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Ceramic Materials

Theses and Dissertations

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Tension-Tension Fatigue Behavior Of Nextel™ 720/Alumina-Mullite Ceramic Composite At 1200°C In Air And In Steam, Sarah A. Witzgall Jun 2020

Tension-Tension Fatigue Behavior Of Nextel™ 720/Alumina-Mullite Ceramic Composite At 1200°C In Air And In Steam, Sarah A. Witzgall

Theses and Dissertations

Uniaxial tension-tension fatigue performance of an oxide-oxide continuous fiber ceramic composite was studied at 1200°C in laboratory air and in steam. The composite is reinforced with laminated, 0/90 mullite/alumina (NEXTEL™720) fibers woven in an eight-harness satin weave and has a porous alumina/mullite matrix. There is no interphase between the fiber and matrix. The composite relies on the porous matrix for crack deflection and flaw tolerance. Tension-tension fatigue was examined for maximum stresses of 45 – 136 MPa in air and in steam. To assess the effects of the steam environment on fatigue performance, experimental results obtained in air are compared …

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Fatigue Behavior Of An Advanced Melt-Infiltrated Sic/Sic Composite With Environmental Barrier Coating At 1200°C In Air And In Steam, Thaddeus M. Williams Mar 2020

Fatigue Behavior Of An Advanced Melt-Infiltrated Sic/Sic Composite With Environmental Barrier Coating At 1200°C In Air And In Steam, Thaddeus M. Williams

Theses and Dissertations

Advanced aerospace applications such as aircraft turbine engine components, hypersonic flight vehicles, and spacecraft reentry thermal protection systems require structural materials that have superior long-term mechanical properties under high temperature, high pressure, and varying environmental factors, such as moisture. Because of their low density, high strength and fracture toughness at high temperatures SiC fiber-reinforced SiC matrix composites are being evaluated for aircraft engine hot-section components. In these applications the composites will be subjected to various types of mechanical loadings at elevated temperatures in oxidizing environments. Because their constituents are intrinsically oxidation-prone, the most significant problem hindering SiC/SiC composites is oxidation …

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Ballistic Evaluation Of Carbon Nanotube Sheet Material In Multifunctional Applications, Casey M. Keilbarth Mar 2019

Ballistic Evaluation Of Carbon Nanotube Sheet Material In Multifunctional Applications, Casey M. Keilbarth

Theses and Dissertations

Significant development of carbon nanotubes has occurred since they were first studied in the 1990's. Attempts to capture the phenomenal molecular properties in practical applications are gaining ground as new methods of producing CNTs have been developed. This thesis sought to determine if the addition of commercially produced CNT sheets to thin carbon fiber panels improved the ballistic properties of the panel. The difference between 0 and 4 CNT sheets was studied. The hypothesis was that inte- grating CNT sheets into the laminate would increase the projectile energy absorbed by the panel and reduce the damage to the panel incurred …

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Creep Of Hafnium Diboride -20 Vol% Silicon Carbide At 1500°C In Air, Glen E. Pry Mar 2018

Creep Of Hafnium Diboride -20 Vol% Silicon Carbide At 1500°C In Air, Glen E. Pry

Theses and Dissertations

Refractory metal borides, commonly referred to as Ultra High Temperature Ceramics (UHTCs), exhibit a number of unique properties, such as extremely high melting temperature and hardness, chemical stability, high electrical and thermal conductivity and corrosion resistance. It has been demonstrated that the addition of SiC improves the oxidation resistance of ZrB2- and HfB2-based UHTCs above 1200°C by modifying the composition of the oxide scale. Addition of SiC retards the oxidation rate of ZrB2 and HfB2 by forming a protective layer of borosilicate glass. Creep deformation is one of the critical criterion for structural application of ceramics at elevated temperatures. Compression …

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Experimental Investigation Of Mechanical Behavior Of An Oxide/Oxide Ceramic Composite In Interlaminar Shear And Under Combined Tension-Torsion Loading, Skyler R. Hilburn Mar 2014

Experimental Investigation Of Mechanical Behavior Of An Oxide/Oxide Ceramic Composite In Interlaminar Shear And Under Combined Tension-Torsion Loading, Skyler R. Hilburn

Theses and Dissertations

Creep behavior in interlaminar shear of an oxide-oxide ceramic composite, Nextel 720™/aluminosilicate (N720/AS), was investigated at 1100°C in laboratory air and in steam. The interlaminar shear strength (ILSS) was determined as 7.65 MPa. The creep behavior was examined for interlaminar shear stresses in the 2-6 MPa range. Primary and secondary creep regimes were observed in all tests conducted in air and in steam. Tertiary creep was noted in the tests performed at 6 MPa. Larger creep strains and higher creep strain rates were produced in steam. Surprisingly, the presence of steam had a beneficial effect on creep lifetimes. It appears …

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Effects Of Environment On Creep Behavior Of Two Oxide-Oxide Ceramic Matrix Composites At 1200°C, Pavlos Koutsoukos Sep 2006

Effects Of Environment On Creep Behavior Of Two Oxide-Oxide Ceramic Matrix Composites At 1200°C, Pavlos Koutsoukos

Theses and Dissertations

Previous studies by the advisor and graduate students examined creep behavior of the Nextel720/Alumina CMC in air and in 100% steam environments at 1200 and 1330°C. Results showed that while this oxide/oxide system exhibits an exceptionally high fatigue limit at 1200°C it also experiences substantial strain accumulation under sustained loading conditions. Furthermore, these earlier investigations revealed a significant degrading effect of 100% steam environment on material performance under both static and cyclic loadings. The present effort will investigate creep rupture behavior of Nextel720/Alumina composite in the inert gas environment. In addition, creep rupture behavior of Nextel720/Aluminosilicate CMC will be investigated …

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Effects Of Frequency And Environment On Fatigue Behavior Of An Oxide-Oxide Ceramic Matrix Composite At 1200°C, Griffin Hetrick Jun 2006

Effects Of Frequency And Environment On Fatigue Behavior Of An Oxide-Oxide Ceramic Matrix Composite At 1200°C, Griffin Hetrick

Theses and Dissertations

Advances in aeronautical engineering in the 21st century depend upon materials that can perform well in extreme environments such as high temperatures and oxidizing conditions. Nextel™720/Alumina (N720/A) is an oxide/oxide ceramic matrix composite with a porous alumina matrix that has been identified as a candidate material for such applications. This research investigated the effects of frequency on fatigue response of N720/A at 1200°C in both air and steam environment. Prior investigation of this material by Eber [8] in 2005 studied fatigue behavior at 1200°C in air and in steam environments at the frequency of 1.0 Hz. The current research focused …

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Effect Of Environment On Creep Behavior Of An Oxide/Oxide Cfcc With ±45° Fiber Orientation, Gregory T. Siegert Jun 2006

Effect Of Environment On Creep Behavior Of An Oxide/Oxide Cfcc With ±45° Fiber Orientation, Gregory T. Siegert

Theses and Dissertations

Aerospace applications require materials capable of maintaining superior mechanical properties while operating at high temperatures and oxidizing environments. Nextel™ 720/A (N720/A), an oxide/oxide ceramic matrix composite (CMC) with a porous alumina matrix was developed specifically to provide improved long-term properties and performance at 1200°C. This research evaluated the creep behavior of N720/A with a ±45° fiber orientation at 1200°C in: laboratory air, steam, and argon environments. Creep-rupture tests at the creep stress levels of: 45, 40, 35, and 15 MPa were conducted in each environment.
The ultimate tensile strength of N720/A with ±45° fiber orientation was 55 MPa, the elastic …

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Effect Of Hold Times On Fatigue Behavior Of Nextel 720™/Alumina Ceramic Matrix Composite At 1200°C In Air And In Steam Environment, John M. Mehrman Mar 2006

Effect Of Hold Times On Fatigue Behavior Of Nextel 720™/Alumina Ceramic Matrix Composite At 1200°C In Air And In Steam Environment, John M. Mehrman

Theses and Dissertations

The aerospace field requires structural materials that can maintain superior mechanical properties while subjected to high temperatures and oxidizing environments. This research investigated the effect of hold times at maximum load on fatigue performance of a Nextel 720/Alumina ceramic matrix composite at 1200 C, explored the influence of environment on material response to cyclic loading with hold times at maximum load, and assessed the effects of loading history on material behavior and environmental durability. The N720/A composite relies on an oxide/oxide composition for inherent oxidation resistance and a porous matrix with no interphase between the fiber and matrix for damage …

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Creep-Rupture And Fatigue Behaviors Of Notched Oxide/Oxide Ceramic Matrix Composite At Elevated Temperature, Mark A. Sullivan Mar 2006

Creep-Rupture And Fatigue Behaviors Of Notched Oxide/Oxide Ceramic Matrix Composite At Elevated Temperature, Mark A. Sullivan

Theses and Dissertations

Oxide/oxide composites are being considered for use in high temperature aerospace applications where their inherent resistance to oxidation provides for better long life properties at high temperature than most other ceramic matrix composites (CMCs). One promising oxide/oxide CMC is Nextel 720/A (N720/A) which uses an 8-harness satin weave (8HSW) of Nextel 720 fibers embedded in a porous alumina matrix. Possible aerospace applications for N720/A will likely require inserting holes into the material for mounting and cooling purposes. The notch characteristics must be understood to ensure designs using the material are sufficient for the desired application. This research effort examined the …

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Characterization Of Compressive Creep Behavior Of Oxide/Oxide Composite With Monazite Coating At Elevated Temperature, Patrick R. Jackson Mar 2006

Characterization Of Compressive Creep Behavior Of Oxide/Oxide Composite With Monazite Coating At Elevated Temperature, Patrick R. Jackson

Theses and Dissertations

The compressive creep behavior of a N610/monazite/alumina composite was investigated in this work. The composite consists of a porous alumina matrix reinforced with NextelTM610 fibers coated with monazite in a symmetric cross-ply (0°/90°/0°/90°)s orientation. Compressive stress-strain behavior was investigated as well. The addition of monazite coating resulted in ~ 35% loss in compressive strength at 900°C and in ~45% loss in compressive strength at 1100°C. Compressive creep behavior was examined at 900 and 1100°C for creep stresses ranging from 50 to 95 MPa. Primary and secondary creep regimes were observed at both temperatures. Minimum creep rate was reached in all …

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Monotonic, Creep-Rupture, And Fatigue Behavior Of Carbon Fiber Reinforced Silicon Carbide (C/Sic) At An Elevated Temperature, John M. Engesser Mar 2004

Monotonic, Creep-Rupture, And Fatigue Behavior Of Carbon Fiber Reinforced Silicon Carbide (C/Sic) At An Elevated Temperature, John M. Engesser

Theses and Dissertations

The main objective of this research effort was to examine the impact that cyclic loading frequency has on the life of a C/SiC composite at an elevated temperature of 550°C. Cyclic loading of C/SiC was investigated at frequencies of 375 Hz, 10 Hz, 1 Hz, and 0.1 Hz. Creep-Rupture tests and tests that were combinations of creep-rupture and fatigue were also accomplished. A monotonic tensile test was performed at 550°C and compared to a room temperature monotonic test. This study showed that an elevated temperature of 550°C has very little effect on the Ultimate Tensile Strength (UTS) of C/SiC. The …

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Investigation Into The Behavior Of Geometrically Nonlinear Composite Arches, John C. Bailey Dec 1994

Investigation Into The Behavior Of Geometrically Nonlinear Composite Arches, John C. Bailey

Theses and Dissertations

This research modifies the existing finite element formulation of a potential energy based large deformation and moderate rotation theory. Hermitian shape functions replace the existing linear bending angle interpolations. Negligible differences between the two formulations indicate the underlying kinematics limit the accuracy, not the finite element interpolations. Using the new program, numerous nonlinear arch geometries are modeled to investigate the effects of arc length and thickness variations. Local and global snapping phenomena are captured as well as through the thickness shear driven nonlinearities.

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Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite At Elevated Temperature Under Tension-Tension Loading, Craig D. Steiner Dec 1994

Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite At Elevated Temperature Under Tension-Tension Loading, Craig D. Steiner

Theses and Dissertations

This study investigated the fatigue behavior and damage mechanisms of a [0-90]4s SiC-MAS ceramic matrix composite under tension-tension loading at two elevated temperatures and two frequencies. Stress and strain hystereses, maximum and minimum strain, and modulus of elasticity were evaluated to characterize the material behavior. Microscopy and fractography were used to evaluate damage progression and mechanisms. Fatigue life was independent of frequency at both temperatures.

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Characterization Of Fatigue Behavior Of 2-D Woven Fabric Reinforced Ceramic Matrix Composite At Elevated Temperature, Daniel J. Groner Dec 1994

Characterization Of Fatigue Behavior Of 2-D Woven Fabric Reinforced Ceramic Matrix Composite At Elevated Temperature, Daniel J. Groner

Theses and Dissertations

This study investigated the fatigue behavior and associated damage mechanisms in notched and unnotched enhanced Sic-SiC ceramic matrix composite specimens at 1100°C. Stiffness degradation, strain variation, and hysteresis were evaluated to characterize material behavior. Microscopic examination was performed to characterize damage mechanisms. During high cycle-low stress fatigue tests, far less fiber-matrix interface debond was evident than in low cycle-high stress fatigue tests. Notched specimens exhibited minimal stress concentration during monotonic tensile testing and minimal notch sensitivity during fatigue testing. Damage mechanisms were also similar to unnotched.

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Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite Subjected To Tension-Tension Cycling With Hold Time, Scott A. Grant Dec 1994

Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite Subjected To Tension-Tension Cycling With Hold Time, Scott A. Grant

Theses and Dissertations

This study was carried out to investigate the elevated temperature behavior of the SiC-MAS5 cross- ply [0-90]4S ceramic matrix composite manufactured by Corning Inc. to fatigue with loading waveforms that combine the characteristics of stress rupture and high cycle fatigue. The test results were compiled in the form of S-N (cycles to failure), S-T (exposure time versus cycles to failure), S-S (energy exposure versus cycles to failure), normalized modulus degradation, strain progression, and hysteresis loop progression. From the mechanical behavior demonstrated by these curves, relationships between the effect of the environment and loading waveform were developed. In addition, a …

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Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite At Elevated Temperatures Under Tension-Tension Loading, Richard J. Tuznik Dec 1993

Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite At Elevated Temperatures Under Tension-Tension Loading, Richard J. Tuznik

Theses and Dissertations

A study was conducted which investigated the behavior of a Nicalon/ Calcium-Aluminosilicate (Nicalon/CAS) cross-ply [0/90]2S ceramic matrix composite at elevated temperatures under tension-tension fatigue loading. Tension-tension fatigue tests were performed with a load ratio of R = 0.10 and a frequency of 10 Hertz at 700°C and 850°C. These results were compared to results from a previous study conducted at room temperature. Material behavior and damage was recorded by fatigue life curves, elastic modulus' maximum and minimum strain, acetate replication techniques, and post-mortem fractography. Analysis of these results showed identical matrix dominated damage behavior at RT and 700°C. Ultimate …

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Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite Under Strain Controlled Tension-Tension And Tension-Compression Loading, James J. Gudaitis Dec 1993

Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite Under Strain Controlled Tension-Tension And Tension-Compression Loading, James J. Gudaitis

Theses and Dissertations

This stuidy investigates the fatigue response of a cross-ply [0/90]2s Nicalon/Calcium Aluminosillicate (Nicalcc/CAS) ceramic matrix composite at room temperature under strain controlled tension-tension and tension-compression fatigue loading. The primary objectives were to determine strain fatigue limits for both loading cases and to complete a fatigue life diagram (Δe-N) for all tests. Failure mechanisms were also studied. The average initial modulus value for this lay-up was 120 GPa. The ultimate tensile strain was 0.00988 mn/mm (285 MPa). Eight tests were conducted with maximum strains that ranged from 0.00300 mm/mm to 0.00722 mm/mm. The tension-tension fatigue limit was found to be …

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Behavior Of A Centrally Notched Cross-Ply And Unidirectional Ceramic Matrix Composite In Tension-Compression Fatigue, William A. Weidenaar Dec 1992

Behavior Of A Centrally Notched Cross-Ply And Unidirectional Ceramic Matrix Composite In Tension-Compression Fatigue, William A. Weidenaar

Theses and Dissertations

Centrally notched (hole), cross-ply, ((0/90)2)s, and unidirectional, (0)8 laminates of Silicon Carbide fiber-reinforced Aluminosilicate glass, SiC/1723, were fatigue tested under tension-compression loading with a load ratio of -1. Damage accumulated continuously for both lay- ups, leading to eventual failure and a reduced fatigue life. Critical damage in the cross-ply consisted of longitudinal cracks in the 90° plies growing and combining with transverse cracks to effectively eliminate the 90° plies' load carrying capability and allowing the specimen to buckle. Critical damage in the unidirectional lay-up consisted of longitudinal cracks which initiated at the shear stress concentration …

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Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite Under Tension-Tension And Tension-Compression Loading, Frank A. Opalski Dec 1992

Fatigue Behavior Of A Cross-Ply Ceramic Matrix Composite Under Tension-Tension And Tension-Compression Loading, Frank A. Opalski

Theses and Dissertations

A study was conducted which investigated the behavior of a cross-ply [0/90]2S Nicalon/Calcium-Aluminosilicate (Nicalon/CAS) ceramic matrix composite at room temperature under tension-compression fatigue loading. Material behavior and damage was recorded by stress-strain curves, elastic modulus, hysteretic energy density, and acetate replication techniques. Tension-tension fatigue tests at a load ratio R of 0.1 (R = σmin/σmax) were completed which determined that 140 MPa was the maximum stress allowable in which cycle runout (1,000,000 cycles) would occur. Above this value, transverse crack density increased with respect to cycles and failure ultimately occurred. Tension-compression tests were then performed …

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Failure Characterization Of A Fiber Reinforced Ceramic Matrix Composite With Circular Holes, Daniel E. Bullock Dec 1991

Failure Characterization Of A Fiber Reinforced Ceramic Matrix Composite With Circular Holes, Daniel E. Bullock

Theses and Dissertations

The purpose of this study was to investigate the performance of a fiber reinforced ceramic matrix composite with circular holes. The specific objectives were to (1) determine the relationship between tensile failure stress and the ratio of hole diameter to specimen width, and (2) to examine the initiation and progression of damage. The ceramic matrix composite used was SiC/ 1723, composed of continuous silicon titanium carbide fibers in an aluminosilicate glass ceramic matrix. Uniaxial tensile tests were performed at room temperature on two different layups; unidirectional [0]8, and [0/90]2s symmetric. Each layup was tested at three diameter-to-width …

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