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Full-Text Articles in Mechanical Engineering
The Effects Of Thermal Procedure On Transformation Temperature, Crystal Structure And Microstructure Of Cu-Al-Co Shape Memory Alloy, Y. Aydoğdu, M. Kök, F. Dağdelen, A. Aydoğdu, Ali S. Turabi, Haluk E. Karaca
The Effects Of Thermal Procedure On Transformation Temperature, Crystal Structure And Microstructure Of Cu-Al-Co Shape Memory Alloy, Y. Aydoğdu, M. Kök, F. Dağdelen, A. Aydoğdu, Ali S. Turabi, Haluk E. Karaca
Mechanical Engineering Faculty Publications
The purpose of this study is to investigate the effects of different thermal procedures of the Cu-Al-Co shape memory alloy on its crystal structure, transformation temperature and microstructure. The alloys were subjected to a heat treatment and then cooling was applied at four different conditions. After the thermal process, XRD, DSC, optical microscopy and micro-hardness measurements were carried out. The experimental studies showed that crystal structure, microstructure and transformation temperature of Cu-Al-Co alloy were changed from the cooling conditions.
A New Method Of Synthesizing Black Birnessite Nanoparticles: From Brown To Black Birnessite With Nanostructures, Shizhi Qian, Marcos A. Cheney, Pradip K. Bhowmik, Sang W. Joo, Wensheng Hou, Joseph M. Okoh
A New Method Of Synthesizing Black Birnessite Nanoparticles: From Brown To Black Birnessite With Nanostructures, Shizhi Qian, Marcos A. Cheney, Pradip K. Bhowmik, Sang W. Joo, Wensheng Hou, Joseph M. Okoh
Mechanical Engineering Faculty Research
A new method for preparing black birnessite nanoparticles is introduced. The initial synthesis process resembles the classical McKenzie method of preparing brown birnessite except for slower cooling and closing the system from the ambient air. Subsequent process, including wet-aging at 7◦C for 48 hours, overnight freezing, and lyophilization, is shown to convert the brown birnessite into black birnessite with complex nanomorphology with folded sheets and spirals. Characterization of the product is performed by X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), thermogravimetric analysis (TGA), and N2 adsorption (BET) techniques. Wet-aging and lyophilization times are shown to …