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GSAS

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Full-Text Articles in Civil Engineering

Separation Study Of Titanomagnetite Fe3-Xtixo4 From Natural Sand At Indramayu, West Java, Sunaryo Sunaryo, Iwan Sugihartono Nov 2010

Separation Study Of Titanomagnetite Fe3-Xtixo4 From Natural Sand At Indramayu, West Java, Sunaryo Sunaryo, Iwan Sugihartono

Makara Journal of Technology

Separation Study of Titanomagnetite Fe3-xTixO4 from Natural Sand at Indramayu, West Java. Titanomagnetite FeTiO4 has been obtained from metal sand which is separated from natural sand at Indramayu using magnetic separator with the magnetic field 0,3 Tesla. This method can improve titanomagnetite content from 32% to 63,6%. According to X-ray diffractometer (XRD) and data processing by general structure analyses system (GSAS) with χ2= 1,454 and Wrp = 0,1142 as correction factor of the peak to peak intensities, we conclude that χ2 about 0 and Wrp aproximately 10%. It indicates the datas with the error merely 0,1 can be accepted. Furthermore, …


Phase Composition Analysis Using Rietveld Methode And It's Influence To The Hardness Of Ti-Si-N Nanocomposites, Keba Moto, Lia Setiarini, Zufar Abubakar Apr 2003

Phase Composition Analysis Using Rietveld Methode And It's Influence To The Hardness Of Ti-Si-N Nanocomposites, Keba Moto, Lia Setiarini, Zufar Abubakar

Makara Journal of Technology

Phase composition analysis using rietveld methode and it’s influence to the hardness of Ti-Si-N nanocomposites. XRD data of nanocomposites Ti-Si-N have been analysed using GSAS based on Rietveld Method in order to identify phases and their composition as well as its influence on the hardness of these nanocomposites. Several new phases have been found in the sample beside the nc-TiN/a-Si3N4& a-/nc-TiSi2 that have been known widely. From the obtained crystalline phase, after the calculation of amorf Si3N4 and TiSi2 phase fraction, it is found that the optimum hardness can be reached when the fraction of a-Si3N4 phase around 8 wt.%