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Microstructure And Interface Characteristics Of B4c, Sic And Al2o3 Reinforced Al Matrix Composites: A Comparative Study, Haseeb Asma Dec 2003

Microstructure And Interface Characteristics Of B4c, Sic And Al2o3 Reinforced Al Matrix Composites: A Comparative Study, Haseeb Asma

Haseeb ASMA

Three aluminium metal matrix composites containing reinforcing particles of B4C, SiC and Al2O3 (0-20 vol.%) were processed. The stir-casting manufacturing route followed by hot extrusion was utilized, being one of the cost-effective industrial methods. A clear interfacial reaction product/layer was found at Al-SiC interface for composites held for a relatively long processing time (>30 min). No reaction product was observed at Al-B4C and Al-Al2O3 interfaces at the resolution limit of the SEM used. On the other hand, two secondary phases (alumina and another phase containing aluminium, boron and carbon) were found in the aluminum matrix away from the interface …


Study On The Nature Of The Electrochemically Synthesized Hard Fe-15.4 Mass % Ni-0.70 Mass % C Alloy Film, Haseeb Asma Apr 2003

Study On The Nature Of The Electrochemically Synthesized Hard Fe-15.4 Mass % Ni-0.70 Mass % C Alloy Film, Haseeb Asma

Haseeb ASMA

Electrochemical synthesis of hard Fe-15.4 mass% Ni-0.70 mass% C alloy film with a hardness 750 HV was carried out from sulfate-based bath containing a small amount of citric acid and L-ascorbic acid. The nature of the alloy was investigated by different characterization techniques including x-ray diffraction, x-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, Mossbauer spectroscopy, differential scanning calorimetry, and magnetic measurements. The decomposition behavior of the alloy was also studied and compared with that of thermally prepared martensite. It was found that the electrochemically deposited Fe-Ni-C alloy exists in a state that is ahead of the freshly quenched …