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Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu Jan 2006

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

The research objectives of this project were as follows:

  • To generate calibration curves of voltage versus oxygen concentration for the YSZ oxygen sensor system under various temperatures in liquid LBE.
  • To determine the sensor characteristics of the YSZ sensor system.
  • To determine oxygen dissolving rates in LBE under different temperatures in vitro.
  • To study the effects of unwanted electrical conductivity, contributed by the mobility of the electrons at high temperatures, for more accurate oxygen measurement.
  • To study alternative and promising oxygen measuring methods.


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Jan. 01 – March. 31, 2005), Yingtao Jiang, Bingmei Fu Mar 2005

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Jan. 01 – March. 31, 2005), Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

We performed data analysis on the data collected from LANL test loop. One student was been hired to perform the data analysis. A new proposal is submitted to TRP program. We have one paper accepted for publication in International Journal of Heat and Mass Transfer, and another paper accepted for oral presentation by IEEE International Symposium of Circuits and Systems for the track Chemical Sensors. A manuscript regarding to the RGA analysis for the calibration of oxygen sensor is on the way.


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu Jan 2005

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

Although liquid lead-bismuth eutectic (LBE) is a good candidate for the coolant that can be employed in a subcritical transmutation blanket, it is known to be very corrosive to stainless steel, the material used in the containment structure. To mitigate this problem, trace levels of oxygen can be introduced into the system, causing the formation of a protective oxide layer at the interface between the LBE and steel. The proper formation of this oxide layer largely depends on the accurate measurement and subsequent control of the oxygen concentration in liquid LBE.

Yttria Stabilized Zirconia (YSZ) oxygen sensors, using molten bismuth …


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (July 1 – Sept. 30, 2004), Yingtao Jiang, Bingmei Fu Sep 2004

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (July 1 – Sept. 30, 2004), Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

Dr. Jiang Ma and Mr. Xiaolong Wu worked in LANL between July 1 and Sept. 15 to conduct the experiment. Test of the corrosion of different materials in LBE was performed. The influence of the process of gas introduction to the LBE was studied. Data analysis work was performed based on accumulated data. In the same time, progress has been made in the simulation for transport in oxygen mixing, and one paper was presented in a conference. Another paper was composed and submitted to IEEE International Symposium of Circuits and Systems for the track Chemical Sensors. Preparation of a paper …


Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy Apr 2004

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada Las Vegas (UNLV) and Idaho State University (ISU) is to evaluate the feasibility of determining residual stresses of welded, bent (three-point-bend), and cold-worked engineering materials using a new nondestructive technique based on positron annihilation spectroscopy (PAS). The proposed technique is to use γ-rays from a small MeV electron linear accelerator (Linac) to generate positrons inside the test sample via 2 pair production. This method can be used for materials characterization and investigation of defects in thick samples that usually cannot be accomplished by conventional positron technique or other …


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu, Woosoon Yim Jan 2004

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

Lead-bismuth eutectic (LBE) is a candidate as a spallation target in sub-critical transmutation systems and as a coolant in nuclear programs. One of the primary concerns with LBE systems is the corrosion of stainless steel, the primary structural material used in nuclear systems. To mitigate this problem, trace levels of oxygen can be introduced into the system, causing the formation of a protective oxide layer at the interface between the LBE and steel. To protect the steel components, this oxide layer must be properly maintained. However, too much oxygen will produce unwanted oxide precipitation within the coolant and elsewhere in …


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Aug. 01 – Oct. 31, 2003), Yingtao Jiang, Bingmei Fu Oct 2003

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Aug. 01 – Oct. 31, 2003), Yingtao Jiang, Bingmei Fu

Transmutation Sciences Materials (TRP)

The experimental setup designed and manufactured in UNLV was shipped to LANL in early Aug. One student has been working in LANL to conduct the experiment since then. In the meantime, one new Ph. D. student has started to run the simulation for transport in oxygen mixing. In Oct., a professional has been hired to work in both experimental and the theoretical studies pertaining to the proposed work.


Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements: Quarterly Progress Report (June 01 – August 31, 2003), Ajit K. Roy Oct 2003

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements: Quarterly Progress Report (June 01 – August 31, 2003), Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada Las Vegas (UNLV), the Idaho State University (ISU), and the Los Alamos National Laboratory (LANL) is to evaluate the feasibility of determining residual stresses in cold-worked, plastically-deformed (bent), and welded materials using a nondestructive method based on positron annihilation spectroscopy (PAS). This technique uses γ-rays from a small MeV electron Linac to generate positrons inside the sample via pair production. This method is known to have capabilities of characterizing defects in thick specimens that could not be accomplished by conventional positron technique or other nondestructive methods. The generated …


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (May. 01 – July 31, 2003), Yingtao Jiang, Bingmei Fu, Woosoon Yim Jul 2003

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (May. 01 – July 31, 2003), Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

The report for Y01 has been prepared and submitted. The final part of our apparatus, the N3Si4 stirrer, was received by the end of May. The assembly of the apparatus has almost been completed. The control plan for our apparatus has been revised. To run FLUENT, a high-end Unix-based Sun workstation has been acquired. Plan has been made to ship our apparatus to LANL.


Study Of Geometric Effects On Local Corrosion Rates For Lbe Loop, Chao Wu Jul 2003

Study Of Geometric Effects On Local Corrosion Rates For Lbe Loop, Chao Wu

UNLV Theses, Dissertations, Professional Papers, and Capstones

Corrosion is an extremely important issue in nuclear cooling system applications. Many scientific and engineering efforts have been contributed to the research of finding an ideal material, which has resistance to corrosive Lead Bismuth Eutectic (LBE). A Delta Loop was designed and constructed in Los Alamos National Lab (LANL) to obtain the experimental data. This loop is a multi-section closed system that differs in diameter from one part to another. As a result, an intensive study on the geometry effect is hence necessary and valuable. In this thesis, this problem was simulated by commercial software STAR-CD. Results provide a good …


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Feb. 01 – Apr. 30, 2003), Yingtao Jiang, Bingmei Fu, Woosoon Yim Apr 2003

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Feb. 01 – Apr. 30, 2003), Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

We received most of the components, everything except the customized and outsourced stirrer, for the new apparatus for oxygen measurement/calibration. Thus far, most of the machining work has been completed. The LaveView module used for the data collection and the control of the apparatus has been tested. 2-D simulation work has been performed using FEMLAB.


Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy Feb 2003

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada, Las Vegas (UNLV) and the Idaho State University (ISU) is to evaluate the feasibility of determining residual stresses of welded, bent (three-point-bend), and cold-worked engineering materials using a new nondestructive technique based on positron annihilation spectroscopy. The proposed technique is to use x-rays from a small MeV electron Linac to generate positrons inside the sample via pair production. This method can be used for materials characterization and investigation of defects in thick samples that could not be accomplished by conventional positron technique or other nondestructive methods. The data …


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Nov. 01 – Jan. 31, 2002), Yingtao Jiang, Bingmei Fu, Woosoon Yim Jan 2003

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Nov. 01 – Jan. 31, 2002), Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

The design of the new apparatus for oxygen measurement/calibration has been completed. This new apparatus shall be of great importance for the UNLV researchers to conduct the research work in the campus.


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu, Woosoon Yim Jan 2003

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic, Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

Lead-bismuth eutectic (LBE) is a candidate as a spallation target in sub-critical transmutation systems and as a coolant in nuclear programs. One of the primary concerns with LBE systems is the corrosion of stainless steel, the primary structural material used in nuclear systems. To mitigate this problem, trace levels of oxygen can be introduced into the system, causing the formation of a protective oxide layer at the interface between the LBE and steel. To protect the steel components, this oxide layer must be properly maintained. However, too much oxygen will produce unwanted oxide precipitation within the coolant and elsewhere in …


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Aug. 01 – Oct. 31, 2002), Yingtao Jiang, Bingmei Fu, Woosoon Yim Oct 2002

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (Aug. 01 – Oct. 31, 2002), Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

After two month intensive work in LANL, some preliminary sensor calibration curves have been obtained. Further data analysis shall be performed to assess the theoretical and measured data. Also, a new experimental apparatus shall be designed and located in UNLV to continue the left work.

Technical Progress:

• A set of calibration curves of voltage vs. temperature ranging from 3000C to 5000C under various oxygen concentrations in liquid LBE for the YSZ oxygen sensor has been obtained and has been reported in one paper.

• A meeting with LBE committee and other faculty members in AAA …


Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements: Quarterly Progress Report (June 1 – August 31, 2002), Ajit K. Roy Aug 2002

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements: Quarterly Progress Report (June 1 – August 31, 2002), Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada Las Vegas (UNLV), the Idaho State University (ISU), and the Los Alamos National Laboratory (LANL) is to evaluate the feasibility of determining residual stresses in cold-worked, plastically-deformed, and welded materials using a nondestructive method based on positron annihilation spectroscopy. This technique uses γ-rays from a small MeV electron Linac to generate positrons inside the sample via pair production. This method is known to have capabilities of characterizing defects in thick specimens, that could not be accomplished by conventional positron technique or other nondestructive methods. The generated data will …


Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (May 01 – July 31, 2002), Yingtao Jiang, Bingmei Fu, Woosoon Yim Jul 2002

Developing A Sensing System For The Measurement Of Oxygen Concentration In Liquid Pb-Bi Eutectic: Quarterly Progress Report (May 01 – July 31, 2002), Yingtao Jiang, Bingmei Fu, Woosoon Yim

Transmutation Sciences Materials (TRP)

Accurate measurement of the oxygen concentration in liquid Lead-Bismuth Eutectic (LBE) cooling system is critical in the active control of the corrosion at the interface between LBE and the stainless steel of transport tubes. Currently, LANL (Los Alamos National Laboratory) scientists have employed an automobile-style YSZ (Yttria Stabilized Zirconia) oxygen sensor unit to measure oxygen levels in an engineeringscaled LBE test system. Although the theoretical model for calculating oxygen concentration based on voltage measurement of YSZ sensor in static conditions is well understood, there is an urgent and strong need to obtain a complete set of calibration curves for YSZ …


Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy Apr 2002

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada, Las Vegas (UNLV) and Idaho State University (ISU) is to evaluate the feasibility of determining residual stresses of welded (after pre-straining) engineering materials using a new nondestructive technique based on positron annihilation spectroscopy. The proposed technique is to use γ-rays 2 from a small MeV electron Linac to generate positrons inside the sample via pair production. This method can be used for materials characterization and investigation of defects in thick samples that could not be accomplished by conventional positron techniques or other nondestructive methods. The data generated will …