; SELF-REPAIR; CULTURE-CONDITIONS; COMPOSITE RESIN; DENTAL PULP STEM CELL; FUNCTIONALLY GRADED DESIGN; MULTI LAYERED POST; FUNCTIONALLY GRADED DENTAL POST; SOFT SKILLS; CLINICAL PAIRING; DENTAL PULP STROMAL CELLS; LONG-TERM EXPANSION

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Full-Text Articles in Dental Public Health and Education

Optimization Of Microencapsulation Process For Self-Healing Polymeric Material, Noor Hayaty Abu Kasim Abu Kasim N.H. Jan 2011

Optimization Of Microencapsulation Process For Self-Healing Polymeric Material, Noor Hayaty Abu Kasim Abu Kasim N.H.

Noor Hayaty Abu Kasim Abu Kasim N.H.

A series of poly(urea-formaldehyde) (PUF) microcapsules filled with dicyclopentadiene (DCPD) was successfully prepared by in situ polymerization. The effect of diverse process parameters and ingredients on the morphology of the microcapsules was observed by SEM, optical microscopy (OM) and digital microscopy. Different techniques for the characterization of the chemical structure and the core content were considered such as FT-IR and (1)H-NMR as well as the characterization of thermal properties by DSC. High yields of free flowing powder of spherical microcapsules were produced. The synthesized microcapsules can be incorporated into another polymeric host material. In the event the host material cracks …