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Articles 1 - 30 of 54
Full-Text Articles in Manufacturing
Anisotropy In Impact Toughness Of Powder Bed Fused Aisi 304l Stainless Steel, Sreekar Karnati, Atoosa Khiabhani, Aaron Flood, Frank W. Liou, Joseph William Newkirk
Anisotropy In Impact Toughness Of Powder Bed Fused Aisi 304l Stainless Steel, Sreekar Karnati, Atoosa Khiabhani, Aaron Flood, Frank W. Liou, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
The current effort involved investigation into the anisotropy of AISI 304L fabricated through laser powder bed fusion. Charpy V‐notch specimens made from material fabricated at three different build orientations were tested and analyzed. A statistically significant difference among the toughness values indicates the presence of anisotropy within the additively manufactured material. While the lowest toughness was found in vertically built specimens, the horizontal specimens were found to exhibit the highest toughness. From the fracture surfaces, an atypical mode of failure was observed. Exclusive crack propagation along the interlayer track boundaries was observed. The toughness variation correlated with the ease of …
Method And Apparatus For Fabricating Ceramic And Metal Components Via Additive Manufacturing With Uniform Layered Radiation Drying, Ming-Chuan Leu, Amir Ghazanfari, Wenbin Li, Greg Hilmas, Robert G. Landers
Method And Apparatus For Fabricating Ceramic And Metal Components Via Additive Manufacturing With Uniform Layered Radiation Drying, Ming-Chuan Leu, Amir Ghazanfari, Wenbin Li, Greg Hilmas, Robert G. Landers
Mechanical and Aerospace Engineering Faculty Research & Creative Works
A freeform extrusion fabrication process for producing three - dimensional ceramic, metal and functionally gradient composite objects, including the steps of filling a plurality of paste sources with a respective plurality of aqueous paste compositions, operationally connecting respective syringes containing respective aqueous paste compositions to a mix ing chamber, moving a first aqueous paste composition from a first respective paste source into the mixing chamber, moving a second aqueous paste composition from a second respective paste source into the mixing chamber, mixing the first and second aqueous paste compositions to define a first admixture having a first admixture composition, extruding …
Recyclability Of 304l Stainless Steel In The Selective Laser Melting Process, Austin T. Sutton, Caitlin S. Kriewall, Ming-Chuan Leu, Joseph William Newkirk
Recyclability Of 304l Stainless Steel In The Selective Laser Melting Process, Austin T. Sutton, Caitlin S. Kriewall, Ming-Chuan Leu, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
During part fabrication by selective laser melting (SLM), a powder-bed fusion process in Additive Manufacturing (AM), a large amount of energy is input from the laser into the melt pool, causing generation of spatter and condensate, both of which have the potential to settle in the surrounding powder-bed compromising its reusability. In this study, 304L stainless steel powder is subjected to five reuses in the SLM process to assess its recyclability through characterization of both powder and mechanical properties. Powder was characterized morphologically by particle size distribution measurements, oxygen content with inert gas fusion analysis, and phase identification by X-ray …
Characterization Of Impact Toughness Of 304l Stainless Steel Fabricated Through Laser Powder Bed Fusion Process, Sreekar Karnati, Atoosa Khiabhani, Aaron Flood, Frank W. Liou, Joseph William Newkirk
Characterization Of Impact Toughness Of 304l Stainless Steel Fabricated Through Laser Powder Bed Fusion Process, Sreekar Karnati, Atoosa Khiabhani, Aaron Flood, Frank W. Liou, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
In this research, the impact toughness of powder bed based additively manufactured 304L stainless steel was investigated. Charpy specimens were built in vertical, horizontal and inclined (45⁰) orientations to investigate the variation in toughness with build direction. These specimens were tested in as-built and machined conditions. A significant difference in toughness was observed with varying build directions. The lowest toughness values were recorded when the notch was oriented in line with the interlayer boundary. The highest toughness was recorded when the notch was perpendicular to the interlayer boundary. A significant scatter in toughness values was also observed. The variation and …
Design Of Lattice Structures With Graded Density Fabricated By Additive Manufacturing, Wenjin Tao, Yong Liu, Austin T. Sutton, Krishna C. R. Kolan, Ming-Chuan Leu
Design Of Lattice Structures With Graded Density Fabricated By Additive Manufacturing, Wenjin Tao, Yong Liu, Austin T. Sutton, Krishna C. R. Kolan, Ming-Chuan Leu
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Lattice structures fabricated by Additive Manufacturing (AM) processes are promising for many applications, such as lightweight structures and energy absorbers. However, predicting and controlling of their mechanical behaviors is challenging due to the complexity of modeling and the uncertainties exist in the manufacturing process. In this paper, we explore the possibilities enabled by controlling the local densities. A set of lattice structures with different density gradients are designed using an implicit isosurface equation, and they are manufactured by Selective Laser Melting (SLM) process with 304L stainless steel. Finite element analysis and compression test are used to evaluate their mechanical properties. …
Building Zr-Based Metallic Glass Part On Ti-6al-4v Substrate By Laser-Foil-Printing Additive Manufacturing, Yingqi Li, Yiyu Shen, Ming-Chuan Leu, Hai-Lung Tsai
Building Zr-Based Metallic Glass Part On Ti-6al-4v Substrate By Laser-Foil-Printing Additive Manufacturing, Yingqi Li, Yiyu Shen, Ming-Chuan Leu, Hai-Lung Tsai
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Through using Zr intermediate layers, Zr52.5Ti5Al10Ni14.6Cu17.9 metallic glass (MG) parts are successfully built on Ti-6Al-4V substrates by laser-foil-printing (LFP) additive manufacturing technology in which MG foils are laser welded layer-by-layer onto the substrate. The printed MG part is free of porosity, cracking and crystallization; additionally, its glass transition temperature, crystallization temperature, micro-hardness, and tensile strength are very similar to the original MG material. The Zr intermediate layers are aimed at preventing direct interaction between the first layer of MG foil and the Ti substrate; otherwise, the welded MG foils would peel …
Fabricating Zirconia Parts With Organic Support Material By The Ceramic On-Demand Extrusion Process, Wenbin Li, Amir Ghazanfari, Devin Mcmillen, Andrew Scherff, Ming-Chuan Leu, Greg Hilmas
Fabricating Zirconia Parts With Organic Support Material By The Ceramic On-Demand Extrusion Process, Wenbin Li, Amir Ghazanfari, Devin Mcmillen, Andrew Scherff, Ming-Chuan Leu, Greg Hilmas
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Ceramic On-Demand Extrusion (CODE) is an extrusion-based additive manufacturing process recently developed for fabricating dense, functional ceramic components. This paper presents a further development of this process and focuses on fabricating 3 mol% yttria-stabilized zirconia (3YSZ) components that cannot be fabricated without using support structures. The 3YSZ paste is deposited through the main nozzle, and a polycaprolactone (PCL) pellet feedstock is melted and deposited through an auxiliary nozzle to build support structures. After a green part is printed and dried, the support structures are removed by heating the part to ~70 ⁰C to melt the PCL. The part is then …
Characterization Of Heat-Affected Powder Generated During Selective Laser Melting Of 304l Stainless Steel Powder, Austin T. Sutton, Caitlin S. Kriewall, Ming-Chuan Leu, Joseph William Newkirk
Characterization Of Heat-Affected Powder Generated During Selective Laser Melting Of 304l Stainless Steel Powder, Austin T. Sutton, Caitlin S. Kriewall, Ming-Chuan Leu, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
The selective laser melting (SLM) process is an Additive Manufacturing (AM) technique that uses a laser to fuse successive layers of powder into near fully dense components. Due to the large energy input from the laser during processing, vaporization and instabilities in the melt pool occur causing the formation of condensate and laser spatter, collectively known as heat-affected powder. Since heat-affected powder settles into the powder bed, the properties of the unconsolidated powder may be altered compromising its reusability. In this study, characterization of 304L heat-affected powder was performed through particle size distribution measurements, x-ray diffraction, metallography, energy-dispersive spectroscopy mapping, …
Influence Of Gage Length On Miniature Tensile Characterization Of Powder Bed Fabricated 304l Stainless Steel, Sreekar Karnati, Jack L. Hoerchler, Frank W. Liou, Joseph William Newkirk
Influence Of Gage Length On Miniature Tensile Characterization Of Powder Bed Fabricated 304l Stainless Steel, Sreekar Karnati, Jack L. Hoerchler, Frank W. Liou, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Miniature tensile specimens with varying aspect ratios were fabricated from 304L stainless steel (SS) made using powder bed additive manufacturing (AM) process. The tensile characteristics measured from these specimens were analyzed to assess the impact of gage length. The study found no impact upon varying gage length on yield and ultimate strength measurements. However, a significant impact was observed on strain measurements. This data was also used to perform Weibull statistics to estimate the stochastic performance of the material. Fractography was performed to visually identify the types of flaws. A comparative study with specimens fabricated from cold rolled annealed 304 …
Bonding Of 304l Stainless Steel To Cast Iron By Selective Laser Melting, Baily Thomas, Austin T. Sutton, Ming-Chuan Leu, Nikhil Doiphode
Bonding Of 304l Stainless Steel To Cast Iron By Selective Laser Melting, Baily Thomas, Austin T. Sutton, Ming-Chuan Leu, Nikhil Doiphode
Mechanical and Aerospace Engineering Faculty Research & Creative Works
While cast iron is widely used in industry, a major limitation is the weldability of a dissimilar material onto cast iron due to hot cracking as a result of lack of ductility from graphite flakes. Consequently, a significant amount of preheat is often employed to reduce the cooling rate in the fusion zone, which, however, may lead to distortion of the welded parts. A potential remedy could be the Selective Laser Melting (SLM) process, where only small melt pools are created and thus the overall energy input is reduced. The present paper describes an investigation of the SLM process to …
Fabricating Zirconia Components With Organic Support Material By The Ceramic On-Demand Extrusion Process, Wenbin Li, Amir Ghazanfari, Devin Mcmillen, Andrew Scherff, Ming-Chuan Leu, Greg Hilmas
Fabricating Zirconia Components With Organic Support Material By The Ceramic On-Demand Extrusion Process, Wenbin Li, Amir Ghazanfari, Devin Mcmillen, Andrew Scherff, Ming-Chuan Leu, Greg Hilmas
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Ceramic On-Demand Extrusion (CODE) is an extrusion-based additive manufacturing process recently developed for fabricating dense, functional ceramic components. This paper presents a further development of this process and focuses on fabricating 3 mol% yttria-stabilized zirconia (3YSZ) components that cannot be fabricated without using support structures. The 3YSZ paste is deposited through the main nozzle, and a polycaprolactone (PCL) pellet feedstock is melted and deposited through an auxiliary nozzle to build support structures. After a green part is printed and dried, the support structures are removed by heating the part to ~70°C to melt the PCL. The part is then sintered …
Mechanical Properties Of 304l Parts Made By Laser-Foil-Printing Technology, Chia-Hung Hung, Yiyu Shen, Ming-Chuan Leu, Hai-Lung Tsai
Mechanical Properties Of 304l Parts Made By Laser-Foil-Printing Technology, Chia-Hung Hung, Yiyu Shen, Ming-Chuan Leu, Hai-Lung Tsai
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Laser-Foil-Printing (LFP) is a novel laminated object manufacturing process for metal additive manufacturing. It fabricates three-dimensional metal parts by using a dual-laser system to weld and cut metal foils layer by layer. A main advantage of LFP is the higher cooling rate compared to powder-based laser additive manufacturing processes due to the thermal conductivity difference between foil and powder. This study focuses on the mechanical properties of 304L stainless steel parts built by the LFP process. The experimental results indicate that the yield strength and ultimate tensile strength of LFP fabricated 304L SS parts are higher by 9% and 8% …
Investigation Of Build Strategies For A Hybrid Manufacturing Process Progress On Ti-6al-4v, Lei Yan, Leon Hill, Frank W. Liou, Joseph William Newkirk
Investigation Of Build Strategies For A Hybrid Manufacturing Process Progress On Ti-6al-4v, Lei Yan, Leon Hill, Frank W. Liou, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
The various processing parameters of a hybrid manufacturing process, including deposition and machining, is being investigated with a Design of Experiment (DoE). The intent was to explore the effect of different build strategies on the final part’s Vickers hardness, tensile test, fatigue life, and microstructure. From this experiment, the processing parameters can be linked to various mechanical properties. This will lead to the ability to create a combination of deposition and machining parameters, which will result in improved mechanical properties.
A Two-Dimensional Simulation Of Grain Structure Growth Within Substrate And Fusion Zone During Direct Metal Deposition, Jingwei Zhang, Wei Li, Frank W. Liou, Joseph William Newkirk
A Two-Dimensional Simulation Of Grain Structure Growth Within Substrate And Fusion Zone During Direct Metal Deposition, Jingwei Zhang, Wei Li, Frank W. Liou, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
In this paper, a predictive model based on a cellular automaton (CA)-finite element (FE) method has been developed to simulate thermal history and microstructure evolution during metal solidification for a laser-based additive manufacturing process. The macroscopic FE calculation that is validated by thermocouple experiment is designed to update the temperature field and a high cooling rate. A cellular automata-finite element (CAFE) method is developed to describe grain growth in the fusion zone. In the mesoscopic CA model, heterogeneous nucleation sites, grain growth orientation and rate, epitaxial growth, remelting of preexisting grains, metal addition, grain competitive growth, and columnar to equiaxed …
Investigation Of Tensile Properties Of Bulk And Slm Fabricated 304l Stainless Steel Using Various Gage Length Specimens, Sreekar Karnati, I. Axelsen, Frank W. Liou, Joseph William Newkirk
Investigation Of Tensile Properties Of Bulk And Slm Fabricated 304l Stainless Steel Using Various Gage Length Specimens, Sreekar Karnati, I. Axelsen, Frank W. Liou, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
The complex solidification dynamics and thermal cycling during Selective Laser Melting process is expected to result in non-equilibrium material characteristics. There is an essential need for characterization techniques which are critical towards the estimation of anisotropies. The current investigation is targeted towards establishing tensile testing methodologies and their relation to differing gage lengths. Dog-bone shaped specimen designs with gage lengths of 1”, 0.3” and 0.12” were employed in this research. The characterization was performed on hot rolled-annealed 304 stainless and SLM fabricated 304L stainless. It was theorized that smaller gage length specimens would be instrumental in mapping material property anisotropy …
Powders For Additive Manufacturing Processes: Characterization Techniques And Effects On Part Properties, Austin T. Sutton, Caitlin S. Kriewall, Ming-Chuan Leu, Joseph William Newkirk
Powders For Additive Manufacturing Processes: Characterization Techniques And Effects On Part Properties, Austin T. Sutton, Caitlin S. Kriewall, Ming-Chuan Leu, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Powder-bed based Additive Manufacturing is a class of Additive Manufacturing (AM) processes that bond successive layers of powder by laser melting to facilitate the creation of parts with complex geometries. As AM technology transitions from the fabrication of prototypes to end-use parts, the understanding of the powder properties needed to reliably produce parts of acceptable quality becomes critical. Consequently, this has led to the use of powder characterization techniques such as scanning electron microscopy (SEM), laser light diffraction, x-ray photoelectron spectroscopy (XPS), and differential thermal analysis (DTA) to both qualitatively and quantitatively study the effect of powder characteristics on part …
Investigation Of Heat-Affected 304l Ss Powder And Its Effect On Built Parts In Selective Laser Melting, Caitlin S. Kriewall, Austin T. Sutton, Ming-Chuan Leu, Joseph William Newkirk, Ben Brown
Investigation Of Heat-Affected 304l Ss Powder And Its Effect On Built Parts In Selective Laser Melting, Caitlin S. Kriewall, Austin T. Sutton, Ming-Chuan Leu, Joseph William Newkirk, Ben Brown
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Selective laser melting (SLM) is a powder bed based additive manufacturing process in which a layer of powder is laid over the surface of a substrate and a laser with sufficient energy is employed to selectively melt particles to build a part layer by layer. During the SLM process, dark smoke was observed coming off of the powder bed surface where the laser was interacting with powder. This phenomenon resulted from heat-affected powder that was visibly different than the base powder. Since the concentration of the heat-affected powder differs throughout the build chamber as a result of the recirculating argon …
Effect Of Powder Particle Size On The Fabrication Of Ti-6al-4v Using Laser Metal Deposition From Elemental Powder Mixture, Xueyang Chen, Lei Yan, Wei Li, Frank W. Liou, Joseph William Newkirk
Effect Of Powder Particle Size On The Fabrication Of Ti-6al-4v Using Laser Metal Deposition From Elemental Powder Mixture, Xueyang Chen, Lei Yan, Wei Li, Frank W. Liou, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Direct Laser Metal Deposition (LMD) was used to fabricate thin-wall Ti-6Al-4V using the powder mixture of Ti-6 wt.%Al-4 wt.%V. Scanning electron microscopy (SEM), optical microscopy (OM) and energy dispersive spectroscopy (EDS) were employed to examine the chemical composition and microstructure of the as-deposited sections. Vickers hardness tests were then applied to characterize the mechanical properties of the deposit samples which were fabricated using pre-mixed elemental powders. The EDS line scans indicated that the chemical composition of the samples was homogenous across the deposit. X-ray diffraction (XRD) was used for the phase identification. After significant analysis, some differences were observed among …
Modeling And Experimental Investigation Of Pre-Mixed Multi-Powder Flow In Fabricating Functional Gradient Material By Laser Metal Deposition Process, Wei Li, Jingwei Zhang, Sreekar Karnati, Yunlu Zhang, Frank W. Liou, Joseph William Newkirk, Karen M. Brown Taminger, W. L. Seufzer
Modeling And Experimental Investigation Of Pre-Mixed Multi-Powder Flow In Fabricating Functional Gradient Material By Laser Metal Deposition Process, Wei Li, Jingwei Zhang, Sreekar Karnati, Yunlu Zhang, Frank W. Liou, Joseph William Newkirk, Karen M. Brown Taminger, W. L. Seufzer
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Laser Metal Deposition (LMD) is an effective process to fabricate Functionally Graded Material (FGM) from pre-mixed powders. Since the supplied multi-powder directly affects the deposited FGM’s composition, investigation on Pre-Mixed Multi-Powder (PMMP) flow during LMD is greatly needed. This paper presents a comprehensive numerical PMMP flow model. By solving discrete particle force balance equations coupled with continuity equations and momentum equations for carrier gas, the dynamic behavior of PMMP flow through powder feeder tube and out of nozzle was calculated. With this model, the particle sizes of multi-powder were optimized to obtain considered FGM composition. To verify the modeling results, …
Proposed Hybrid Processes For Part Building Using Fusion Welding And Friction Stir Processing, Megan A. Gegesky, Frank W. Liou, Joseph William Newkirk
Proposed Hybrid Processes For Part Building Using Fusion Welding And Friction Stir Processing, Megan A. Gegesky, Frank W. Liou, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
It has been shown that a hybrid laser additive manufacturing and friction stir processing can deposit components with forged-like structures. This paper reports a hybrid fusion welding and friction stir process to create parts with quality structures. Combining traditional fusion welding and friction stir processing techniques for non-weldable aluminum alloys could facilitate the joining of difficult geometries in manufactured parts. This research illustrates mechanical property changes for non-weldable and weldable aluminum alloys. The Vickers hardness, and microhardness in the case of AA5052-H32, tensile strength and corrosion resistance of four processing states: base material, fusion welded material, friction stir welded material, …
3d Printing Of A Polymer Bioactive Glass Composite For Bone Repair, Caroline Murphy, Krishna C. R. Kolan, M. Long, Ming-Chuan Leu, Julie A. Semon, D. E. Day
3d Printing Of A Polymer Bioactive Glass Composite For Bone Repair, Caroline Murphy, Krishna C. R. Kolan, M. Long, Ming-Chuan Leu, Julie A. Semon, D. E. Day
Mechanical and Aerospace Engineering Faculty Research & Creative Works
A major limitation of synthetic bone repair is insufficient vascularization of the interior region of the scaffold. In this study, we investigated the 3D printing of adipose derived mesenchymal stem cells (AD-MSCs) with polycaprolactone (PCL)/bioactive glass composite in a single process. This offered a three-dimensional environment for complex and dynamic interactions that govern the cell’s behavior in vivo. Borate based bioactive (13-93B3) glass of different concentrations (10 to 50 weight %) was added to a mixture of PCL and organic solvent to make an extrudable paste. AD-MSCs suspended in Matrigel was extruded as droplets using a second syringe. Scaffolds measuring …
Designed Extrudate For Additive Manufacturing Of Zirconium Diboride By Ceramic On-Demand Extrusion, Devin Mcmillen, Wenbin Li, Ming-Chuan Leu, Greg Hilmas, Jeremy Lee Watts
Designed Extrudate For Additive Manufacturing Of Zirconium Diboride By Ceramic On-Demand Extrusion, Devin Mcmillen, Wenbin Li, Ming-Chuan Leu, Greg Hilmas, Jeremy Lee Watts
Mechanical and Aerospace Engineering Faculty Research & Creative Works
This work describes a process by which zirconium diboride (ZrB2) parts may be fabricated using the Ceramic On-Demand Extrusion (CODE) process. An oxide-carbide-nitride system consisting of ceramic powders and pre-ceramic organics, designed to yield ZrB2 after reaction sintering, has been developed to produce an aqueous-based extrudate for subsequent processing in the CODE system. Pressurelessly sintered test specimens containing 1 wt% PVA binder achieve high relative density ≥ 99%. The viscoelastic response of the extrudate was characterized via spindle rheometry with a small sample adapter. Batches with 1 wt% PVA and 0.5 wt% Methocel show strong shear thinning characteristic, under …
Novel Extrusion-Based Additive Manufacturing Process For Ceramic Parts, Amir Ghazanfari, Wenbin Li, Ming-Chuan Leu, Greg Hilmas
Novel Extrusion-Based Additive Manufacturing Process For Ceramic Parts, Amir Ghazanfari, Wenbin Li, Ming-Chuan Leu, Greg Hilmas
Mechanical and Aerospace Engineering Faculty Research & Creative Works
An extrusion-based additive manufacturing process, called the Ceramic On-Demand Extrusion (CODE) process, for producing three-dimensional ceramic components with near theoretical density is introduced in this paper. In this process, an aqueous paste of ceramic particles with a very low binder content (< 1 vol%) is extruded through a moving nozzle at room temperature. After a layer is deposited, it is surrounded by oil (to a level just below the top surface of most recent layer) to preclude non-uniform evaporation from the sides. Infrared radiation is then used to partially, and uniformly, dry the just-deposited layer so that the yield stress of the paste increases and the part maintains its shape. The same procedure is repeated for every layer until part fabrication is completed. Several sample parts for various applications were produced using this process and their properties were obtained. The results indicate that the proposed method enables fabrication of large, dense ceramic parts with complex geometries.
Properties Of Partially Stabilized Zirconia Components Fabricated By The Ceramic On-Demand Extrusion Process, Wenbin Li, Amir Ghazanfari, Devin Mcmillen, Ming-Chuan Leu, Greg Hilmas, Jeremy Lee Watts
Properties Of Partially Stabilized Zirconia Components Fabricated By The Ceramic On-Demand Extrusion Process, Wenbin Li, Amir Ghazanfari, Devin Mcmillen, Ming-Chuan Leu, Greg Hilmas, Jeremy Lee Watts
Mechanical and Aerospace Engineering Faculty Research & Creative Works
The Ceramic On-Demand Extrusion (CODE) process is a novel additive manufacturing process for fabricating dense ceramic components from aqueous pastes of high solids loading. In this study, 3 mol% Y2O3 stabilized tetragonal zirconia polycrystal (3Y-TZP) parts were fabricated using the CODE process. The parts were then dried in a humidity controlled environmental chamber and sintered under atmospheric pressure. Mechanical properties of the sintered parts were examined using ASTM standard test techniques, including density, Young’s modulus, flexural strength, Weibull modulus, fracture toughness and Vickers hardness. The microstructure was analyzed, and grain size was measured using scanning electron microscopy. …
A Novel Extrusion-Based Additive Manufacturing Process For Ceramic Parts, Amir Ghazanfari, Wenbin Li, Ming-Chuan Leu, Greg Hilmas
A Novel Extrusion-Based Additive Manufacturing Process For Ceramic Parts, Amir Ghazanfari, Wenbin Li, Ming-Chuan Leu, Greg Hilmas
Mechanical and Aerospace Engineering Faculty Research & Creative Works
An extrusion-based additive manufacturing process, called the Ceramic On-Demand Extrusion (CODE) process, for producing three-dimensional ceramic components with near theoretical density is introduced in this paper. In this process, an aqueous paste of ceramic particles with a very low binder content ( < 1 vol%) is extruded through a moving nozzle at room temperature. After a layer is deposited, it is surrounded by oil (to a level just below the top surface of most recent layer) to preclude non-uniform evaporation from the sides. Infrared radiation is then used to partially, and uniformly, dry the just-deposited layer so that the yield stress of the paste increases and the part maintains its shape. The same procedure is repeated for every layer until part fabrication is completed. Several sample parts for various applications were produced using this process and their properties were obtained. The results indicate that the proposed method enables fabrication of large, dense ceramic parts with complex geometries.
Freeform Extrusion Fabrication Of Titanium Fiber Reinforced Bioactive Glass Scaffolds, Albin Thomas, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas
Freeform Extrusion Fabrication Of Titanium Fiber Reinforced Bioactive Glass Scaffolds, Albin Thomas, Krishna C. R. Kolan, Ming-Chuan Leu, Greg Hilmas
Mechanical and Aerospace Engineering Faculty Research & Creative Works
Although implants made with bioactive glass have shown promising results for bone repair, their application in repairing load-bearing long bones is limited due to their low fracture toughness and fairly fast degradation response in vivo. In this paper, we describe our investigation of freeform extrusion fabrication of silicate based 13-93 bioactive glass scaffolds reinforced with titanium fibers. A composite paste was prepared with 13-93 bioactive glass filled with titanium fibers (~16 µm in diameter and aspect ratio of ~250) having a volume fraction of 0.4 vol. %. This paste was then extruded to fabricate scaffolds with an extrudate diameter …
Effects Of Temperature On Aqueous Freeform Extrusion Fabrication, Jie Li, Ming-Chuan Leu, Greg Hilmas
Effects Of Temperature On Aqueous Freeform Extrusion Fabrication, Jie Li, Ming-Chuan Leu, Greg Hilmas
Mechanical and Aerospace Engineering Faculty Research & Creative Works
An experimental study was conducted to investigate the effect of temperature on ceramic parts produced by paste extrusion based additive manufacturing followed by sintering. A computer-controlled gantry system equipped with a piston extruder was used to extrude aqueous alumina paste. The system includes a temperature control subsystem that allows for freeform extrusion fabrication inside a low-temperature (<0°C) chamber. It can also be used for fabricating parts on a hot plate at ambient or higher temperatures (≥20°C). Test specimens were fabricated from aqueous aluminum pastes at -20°C in the low-temperature chamber and also on the hot plate at 40°C. The minimum angles achievable by these two processes for part fabrication, without use of support material, were compared. Also compared were the relative density and mechanical properties of the parts obtained after sintering. Microstructures were examined via scanning electron microscopy in order to obtain a deeper understanding of the effect of fabrication temperature.
Laser Metal Deposition Of Functionally Gradient Materials From Elemental Copper And Nickel Powders, Sreekar Karnati, Todd E. Sparks, Frank W. Liou, Joseph William Newkirk, Karen M. Brown Taminger, William J. Seufzer
Laser Metal Deposition Of Functionally Gradient Materials From Elemental Copper And Nickel Powders, Sreekar Karnati, Todd E. Sparks, Frank W. Liou, Joseph William Newkirk, Karen M. Brown Taminger, William J. Seufzer
Mechanical and Aerospace Engineering Faculty Research & Creative Works
This work deals with the planning and fabrication of a functionally gradient copper-nickel composition via Laser Metal Deposition (LMD). Various compositions of copper and nickel were made by blending different weight percentages which were then sequentially deposited to fabricate functionally gradient copper-nickel thin-wall structures. Analyses were performed by sectioning the thin-wall samples for metallographic, hardness, X-ray diffraction (XRD) and Energy Dispersive X-ray Spectroscopy (EDS) studies. The fabrication was studied for identifying and corroborating the deposited compositions and their corresponding gradients. XRD analyses were performed to identify the crystal structure of the deposit. EDS analysis was instrumental in identifying the variation …
Microstructure And Property Of Tib-Reinforced Ti Alloy Composites By Laser Metal Deposition, Yunlu Zhang, Jingwei Zhang, Frank W. Liou, Joseph William Newkirk
Microstructure And Property Of Tib-Reinforced Ti Alloy Composites By Laser Metal Deposition, Yunlu Zhang, Jingwei Zhang, Frank W. Liou, Joseph William Newkirk
Mechanical and Aerospace Engineering Faculty Research & Creative Works
TiB-reinforced Ti alloy composites have been laser deposited with pre-alloyed Ti-6Al4V-1B powder. The microstructure of the as-deposited and heat treated composites have been characterized in detail using scanning electron microscope (SEM). A homogeneous dispersion of needle-like TiB precipitates is formed in the Ti-6Al-4V α/β matrix. TiB precipitates promote formation of small near equaxed α/β grain after β annealing process. The micro-hardness of the laser deposited composites increase 20-30% with 5 vol. % TiB precipitates compared to unreinforced Ti-6Al-4V deposits.
In Vitro Assessment Of Laser Sintered Bioactive Glass Scaffolds With Different Pore Geometries, Krishna C. R. Kolan, Albin Thomas, Ming-Chuan Leu, Greg Hilmas
In Vitro Assessment Of Laser Sintered Bioactive Glass Scaffolds With Different Pore Geometries, Krishna C. R. Kolan, Albin Thomas, Ming-Chuan Leu, Greg Hilmas
Mechanical and Aerospace Engineering Faculty Research & Creative Works
The pore geometry of bioactive glass scaffolds intended for use in bone repair or replacement is one of the most important parameters that could determine the rate of bone regeneration. The pore geometry would also affect the mechanical properties of the scaffolds and their rate of degradation. Scaffolds with five different architectures, having ~50% porosity, were fabricated with silicate (13–93) and borate (13–93B3) based bioactive glasses using a laser sintering process. An established, late-osteoblasts/early-osteocytes cell line was used to perform cell proliferation tests on the scaffolds. The results indicated that the cells proliferate significantly more on the scaffolds which mimic …