Other Materials Science and Engineering Commons^™

Mechanical Characterization Of Selectively Laser Melted 316l Stainless Steel Body Centered Cubic Unit Cells And Lattice Of Varying Node Radii And Strut Angle, Christopher James Hornbeak

Master's Theses

An experimental study of several variants of radius and strut angle of the body centered cubic unit cell was performed to determine the mechanical properties and failure mechanisms of the mesostructure. Quasi static compression tests were performed on an Instron® universal testing machine with a 50kN load cell at 0.2mm/min. The test samples were built using a SLM Solutions 125 selective laser melting machine with 316L stainless steel. Test specimens were based on 5mm cubic unit cells, with a strut diameter 10% of the unit cell size, with skins on top and bottom to provide a cantilever boundary constraint. Specimens …

The Effect Of Biocomposite Material In A Composite Structure Under Compression Loading, Benjamin Andrew Sweeney

Master's Theses

While composite structures exhibit exceptional strength and weight saving possibilities for engineering applications, sometimes their overall cost and/or material performance can limit their usage when compared to conventional structural materials. Meanwhile ‘biocomposites’, composite structures consisting of natural fibers (i.e. bamboo fibers), display higher cost efficiency and unique structural benefits such as ‘sustainability’. This analysis will determine if the integration of these two different types of composites are beneficial to the overall structure. Specifically, the structure will consist of a one internal bamboo veneer biocomposite ply; and two external carbon fiber weave composite plies surrounding the bamboo biocomposite. To acquire results …

Evaluation Of Efficiency Of Various Materials To Shield From Radiation In Space Using The Monte Carlo Transport Code Called Fluka, Roman Savinov

Master's Theses

The purpose of this study is to improve spacecraft shielding from radiation in space. It focuses on the evaluation of shielding efficiency of different materials. The efficiency of a shield is evaluated by the dose profile within the shield and the amount of dose absorbed by a target using the Monte Carlo transport code called FLUKA. The output of this code is validated by recreating the experiments from published papers and comparing the results. Once the FLUKA’s output is validated, the efficiency of sixteen materials, subject to SPE and GCR sources, are evaluated. The efficiency comparison is made by fixing …

Effect Of Surfactant Architecture On Conformational Transitions Of Conjugated Polyelectrolytes, Greg A. Braggin

Master's Theses

Water soluble conjugated polyelectrolytes (CPEs), which fall under the category of conductive polymers, possess numerous advantages over other conductive materials for the fabrication of electronic devices. Namely, the processing of water soluble conjugated polyelectrolytes into thin film electronic devices is much less costly as compared to the processing of inorganic materials. Moreover, the handling of conjugated polyelectrolytes can be performed in a much more environmentally friendly manner than in the processing of other conjugated polymers because conjugated polyelectrolytes are water soluble, whereas other polymers will only dissolve in toxic organic solvents. The processing of electronic devices containing inorganic constituents such …

An Investigation Into The Properties And Fabrication Methods Of Thermoplastic Composites, Ann E. Livingston-Peters

Master's Theses

As applications for thermoplastic composites increase, the understanding of their properties become more important. Fabrication methods for thermoplastic composites continually improve to match designs specifications. These advanced thermoplastics have begun to show an improvement in mechanical properties over those found in thermoset composites commonly used in industry. Polyaryletherketones (PEK) have high service temperatures, good mechanical properties, and improved processing capabilities compared to thermoplastics used in the past making them important to the aerospace industry. The wide range of types of PEK make them suitable for a variety of applications, but selection of specific chemistries, processing parameters, and composite stack-ups determine …

Developent Of A Phospholipid Encapsulation Process For Quantum Dots To Be Used In Biologic Applications, Logan Grimes

Master's Theses

The American Cancer Society predicts that 1,665,540 people will be diagnosed with cancer, and 585,720 people will die from cancer in 2014. One of the most common types of cancer in the United States is skin cancer. Melanoma alone is predicted to account for 10,000 of the cancer related deaths in 2014. As a highly mobile and aggressive form of cancer, melanoma is difficult to fight once it has metastasized through the body. Early detection in such varieties of cancer is critical in improving survival rates in afflicted patients. Present methods of detection rely on visual examination of suspicious regions …

Mode I Fracture Toughness Of Eight-Harness-Satin Carbon Cloth Weaves For Co-Cured And Post-Bonded Laminates, Josh E. Smith

Master's Theses

Mode I interlaminar fracture of 3k 8-Harness-Satin Carbon cloth, with identical fill and weft yarns, pre-impregnated with Newport 307 resin was investigated through the DCB test (ASTM D5528). Crack propagations along both the fill and weft yarns were considered for both post-bonded (co-bonded) and co-cured laminates. A patent-pending delamination insertion method was compared to the standard Teflon film option to assess its applicability to mode I fracture testing. The Modified Beam Theory, Compliance Calibration method, and Modified Compliance Calibration method were used for comparative purposes for these investigations and to evaluate the validity of the proposed Equivalent Stiffness (EQS) method. …

Soil Nutrient Availability Properties Of Biochar, Nicole C. Esposito

Master's Theses

Biochar’s high porosity and negative surface charge allows for numerous soil and plant benefits such as increased water retention, high nutrient availability, and plant growth. By analysing biochar’s effect of all of these factors, a system can be put in place in which soils can be remediated with the proper soil amendments. This report discusses and tests the effects of varying rates of biochar on pH levels, cation exchange capacity, and nutrient exchangeability (of calcium, magnesium, sodium, and potassium) in soil. Corn plants were also grown in soils of varying amendment types and analysed for plant growth and germination to …

Analysis Of Bimetallic Adhesion And Interfacial Toughness Of Kinetic Metallization Coatings, Alec D. Guraydin

Master's Theses

Due to their ability to confer enhanced surface properties without compromising the properties of the substrate, coatings have become ubiquitous in heavy industrial applications for corrosion, wear, and thermal protection, among others. Kinetic Metallization (KM), a solid-state impact consolidation and coating process, is well-suited for depositing industrial coatings due to its versatility, low substrate heat input, and low cost. The ability of KM coatings to adhere to the substrate is determined by the quality of the interface. The purpose of this study is to develop a model to predict the interfacial quality of KM coatings using known coating and substrate …

Deposition, Characterization, And Fabrication Of A Zinc Oxide Piezoelectric Thin Film Microspeaker Using Dc Reactive Sputtering, Adam Olzick

Master's Theses

A piezoelectric microspeaker device that could be used in a variety of acoustic applications was designed and fabricated using a thin film ZnO layer that was reactively DC sputtered onto a single crystalline n-type silicon substrate. When tested the microspeaker did not produce sound due to complications in the etching process, the thickness of the diaphragms, and clamping effects. Instead, a characterization approach was taken and the structural, optical, electrical, and piezoelectric properties of the ZnO were investigated. Scanning electron microscopy, x-ray diffraction, and atomic force microscopy were utilized to discover the ZnO’s structural properties. Using the XRD and SEM, …

Characterization Of Mixing In A T-Style Microfluidic Chip, Brian Eric Harley

Master's Theses

The goal of this study is to characterize the mixing that occurs in a microfluidic chip. To characterize the mixing, the minimum length to complete mixing and evolution of mixing will be investigated. There are two types of mixing that occur within a microfluidic channel, diffusion and advection. In the beginning of the microfluidic chip, diffusion is the dominant form of mixing, and in the later portion of the microfluidic chip advection is the dominant form of mixing. The type of design used for this experiment was a zig zag geometry microfluidic chip with channel dimensions of 60 µm X …

Design, Fabrication, And Characterization Of A Thin-Film Nickel-Titanium Shape Memory Alloy Diaphragm For Use In Micro-Electro-Mechanical Systems, Brian Joel Alvarez

Master's Theses

Previous work done at Cal Poly has shown that thin-film nickel-titanium (NiTi) can be easily sputtered onto silicon wafers and annealed to create a crystallized shape memory alloy (SMA) film. Initial work on creating devices yielded cantilevers that were highly warped due to thin-film stress created during the sputtering process. The objective of this work was to create a thin-film NiTi SMA device that could be better characterized. A membrane was selected due to the simplicity of fabrication and testing which would also oppose the thin-film stress due to the increase in attachment points to the substrate.

Silicon wafers were …

Investigating Wood Welding Parameters Using A Prototype Welding Machine, Timothy R. Melin

Master's Theses

Understanding how different processing variables influence wood welded bonds is vital if the technique will ever be used to create engineered lumber without using adhesives. A variation of vibration welding, wood welding uses pressure and friction to bond materials together. During welding, heat causes a softening in the wood, a naturally occurring composite material. This softening leads to fiber entanglement and a bond forms upon cooling.

The goal of this research was to investigate several processing aspects of the wood welding procedure. A prototype wood welding machine, designed and fabricated from the ground up, was used to investigate the effects …

Nanoindentation Of Annealed And As-Sputtered Thin Films Of Nickel Titanium Shape Memory Alloys, Matthew Tyson Lewis

Master's Theses

The bottom-up processing techniques used for making Microelectromechanical systems (MEMS) devices can produce material properties different from bulk processing. The material properties must be evaluated with the process parameters used and for changes in the process parameters. The mechanical properties are needed to design MEMS devices. A material of interest for MEMS devices is nickel titanium (NiTi) shape memory alloy (SMA) because of the high work output (~107 J/m3). This thesis will focus on the fabrication of thin film NiTi by DC magnetron sputtering deposition and testing mechanical properties of the fabricated films by nanoindentation. Thin film NiTi SMA was …

The Effects Of Applied Strain And Heat Treatment On The Properties Of Niti Wire During Shape Setting, Frank Zapoticla

Master's Theses

NiTi components are commonly subjected to thermo-mechanical heat treatments during production and fabrication. This study investigates the effects of applied strain of 0-10% and heat treatments of 300-600ºC for times of 2-30 minutes during shape-setting of Ti–50.8 at% Ni wire with a nominal diameter of 0.495 mm and an initial transition temperature, Af, of 12ºC. Strain was applied prior to heat treatments by coiling NiTi wire, essentially producing coiled springs, around different diameter steel mandrels to obtain different strain levels. The samples of NiTi wire under applied strain were heat treated in a salt bath, followed by a rapid quench. …

Tribological Comparison Of Traditional And Advanced Firearm Coatings, Greg Boban

Master's Theses

The objective of this project is to find which type of coating has the best performance characteristics for finishing firearms. This is accomplished by measuring and comparing several performance characteristics, such as: adhesion, hardness, wear resistance, friction control, and corrosion resistance. Appearance is not a factor since any exterior coating that is flashy can be subdued or camouflaged with special purpose paints, which have proven durable enough for such purposes. Cost will not be a limiting factor for this experiment, but will be discussed in the conclusion as a secondary concern. This data will be used to identify the best …

The Characterization And Analysis Of In-Vitro And Elevated Temperature Repassivation Of Ti-6al-4v Via Afm Techniques, Aaron J. Guerrero

Master's Theses

ABSTRACT

The Characterization and Analysis of In-vitro and Elevated Temperature Repassivation of

Ti-6Al-4V via AFM Techniques

Aaron J Guerrero

Research in the corrosion of orthopaedic implants is a growing research field where implants have been known to show adverse effects in patients who have encountered the unfortunate dissolution of their implants due to corrosion. Once corrosion begins within the body, many adverse biological reactions can occur such as late on-set infections resulting in severe health complications. The focus of this research is specifically related to the problem of late on-set infections caused by localized corrosion of orthopaedic implants. In medical …

Time-Temperature Curing Relationship Of An Adhesive Binder With Rice Straw, Kevin Ka-Wan Ng

Master's Theses

Rice straw is a global and proliferate agricultural waste whose production grossly outstrips viable uses. Current disposal methods are not sustainable, and more convenient methods – such as incineration – exude poor environmental stewardship. Although the direct use of straw bales in building construction presents a practical and sustainable alternative, engineering challenges associated with using it prevent its wide adoption. The Stak Block – a composite formed from compressed rice straw and a heat-cured adhesive – may overcome challenges associated with straw bale building. However, the times and temperatures needed to cure the binder with straw are not well understood. …

Design And Development Of Rapid Battery Exchange Systems For Electric Vehicles To Be Used As Efficient Student Transportation, Jonathan A. Bevier

Master's Theses

Rapid battery exchange systems were built for an electric van and pedal assist electric bike as a method of eliminating the need to recharge the vehicles batteries in order to increase the feasibility of using electric propulsion as a method of efficient student transportation. After selecting proper materials it was found that the systems would need a protective coating to ensure consistent operation. 1020 cold rolled steel samples coated with multiple thicknesses of vinyl resin paint, epoxy resin paint, and powder coating were subjected to environmental wear tests in order to determine if the type and thickness of common protective …

Characterization Of A Viscoelastic Response From Thin Metal Films Deposited On Silicon For Microsystem Applications, Steven L. Meredith

Master's Theses

Understanding the mechanisms that control the mechanical behavior of microscale actuators is necessary to design an actuator that responds to an applied actuation force with the desired behavior. Micro actuators which employ a diaphragm supported by torsional hinges which deform during actuation are used in many applications where device stability and reliability are critical. The material response to the stress developed within the hinge during actuation controls how the actuator will respond to the actuating force. A fully recoverable non-linear viscoelastic response has been observed in electrostatically driven micro actuators employing torsional hinges of silicon covered with thin metal films. …

Effectiveness Of Thermal Oxidation In Relation To Anterior Cervical Plates, Katherine A. Miyashiro

Master's Theses

Ti-6Al-4V anterior cervical plates (ACP) are used in spinal fusion surgeries to fixate cervical vertebrae during graft adhesion. However, documented cases of implant failure and the potential for ACP corrosion raise concerns regarding any degradation of material resulting from extended implantation. In addition, abrasion during implantation may damage a section of the protective oxide layer, potentially exposing surrounding tissues to the harmful effects of bare titanium, aluminum, and vanadium. Thermal oxidation has been shown to improve corrosion-resistance and wear-resistance, depending on temperature and time. To quantify the attributes of the thermally grown oxide layer, Ti-6Al-4V coupons underwent thermal oxidation treatments …