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Study On Synthesis Of M-Phenoxy Benzoic Acid By Electrolysis Oxidation Method, Wei Xu, Chong-Tao Zhao
Study On Synthesis Of M-Phenoxy Benzoic Acid By Electrolysis Oxidation Method, Wei Xu, Chong-Tao Zhao
Journal of Electrochemistry
The m-phenoxy benzoic acid was synthesized by oxidation m-phenoxy toluene using Cr(Ⅵ)as oxidation media, which was prepared by electrolysis oxidation of Cr(Ⅲ)in the electrochemical bath using Nafion 417 as a diaphragm, Pb-PbO_(2) as an anode and Pb as cathode. The effect factors on the electrochemical oxidation of Cr(Ⅲ)to Cr(Ⅵ)in this electrolysis were studied. Furthermore, the optimal conditions for electronic synthesis of m-phenoxy benzoic acid were also discussed.