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Articles 31 - 60 of 112
Full-Text Articles in Engineering
Static Hand Gesture Recognition Of Indonesian Sign Language System Based On Backpropagation Neural Networks, Farida Asriani, Hesti Susilawati
Static Hand Gesture Recognition Of Indonesian Sign Language System Based On Backpropagation Neural Networks, Farida Asriani, Hesti Susilawati
Makara Journal of Technology
Static Hand Gesture Recognition of Indonesian Sign Language System Based on Backpropagation Neural Networks. The main objective of this research is to perform pattern recognition of static hand gesture in Indonesian sign language. Basically, pattern recognition of static hand gesture in the form of image had three phases include: 1) segmentation of the image that will be recognizable form of the hands and face, 2) feature extraction and 3) pattern classification. In this research, we used images data of 15 classes of words static. Segmentation is performed using HSV with a threshold filter based on skin color. Feature extraction performed …
Dye Sensitized Solar Cell With Conventionally Annealed And Post-Hydrothermally Treated Nanocrystalline Semiconductor Oxide Tio2 Derived From Sol-Gel Process, Akhmad Herman Yuwono, Badrul Munir, Alfian Ferdiansyah, Arif Rahman, Wulandari Handini
Dye Sensitized Solar Cell With Conventionally Annealed And Post-Hydrothermally Treated Nanocrystalline Semiconductor Oxide Tio2 Derived From Sol-Gel Process, Akhmad Herman Yuwono, Badrul Munir, Alfian Ferdiansyah, Arif Rahman, Wulandari Handini
Makara Journal of Technology
Dye-sensitized solar cell (DSSC) is one of the very promising alternative renewable energy sources to anticipate the declination in the fossil fuel reserves in the next few decades and to make use of the abundance of intensive sunlight energy in tropical countries like Indonesia. In the present study, TiO2 nanoparticles of different nanocrystallinity was synthesized via sol−gel process with various water to inorganic precursor ratio (Rw) of 0.85, 2.00 and 3.50 upon sol preparation, followed with subsequent drying, conventional annealing and post-hydrothermal treatments. The resulting nanoparticles were integrated into the DSSC prototype and sensitized with an organic dye made of …
Immobilization Of Saccharomyces Cerevisiae In Rice Hulls For Ethanol Production, Edita Martini, Dian Andriani, Sriramulu Gobikrishnan, Kyeong Eop Kang, Surn-Teh Bark, Changshin Sunwoo, Bambang Prasetya, Don-Hee Park
Immobilization Of Saccharomyces Cerevisiae In Rice Hulls For Ethanol Production, Edita Martini, Dian Andriani, Sriramulu Gobikrishnan, Kyeong Eop Kang, Surn-Teh Bark, Changshin Sunwoo, Bambang Prasetya, Don-Hee Park
Makara Journal of Technology
The whole cell immobilization in ethanol fermentation can be done by using natural carriers or through synthetic carriers. All of these methods have the same purpose of retaining high cell concentrations within a certain defined region of space which leads to higher ethanol productivity. Lignocellulosic plant substance represents one of highly potential sources in ethanol production. Some studies have found that cellulosic substances substances can also be used as a natural carrier in cell immobilization by re-circulating pre-culture medium into a reactor. In this experiment, rice hulls without any treatment were used to immobilize Saccharomyces cerevisiae through semi solid state …
The Effect Of Enzymatic Hydrolysis On The Properties Of Protein Hydrolysate From Paddy Mushroom, Niken Widya Palupi, Wiwik Siti Windrati, Tamtarini Tamtarini
The Effect Of Enzymatic Hydrolysis On The Properties Of Protein Hydrolysate From Paddy Mushroom, Niken Widya Palupi, Wiwik Siti Windrati, Tamtarini Tamtarini
Makara Journal of Technology
Protein hydrolysate was prepared from Paddy (Volvariella volvaceae) mushroom. Hydrolysis uses commercially protease available Protamex ™ with enzyme concentration of 0.1% (w/w). Hydrolysis was performed at three different temperatures (room temperature, 40 °C, and 50 °C) with different incubation periods (60, 90, and 120 minutes). Enzyme inactivation was done in 90 °C for 3 minutes. Yield and degree of hydrolysis ranged from 94.76% to 99.55% and 19.06% to 24.59%. Protein solubility was about 89–11,8%. The longer time of hydrolysis, the darker the color of protein hydrolysate. Protein hydrolysate which has hydrolysis at 50 °C for 120 minutes has the highest …
Wimax Implementation As Existing Hotspot Network Backhaul In Jakarta, Djamhari Sirat, Muhamad Asvial, Luther B. Marpaung
Wimax Implementation As Existing Hotspot Network Backhaul In Jakarta, Djamhari Sirat, Muhamad Asvial, Luther B. Marpaung
Makara Journal of Technology
WiMAX Implementation as Existing Hotspot Network Backhaul in Jakarta The development of Broadband Wireless Access (BWA), such as WiMAX, as a global standard for data transmission media has been used by high speed internet access provider. WiMAX application which supported by capabilities of interoperability, flexibility and commercial aspect make the internet services become more efficient, cheaper and easier to the customer. This phenomenon should be responded by ISPs. Based on technical and financial aspect in deciding the implementation of Wireless Network with WiMAX technology as a substitute, this research will observe and analyze the projection of WiMAX technology implementation as …
Plant Growth Modeling Using L-System Approach And Its Visualization, Atris Suyantohadi, Alfiyan Alfiyan, Mochamad Hariadi, Mauridhi Hery Purnomo
Plant Growth Modeling Using L-System Approach And Its Visualization, Atris Suyantohadi, Alfiyan Alfiyan, Mochamad Hariadi, Mauridhi Hery Purnomo
Makara Journal of Technology
The visualization of plant growth modeling using computer simulation has rarely been conducted with Lindenmayer System (L-System) approach. L-System generally has been used as framework for improving and designing realistic modeling on plant growth. It is one kind of tools for representing plant growth based on grammar sintax and mathematic formulation. This research aimed to design modeling and visualizing plant growth structure generated using L-System. The environment on modeling design used three dimension graphic on standart OpenGL format. The visualization on system design has been developed by some of L-System grammar, and the output graphic on three dimension reflected on …
Remote Sensing And Geographical Information System To Identify Drought Potency, Puguh Dwi Raharjo
Remote Sensing And Geographical Information System To Identify Drought Potency, Puguh Dwi Raharjo
Makara Journal of Technology
Remote Sensing and Geographical Information System to Identify Drought Potency. Kebumen regency was drought in year 2008, community clean water shortages and irrigation water following a decline in water resources. The use of remote sensing data and GIS can be used to identify the potential for drought-prone areas. Transformation of Landsat TM satellite imagery to obtain the brightness index, wetness index and vegetation index used to determine surface conditions in relation to drought. Brightness index and wetness index derived from the tasseled cap modifications, while the vegetation index derived from normalized difference vegetation index (NDVI) values. Other parameters such as …
Hydrogen Absorption Induced Slow Crack Growth In Austenitic Stainless Steels For Petrochemical Pressure Vessel Industries, Ronnie Higuchi Rusli
Hydrogen Absorption Induced Slow Crack Growth In Austenitic Stainless Steels For Petrochemical Pressure Vessel Industries, Ronnie Higuchi Rusli
Makara Journal of Technology
Type 304L and type 309 austenitic stainless steels were tested either by exposed to gaseous hydrogen or undergoing polarized cathodic charging. Slow crack growth by straining was observed in type 304L, and the formation of α‘ martensite was indicated to be precursor for such cracking. Gross plastic deformation was observed at the tip of the notch, and a single crack grew slowly from this region in a direction approximately perpendicular to the tensile axis. Martensite formation is not a necessary condition for hydrogen embrittlement in the austenitic phase.
Simulation On The Use Of Losat Data For Rice Field Mapping, Bambang H. Trisasongko, Dyah R. Panuju, Boedi Tjahjono, Baba Barus, Hari Wijayanto, Mahmud A. Raimadoya, Irzaman Irzaman
Simulation On The Use Of Losat Data For Rice Field Mapping, Bambang H. Trisasongko, Dyah R. Panuju, Boedi Tjahjono, Baba Barus, Hari Wijayanto, Mahmud A. Raimadoya, Irzaman Irzaman
Makara Journal of Technology
Simulation on the Use of LOSAT Data for Rice Field Mapping. Since the launch of LAPAN-TUBSAT satellite in 2007, Indonesia has been developing mission on earth observation missions for various applications. The next generation mission, called LAPAN-ORARI Satellite (LOSAT), is currently under development and expected to be launched in 2011. In order to facilitate the applications, a thorough assessment of the sensor should be made. This paper presents an examination of simulated LOSAT data for rice monitoring and mapping purposes coupled with QUEST statistical tree. We found that three-band simulated LOSAT data were suitable for the task with reasonably high …
High Pressure Adsorption Isotherm Of Co2 On Activated Carbon Using Volumetric Method, Awaludin Martin, Bambang Suryawan, Muhammad Idrus Alhamid, Nasruddin Nasruddin
High Pressure Adsorption Isotherm Of Co2 On Activated Carbon Using Volumetric Method, Awaludin Martin, Bambang Suryawan, Muhammad Idrus Alhamid, Nasruddin Nasruddin
Makara Journal of Technology
High Pressure Adsorption Isotherm of CO2 on Activated Carbon using Volumetric Method. Adsorption system is ones of the most effective methods for CO2 separating with other substances that produced from the burning of fossil fuels. In the design for that application, beside of characteristics of porous material (adsorbent) data, CO2 adsorption data on the adsorbent (kinetic and thermodynamic) are also needed. The aim of this research is resulting isothermal adsorption data at pressures up to 3.5 MPa by indirect methods (volumetric method) at isothermal temperature of 300, 308, 318 and 338 K. Adsorbent that used in this research is activated …
Shaft Torsional Vibration Response Of Vertical Axis Ocean Current Turbine Model Due To Torque Excitation, Adi Wirawan Husodo, I Ketut Aria Pria Utama, I Made Ariana
Shaft Torsional Vibration Response Of Vertical Axis Ocean Current Turbine Model Due To Torque Excitation, Adi Wirawan Husodo, I Ketut Aria Pria Utama, I Made Ariana
Makara Journal of Technology
Shaft Torsional Vibration Response of Vertical Axis Ocean Current Turbine Model Due to Torque Excitation. The current research aimed to study the torsional vibration response of Vertical Axis Ocean Current Turbine due to randomly torque excitation pattern, owing to the variety of ocean current velocity. The turbine model is composed of 3 aluminum blades of NACA 0018 connected to steel shaft. Turbine dimensions are 10 cm of chord, 1.8 cm of chamber and 100 cm of span. The variation of ocean current velocity is 0.5 m/s, 1.0 m/s, 1.5 m/s, 2.0 m/s, 2.5 m/s and 3.0 m/s. The Model has …
Concept Design And Testing Of Multi-Nozzle Water Mist Fire Suppression System, Danardono A. Sumarsono, Yulianto S. Nugroho, Mariance Mariance, I Gede Wahyu W. Ariasa
Concept Design And Testing Of Multi-Nozzle Water Mist Fire Suppression System, Danardono A. Sumarsono, Yulianto S. Nugroho, Mariance Mariance, I Gede Wahyu W. Ariasa
Makara Journal of Technology
In this work a flexible design of multi-nozzle arrangement of water mist fire suppression system was studied. The source of fire was a 65 mm diameter cooking oil fire. An investigation on the impact of nozzle arrangement on the temperature profile of fires was conducted. The occurance of oil splash due to the application of water mist was also studied. The water mist systems developed in the present work can effectively extinguish cooking oil fires and prevented them from re-ignition. The spray angle, discharge pressure, and water flow rate were important factors to determine the effectiveness of water mist in …
An Empirical Model For Build-Up Of Sodium And Calcium Ions In Small Scale Reverse Osmosis, Subriyer Nasir
An Empirical Model For Build-Up Of Sodium And Calcium Ions In Small Scale Reverse Osmosis, Subriyer Nasir
Makara Journal of Technology
A simple models for predicting build-up of solute on membrane surface were formulated in this paper. The experiments were conducted with secondary effluent, groundwater and simulated feed water in small-scale of RO with capacity of 2000 L/d. Feed water used in the experiments contained varying concentrations of sodium, calcium, combined sodium and calcium. In order to study the effect of sodium and calcium ions on membrane performance, experiments with ground water and secondary effluent wastewater were also performed. Build-up of salts on the membrane surface was calculated by measuring concentrations of sodium and calcium ions in feed water permeate and …
Effect Of Diafiltration On Preparation Of Fermented Mung Beans Concentrate As Probiotic Savory Flavor Through Ultrafiltration Membrane, Aspiyanto Aspiyanto, Agustine Susilowati
Effect Of Diafiltration On Preparation Of Fermented Mung Beans Concentrate As Probiotic Savory Flavor Through Ultrafiltration Membrane, Aspiyanto Aspiyanto, Agustine Susilowati
Makara Journal of Technology
Diafiltration by means of the ultrafiltration system of probiotic fermented Mung beans (Phaseolus radiatus L.) concentrate has been performed to reduce or eliminate salts and smaller impurities than the nominal cut-off of the membrane of 20,000 nominal weight cut-off (NWCO). These processes have been conducted as an attempt in order to get a probiotic product with organoleptic acceptability, composition, and the optimal total lactic acid bacteria (LAB) counts because the presence of salts will affect on the viability of LAB and the cell lysis of LAB and limit its utility in food products. Concentrate of probiotic mung beans was prepared …
Electrooxidation Of Carbon Monoxide On Pd Thin Film-Coated Au Electrodes:Film Thickness Dependence, Yuqing Yang, Shouzhong Zou
Electrooxidation Of Carbon Monoxide On Pd Thin Film-Coated Au Electrodes:Film Thickness Dependence, Yuqing Yang, Shouzhong Zou
Journal of Electrochemistry
The adsorption and electrooxidation of CO on Pd-coated Au electrodes were studied by cyclic voltammetry and surface-enhanced Raman spectroscopy (SERS) . It is found that CO oxidation activity is film thickness dependent. Cyclic voltammograms (CVs) showed that CO oxidation peak potential shifted positively with the increase of the Pd thickness. SERS showed a redshift of the C—O stretching frequency with increasing Pd film thickness. These observations were explained by the dband theory. The strain effect strengthens CO adsorption and stabilizes adsorbed CO,while the ligand effect weakens CO adsorption and eases its oxidation. The ligand effect overpowers the strain effect.
In-Situ Surface Enhanced Raman Scattering Electrochemical Investigation Of 4-Aminoantipyrine On Silver Electrode, Li-Jun Zhang, Wei Song, Ling Chen, Zong-Rang Zhang, Hai-Feng Yang
In-Situ Surface Enhanced Raman Scattering Electrochemical Investigation Of 4-Aminoantipyrine On Silver Electrode, Li-Jun Zhang, Wei Song, Ling Chen, Zong-Rang Zhang, Hai-Feng Yang
Journal of Electrochemistry
In this paper,4-AAP was self-assembled on silver surface to form monolayers. Surface-enhanced Raman Spectroscopy ( SERS) was used to in-situ investigate the adsorption mechanism of the 4-aminoantipyrine( 4-AAP) on silver surface dependent on shifting potentials and the effect of solution pH. Based on density functional theory( DFT) calculation of vibration modes,approximate assignment of 4-AAP SERS spectrum was conducted. In situ SERS spectral electrochemical experiments indicated that the 4-AAP monolayers experience a dynamic adsorption process from a tilted fashion to a more vertical mode for benzene ring and more parallel for pyrine ring with the potential applied toward more negative voltages. …
Multi-Electron Redox Materials For High Energy Density Electrodes, Xin-Ping Ai, Han-Xi Yang
Multi-Electron Redox Materials For High Energy Density Electrodes, Xin-Ping Ai, Han-Xi Yang
Journal of Electrochemistry
Various new energy technologies being developed require electrochemical energy batteries to have a real breakthrough in energy density and rate capability,which imposes a great challenge for electrochemists and materials chemists. Multi-electron redox reactions seem to open a promising avenue to create new batteries with dramatically enhanced energy densities. This paper describes simply our research works on the multi-electron redox systems,including metal boride anode,lithium alloying compounds and electrochemical conversion materials, and also discusses the problems hindering these systems for battery applications.
Preliminary Investigation Of Iron Protoporphyrin Sams On Platinum Electrodes By Surface Enhanced Vibrational Spectroscopies, Min Ma, Yao-Yue Yang, Han-Xuan Zhang, Wen-Bin Cai
Preliminary Investigation Of Iron Protoporphyrin Sams On Platinum Electrodes By Surface Enhanced Vibrational Spectroscopies, Min Ma, Yao-Yue Yang, Han-Xuan Zhang, Wen-Bin Cai
Journal of Electrochemistry
In situ SERS and ATR-SEIRAS were applied to investigate the electrochemical and structural properties of iron protoporphyrin IX (FePP) self-assembled monolayers (SAMs) on Pt electrodes in 0. 1 mol· L -1 HClO4. The potential dependent SERS spectra of the FePP SAM on a roughened Pt electrode with the enhancement factor of ca. 40 were acquired with the excitation line of 514 nm. Analyses of SERS data over the potential region from 0. 5 to -0. 3 V enabled to obtain potential dependent adsorption isotherms,from which the formal redox potential could be estimated to be ca. - 0. 2 V. Up-tilted …
Studies Of Oxidation Processes Of Adsorbed And Solution Co On Pt(110) Electrode By Cyclic Voltammetry And In Situ Ftirs, Li Tian, Jun-Tao Li, Jin-Yu Ye, Chun-Hua Zhen, Shi-Gang Sun
Studies Of Oxidation Processes Of Adsorbed And Solution Co On Pt(110) Electrode By Cyclic Voltammetry And In Situ Ftirs, Li Tian, Jun-Tao Li, Jin-Yu Ye, Chun-Hua Zhen, Shi-Gang Sun
Journal of Electrochemistry
The oxidation processes of adsorbed CO (COad) and solution phase CO (COsol) on Pt(110) electrode were investigated by cyclic voltammetry and in-situ FTIR spectroscopy. It has revealed that in comparison with COad on Pt(110) in a CO-free solution,the oxidation current peak of COsol in a CO-saturated solution is positively shifted ca. 168 mV,and the peak current density has been increased by 6. 70 times. Linear adsorbed CO (COL) is determined by in-situ FTIR spectroscopy as the main species,which is uniformly distributed on Pt (110) surface. In a CO-free solution,the onset potential of COL is measured by in-situ FTIRS ca. 0. …
The Mechanism Of ~(13)Co_(Ad)/~(12)Co Isotope Exchange At Pt Electrode,A Combined Study By Electrochemical In-Situ Infrared Spectroscopy And Dipole-Dipole Coupling Analysis, Sang-Zi Liang, Shao-Xiong Liu, Ling-Wen Liao, Qian Tao, Jing Kang, Yan-Xia Chen
The Mechanism Of ~(13)Co_(Ad)/~(12)Co Isotope Exchange At Pt Electrode,A Combined Study By Electrochemical In-Situ Infrared Spectroscopy And Dipole-Dipole Coupling Analysis, Sang-Zi Liang, Shao-Xiong Liu, Ling-Wen Liao, Qian Tao, Jing Kang, Yan-Xia Chen
Journal of Electrochemistry
In this contribution,we have analyzed the IR spectra of saturated CO adlayer at rough Pt film electrode as a function of fractional surface coverage of 13COad/12COad recorded during 13COad /12CO isotope exchange process according to dipole-dipole coupling theory and coherent potential approximation. By properly choosing the parameters of adlayer structure and dipole-dipole coupling interaction under coherent potential approximation, we demonstrated that we can successfully simulate the IR spectra as a function of the surface coverage of CO adlayer at rough Pt film electrodes by assuming that COad molecules with low C—O stretching frequencies are dis- placed preferentially during the 13COad/12CO …
An In Situ Fourier Transform Infrared Spectroelectrochemical Study On Alcohols Electrocatalytic Oxidation At Pd Electrode In Acidic Solution, Hai-Ping Huang, Lian-Qin Wang, Pei-Kang Shen
An In Situ Fourier Transform Infrared Spectroelectrochemical Study On Alcohols Electrocatalytic Oxidation At Pd Electrode In Acidic Solution, Hai-Ping Huang, Lian-Qin Wang, Pei-Kang Shen
Journal of Electrochemistry
The methanol and ethylene glycol electrooxidation on palladium electrode in acidic solution has been investigated by cyclic voltammetry and in situ Fourier transform infrared spectroelectrochemistry. It shows that the oxidation of methanol and ethylene glycol at Pd electrode cannot proceed until over 1. 5 V in acidic and neutral media. The overpotential decreases and the peak current density increases with the reduction in pH values. The formation of the oxygen-containing species significantly affects the alcohol oxidation on Pd electrode. The in situ FTIR spectroscopic measurements show that the oxidation products of ethylene glycol on Pd electrode are CO2 and oxalic …
Solid State Nmr Studies Of Lithium Manganese Silicate As Positive Electrode Materials For Li-Ion Batteries, Hu Cheng, Zi-Geng Liu, Yi-Xiao Li, Zhong Chen, Yong Yang
Solid State Nmr Studies Of Lithium Manganese Silicate As Positive Electrode Materials For Li-Ion Batteries, Hu Cheng, Zi-Geng Liu, Yi-Xiao Li, Zhong Chen, Yong Yang
Journal of Electrochemistry
The Li2MnSiO4 cathode material for lithium ion batteries was synthesized by sol-gel assisted hydrothermal method. XRD,FTIR and SS-NMR were used to study the phase,structure and morphology of obtained samples. Electrochemical performance of cathode material was tested. The results show that the main phase of sample prepared was Li2MnSiO4,whereas a small amount of impurities ( Li2CO3) were existed. The Li2MnSiO4 cathode material gave an initial discharging capacity of about 190 mAh·g -1. But this capacity faded rapidly during the cycling process due to the decomposition of Li2MnSiO4.
In Situ Surface-Enhanced Raman Scattering Spectroscopic Study Of Sulfur Adsorption On Polycrystalline Platinum Electrode Surface, Bolian Xu-, In-Su Park, Ying Li, De-Jun Chen, Yuye J. Tong
In Situ Surface-Enhanced Raman Scattering Spectroscopic Study Of Sulfur Adsorption On Polycrystalline Platinum Electrode Surface, Bolian Xu-, In-Su Park, Ying Li, De-Jun Chen, Yuye J. Tong
Journal of Electrochemistry
The paper reports the first in situ surface enhanced Raman scattering (SERS) spectroelectrochemistry study of sulfur adsorption and electro-oxidation on highly roughened polycrystalline Pt surface in both acidic and basic supporting electrolytes. The SERS spectra were taken at a constant electrode potential after accumulative electro-oxidation CVs of the Pt electrode with pre-adsorbed sulfur species and at different electrode potentials that were varied stepwise of the Pt electrode immersed in sulfur-containing electrolytes without pre-adsorbed sulfur species. In both cases,a dominant vibrational band at 299 cm -1 in acidic electrolyte but at 310 cm-1 in basic electrolyte was observed,which was assigned to …
Comparative Study Of Nanoporous Pt,Ptru And Ptruir Catalysts Using Electrochemical Ftir Spectroscopy, M. Amussen Robert, Holt-Hindle Peter, Nigro Samantha, Chen Aicheng
Comparative Study Of Nanoporous Pt,Ptru And Ptruir Catalysts Using Electrochemical Ftir Spectroscopy, M. Amussen Robert, Holt-Hindle Peter, Nigro Samantha, Chen Aicheng
Journal of Electrochemistry
In recent years much effort has been put towards developing efficient Pt-based electrocatalysts for applications in fuel cells. With the rising cost of precious metals such as Pt,the need to enhance the activity and to decrease the load of catalysts is prominent. Herein we report on the synthesis and comparative study of nanoporous Pt,PtRu and PtRuIr electrocatalysts. The nanoporous electrodes were fabricated using a hydrothermal method and characterized by scanning electron microscopy (SEM) ,energy dispersive spectroscopy (EDS) ,X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS) . The electrocatalytic activity of the fabricated nanopo- rous materials was evaluated using both CO …
52nd Rocky Mountain Conference On Analytical Chemistry
52nd Rocky Mountain Conference On Analytical Chemistry
Rocky Mountain Conference on Magnetic Resonance
Final program, abstracts, and information about the 52nd annual meeting of the Rocky Mountain Conference on Analytical Chemistry, co-endorsed by the Colorado Section of the American Chemical Society and the Society for Applied Spectroscopy. Held in Snowmass, Colorado, August 1-5, 2010.
An Investigation Of Microstructural Change Of Low Alloy Steel Aisi 4150 By Seebeck Coefficient, T Samran, P Termsuksawad
An Investigation Of Microstructural Change Of Low Alloy Steel Aisi 4150 By Seebeck Coefficient, T Samran, P Termsuksawad
Journal of Metals, Materials and Minerals
Low alloyed steels, whose hardness can be modified by heat treatment, have been widely used in various applications. After heat treatment, they are normally destructively characterized and tested by many approaches via optical microscope and hardness testing. It is useful to develop a non-destructive method relating to its properties and microstructures. The proposed non-destructive approach in this study is the Seebeck coefficient measurement. The materials in this study were carbon steels AISI 4150 rod with a diameter of 1.3 cm and length of 3 cm. The specimens were heat-treated at 900ºC for 1 hour and were then cooled to room …
Preparation Of Hydrophobic Chitosan Using Complexation Method For Pla/Chitosan Blend, P Chouwatat, P Polsana, P Noknoi, K Siralertmukul, K Srikulkit
Preparation Of Hydrophobic Chitosan Using Complexation Method For Pla/Chitosan Blend, P Chouwatat, P Polsana, P Noknoi, K Siralertmukul, K Srikulkit
Journal of Metals, Materials and Minerals
In this study, dioctyl sulfosuccinate-chitosan complex was prepared by a mechanical mixing of aqueous chitosan with sodium dioctyl sulfosuccinate. As a result, hydrophobic chitosan was achieved. Characterizations of the complex were carried out including XRD, TGA, and FT-IR in order to follow changes in the chitosan structure. Thus produced chitosan complex was hydrophobic and anticipated to be compatible with PLA. Solution blending of PLA and hydrophobic chitosan was then conducted. Characterization techniques including XRD and FT-IR were employed to investigate the structure of the polymer blend. FTIR spectra showed that changes in the fingerprint of the chitosan amide band in …
Thermal Analysis Of Fe-Carbide And Fe-C Mixtures, R Tongsri, B Vetayanugul
Thermal Analysis Of Fe-Carbide And Fe-C Mixtures, R Tongsri, B Vetayanugul
Journal of Metals, Materials and Minerals
Differential thermal analysis (DTA) was employed to monitor changes which occurred during heating of Fe-carbide and Fe-C mixtures. The DTA curves showed a relationship between endothermic peaks and phase transformations given in the Fe-C phase diagram. The transformations included (i) magnetic Fe to non-magnetic Fe, (ii) pure α-Fe to pure γ-Fe, (iii) γ + Fe3C → Liquid and (iv) pure γ-Fe to pure δ-Fe. Melting of the Fe-SiC powder compacts when sintered at temperatures higher than 1200°C was revealed and indicated by the endothermic peak of 1230°C. This peak corresponded to the transformation of γ + Fe3C → Liquid. That …
Effects Of Replacing Binder With Powder Space Holder On Properties Of Metal Injection Moulded Foam, U Koikul, A Manonukul, S Suranuntchai
Effects Of Replacing Binder With Powder Space Holder On Properties Of Metal Injection Moulded Foam, U Koikul, A Manonukul, S Suranuntchai
Journal of Metals, Materials and Minerals
Metal foam can be produced using metal injection moulding with powder space holder. In this study, the effects of volume fraction of spacer holder on the foam properties were studied. Spherical poly (methyl methacrylate) (PMMA) particles were used as a space holder material. The 30% volume fraction of stainless steel 316L powder was mixed with varied volume fractions of binder and PMMA. There were five volume fractions of PMMA, namely 30% to 50%, with an increment of 5%. The results showed that the volume fraction of PMMA affected the properties. As the volume fraction of PMMA increased, the number of …
Study Of Covering Conditions For Sintering Of Metal Injection Moulded Commercially Pure Titanium, N Muenya, A Manonukul
Study Of Covering Conditions For Sintering Of Metal Injection Moulded Commercially Pure Titanium, N Muenya, A Manonukul
Journal of Metals, Materials and Minerals
In metal injection moulding process, sintering for some specific materials is different from general materials. Titanium is a material that is not easy to sinter because it is a very reactive metal at high temperature. The high quality of the titanium component is difficult to control, especially so in point of the levels of carbon and oxygen, which have large effects on the mechanical properties. Commercially pure titanium was injected, debinded and sintered at 1150°C and 1250°C in high vacuum without a cover, and with a quartz cover, a mullite cover and an alumina cover, respectively. From the physical and …