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Full-Text Articles in Metallurgy
Investigation Into Oxygen Diffusion As It Relates To Alpha Case Formation In Ti-6al-4v Based On Different Forging Thermal Cycles, Tyler J. Meador, Jon Leduc, Francesca Hope
Investigation Into Oxygen Diffusion As It Relates To Alpha Case Formation In Ti-6al-4v Based On Different Forging Thermal Cycles, Tyler J. Meador, Jon Leduc, Francesca Hope
Materials Engineering
An investigation into the growth kinetics of alpha case in Ti-6Al-4V in the presence of oxygen was conducted for different forging thermal cycles. This was done to determine whether the alpha case should be removed after each thermal cycle or as the final step after forging. The thermal cycles consisted of four hours at 1750 °F. Samples were subjected to this treatment one, two, three, and four times along with a continuous sixteen hour hold. Four cycle and Hold samples were subjected to an additional thermal cycle above the beta transus at 1925 °F. These then went through a final …
Improving The Tensile Mechanical Properties Of Direct Energy Deposited (Ded) Inconel 718 Aircraft Components Using A Standard Heat Treatment, Spencer Vincent Flynn
Improving The Tensile Mechanical Properties Of Direct Energy Deposited (Ded) Inconel 718 Aircraft Components Using A Standard Heat Treatment, Spencer Vincent Flynn
Materials Engineering
This project aimed to improve the mechanical properties of as-printed additively manufactured Inconel 718 samples using a heat treatment usually used for cast and wrought Inconel 718. The mechanical properties sought to be optimized were yield strength, ultimate tensile strength, elongation, and reduction in area. The property goals were to match or exceed those of cast and heat treated Inconel 718. Wire-fed electron beam direct energy deposition (DED) was used to manufacture the samples, which were then heat treated using the AMS 5663 standard in an inert atmosphere. The samples were then tested in tension to obtain data on their …
Analysis Of Novel Corrosion Resistant Maraging Steels For Use In Additive Manufacturing, Bradley Michael Samuel, James Knowlton Smith
Analysis Of Novel Corrosion Resistant Maraging Steels For Use In Additive Manufacturing, Bradley Michael Samuel, James Knowlton Smith
Materials Engineering
Stainless maraging steel has been proven to be an industry standard material for plastic injection molds. Its high hardness and corrosion resistance extend the lifetime of the tool. This alloy system is also well-suited to additive manufacturing, which can be utilized to form internal cooling channels, further increasing tool life. Using Rapid Alloy Development (RAD) Oerilkon METCO is developing a new composition of stainless maraging tool steel that has high hardness/strength, is corrosion resistant, and has additive-capable melting and solidification properties. This study tests the hardness and corrosion resistance of the new RAD alloys against the current market competitor Corrax …
Microstructure And Tensile Properties Of Close-Die Forged Ti-6al-4v Aircraft Engine Mount, Renee Roeder, Nick Chen, Michael Viksne
Microstructure And Tensile Properties Of Close-Die Forged Ti-6al-4v Aircraft Engine Mount, Renee Roeder, Nick Chen, Michael Viksne
Materials Engineering
The microstructural characteristics of a Ti-6Al-4V close-die forging that passes yield strength specifications are examined and found to be consistent with literature recommendations. Originally, the intent was to compare the microstructure of a forging that passed specification to the microstructure of a forging that did not pass specifications using the imaging software ImageJ. Due to time and safety constraints considering the COVID-19 pandemic, the data that is presented is incomplete data on only the forging that passes specifications. There are no comparisons between the forging that did not pass and the forging that passed.
Microstructural Transformation Of Cold-Sprayed Grcop-42 For Rocket Engine Combustion Chamber Liners, Mason Souther
Microstructural Transformation Of Cold-Sprayed Grcop-42 For Rocket Engine Combustion Chamber Liners, Mason Souther
Materials Engineering
Rocket engines have always relied on high-conductivity copper liners to protect structural components from extreme thermal loads produced by combustion. Forged NARloy-Z has been the material of choice for decades but increasing cost of its constituent silver and high waste in the machining process has reduced the alloy’s cost effectiveness. Aerojet Rocketdyne wants to determine the viability of cold-spray additively manufactured GRCop-42 as a replacement alloy to reduce liner cost. Screening tests were performed to observe the microstructural development and microhardness changes of cold-sprayed GRCop-42 after being subjected to multiple stages of the typical heat treatment of a combustion chamber …
Weld Fracture Between C450 Stainless And C300 Maraging Steels In Golf Club Heads, Emily Oreste, Shea Costner
Weld Fracture Between C450 Stainless And C300 Maraging Steels In Golf Club Heads, Emily Oreste, Shea Costner
Materials Engineering
This project studied fractures along the weld on the face of TaylorMade metalwood golf clubs. The weld joint investigated was between investment cast C450 stainless steel and hot rolled C300 maraging steel that had been joined by plasma arc welding (PAW). Cracking in the welds between these two metals was discovered during in-house prototype testing. To understand the differences between the clubs with intact weld joints and clubs with fractured weld joints, the microstructures throughout the weld zones were imaged and a grid of microhardness values of the entire sample cross-section was generated. The images and hardness values were analyzed …
Investment Cast C450 Microstructural Characterization In Golf Club Heads, Kenneth Yin-Fai Lau
Investment Cast C450 Microstructural Characterization In Golf Club Heads, Kenneth Yin-Fai Lau
Materials Engineering
Two types of tensile bars were observed in this study of golf iron heads for TaylorMade Golf. As-cast and as-cast then machined tensile bars. The tensile bars underwent tensile tests to observe tensile strength, percent elongation, and fracture mechanisms. Furthermore, the hardness of the tensile bars was also taken despite seeing no difference in sample types. However, the as-cast samples did not consistently meet the requirements of percent elongation > 10.00% as there was a sample with 0.00% and another with 1.26%. These samples also showed brittle fracture, instead of the desired cup-and- cone ductile fracture. To investigate further, transverse sections …
Investigation Of Copper Infiltration Alloys For Use In Metal Matrix Composite Drill Bits, Samuel J. Stueland, Timothy P. Markiewicz
Investigation Of Copper Infiltration Alloys For Use In Metal Matrix Composite Drill Bits, Samuel J. Stueland, Timothy P. Markiewicz
Materials Engineering
A newly developed copper-based alloy, P98-X1 was tested for compressive strength to predict qualitative performance compared to MF53, F-Bronze, CuNiSn, and CuMnNi for use as the infiltration alloy in metal matrix composite (MMC) drill bits. Ingots of each alloy were cast using an arc furnace and cut into compression testing samples using wire electrical discharge machining (EDM). The alloys were selected for testing based on solid solution strengthening coefficient and melting point. Five of each alloy were compression tested to determine yield strength of the infiltration alloy. Yield strength was determined using a 0.002mm displacement offset from the linear elastic …
Rotating Beam Fatigue Of Forged 2219-T852 Aluminum Alloy, Julio Escamilla, Madison Reed
Rotating Beam Fatigue Of Forged 2219-T852 Aluminum Alloy, Julio Escamilla, Madison Reed
Materials Engineering
2219 aluminum has been used extensively in aerospace applications due to its ability to retain strength in large section thicknesses, thus making it ideal for large forgings. However, the Metallic Materials Properties Development and Standardization (MMPDS) handbook, a source of design data for aerospace industry applications, lacks information on 2219 in the T852 condition, particularly concerning the behavior of the alloy under cyclic loading conditions. Data was collected for forgings of 2219-T852 aluminum as produced by Weber Metals to determine the fatigue life of the alloy-temper combination and to assess the effects of forge thickness and orientation on fatigue life. …
The Effects Of Varying Composition And Build Direction On Direct Metal Deposition Fabricated Inconel 718, Abigail P. Nilan, Jessica M. Fordham
The Effects Of Varying Composition And Build Direction On Direct Metal Deposition Fabricated Inconel 718, Abigail P. Nilan, Jessica M. Fordham
Materials Engineering
Inconel 718 (IN718) is a popular wrought superalloy, and is currently being investigated for additive manufacturing (AM) applications in the aerospace industry. However, overaging and the presence of microcracks have caused a significant reduction in properties. The purpose of this study is to meet or exceed the mechanical properties of wrought IN718 by varying the composition and build direction of the AM alloy. Alternative compositions were selected with Oerlilon Metco’s Rapid Alloy Development (RAD) software, and differ in niobium content, which increases the fraction of the primary strengthening phase (γʺ). Direct metal deposition (DMD) was used to fabricate the samples, …
Effects Of Head Formation And Heat Treatment On The Mechanical Properties Of Connecting Rod Bolts, Caleb A. Leavitt, Matthew R. Lauretta
Effects Of Head Formation And Heat Treatment On The Mechanical Properties Of Connecting Rod Bolts, Caleb A. Leavitt, Matthew R. Lauretta
Materials Engineering
Oliver Racing Parts (ORP; Charlevoix, Michigan) is looking to optimize their manufacturing process for high-strength connecting rod bolts. A high yield strength is desired for the bolts because deformation would result in catastrophic engine failure. The bolts were made of H11, a chromium hot-work tool steel; and MLX17, a precipitation hardenable stainless steel. Tensile testing was performed to determine the tensile and yield strengths of the bolts. Fracture surfaces were imaged via scanning electron microscopy to characterize the failure modes. To observe the effects of bolt heading on microstructure and bolt strength, two batches of MLX17 were prepared; one batch …
Characterization Of The 15-5 Stainless Steel Electric Discharge Machining Recast Layer, Julian R. Lohser, Rhys W. Gilmore
Characterization Of The 15-5 Stainless Steel Electric Discharge Machining Recast Layer, Julian R. Lohser, Rhys W. Gilmore
Materials Engineering
Electric discharge machining (EDM) is a non-conventional machining process that is used for tough, hard materials or materials that require no tool force. Wire EDM produces a recast layer and heat-affected zone as a result of rapid melting and quenching at the surface of the cut. A secondary machining operation has been required to remove this layer. Previous estimates of the depth of the recast layer are likely too conservative due to improvements in the technology; therefore, the goal of this study is to characterize and more accurately investigate the size of the layer. Two EDM machine parameters, voltage and …
Analysis Of Shear Strength Variance Of Ph 15-7 Mo Blind Rivet Stems For Aerospace Applications, Miles Macarthur, Kent C. Majewski
Analysis Of Shear Strength Variance Of Ph 15-7 Mo Blind Rivet Stems For Aerospace Applications, Miles Macarthur, Kent C. Majewski
Materials Engineering
This project attempts to reduce manufacturing costs incurred to Cherry Aerospace by variance in material properties. To track and predict the shear strength of PH 15-7 Mo stainless steel rivet stems throughout the heat treatment process, samples were taken from several steps in the manufacturing process and experimental heat treatments were performed across a range of temperatures. The supplied rivet stems were heat treated for four hours at temperatures from 520°C to 560°C, in increments of 10°C. Double shear testing in accordance with ASTM 1312-13A revealed that there is no apparent correlation between the strength of the supplied wire and …
The Effects Of Austempering And Cryogenic Processing On The Mechanical Properties Of Forged E4340 Steel For Automotive Engine Connecting Rods, Aaron Taylor Ludlow
The Effects Of Austempering And Cryogenic Processing On The Mechanical Properties Of Forged E4340 Steel For Automotive Engine Connecting Rods, Aaron Taylor Ludlow
Materials Engineering
The components in top-fuel dragster and stock car engines undergo significantly more force than their production passenger vehicle counterparts do. Therefore, they must be manufactured and processed to withstand those forces so that they do not catastrophically fail while in service. In this project, the effects of austempering and adding a cryogenic processing step to the control quench and double temper heat treatment on the tensile and hardness properties of E4340 high-strength steel were examined. Tensile test samples were machined from raw connecting rod forgings and underwent either a quench-double temper heat treatment, an austempering heat treatment, or the quench-double …
Electrochemical Characterization Of Precious Metal Braze Alloys Using Potentiodynamic Polarization, Maxwell Glen Martin, Mason Gregory Morgan, Matthew David Vance
Electrochemical Characterization Of Precious Metal Braze Alloys Using Potentiodynamic Polarization, Maxwell Glen Martin, Mason Gregory Morgan, Matthew David Vance
Materials Engineering
This study aimed to characterize the electrochemical behavior of six precious metal braze alloys by performing potentiodynamic polarization tests (ParStat 2273) based on ASTM Specifications G5 and G59. To determine the extent to which the alloys will contribute to galvanic corrosion in a marine environment (3.5 wt% NaCl), corrosion analysis software was used to produce fitted Tafel lines to determine the open circuit potential, Voc, for each alloy. The Voc values for the alloys were found to be -66.58 mV for Gold ABA, 13.01 mV for Nicoro®, -39.00 mV for Nioro®, 23.4 mV …
High Cycle Rotating Bending Fatigue Of 6061-T6 Friction Stir Welded Extrusions, John Chang, Travis Miller
High Cycle Rotating Bending Fatigue Of 6061-T6 Friction Stir Welded Extrusions, John Chang, Travis Miller
Materials Engineering
Fatigue testing was done on friction stir welded joints of 6061-T6 aluminum extrusions. Tests were run using a rotating bending fatigue machine at stresses from 111.5 to 138.7 MPa. Failures occurred on the order of 105 to 107 cycles, and an S-N curve was generated based off of the failure results. After the samples failed, the location of the failure and the number of cycles to failure were noted. Fatigue samples were designed in SolidWorks with a tapered 2 inch reduced section. The 2 inch reduced section will include the entire weld region as seen from the microhardness …
Relationship Between Bagging Methods And Pre-Weld Holding Times On Porosity Formation In 2219 Aluminum Ac-Tig Welds, Mariah Grace Head, Tyson Daniel Mobley
Relationship Between Bagging Methods And Pre-Weld Holding Times On Porosity Formation In 2219 Aluminum Ac-Tig Welds, Mariah Grace Head, Tyson Daniel Mobley
Materials Engineering
The purpose of this study was to determine relationships between bagging methods and pre-weld holding times on the formation of porosity when AC-TIG welding 2219 aluminum. Considering the strict guidelines and specifications required within the aerospace industry, maintaining quality welds is of paramount importance to control part integrity for aerospace applications. This project focused on two parameters involved in the preparation of aluminum parts for welding: bagging method and pre-weld holding time. Welding geometry was simplified to bead-on plate instead of the standard joint welds. Radiographic analysis of the samples showed that all levels of both parameters produced “passing welds.” …
Residual Stress Measurement Of 7050 Aluminum Alloy Open Die Forgings Using The Hole-Drilling Method, Alexandra Viksne
Residual Stress Measurement Of 7050 Aluminum Alloy Open Die Forgings Using The Hole-Drilling Method, Alexandra Viksne
Materials Engineering
Open die forged 7050 aluminum alloy has residual stresses that can be measured by the hole-drilling method following standard ASTM E837-01. Weber Metals (Paramount, CA) assumes that the stress is uniform throughout the thickness of an open die forged plate. Four different stress relieved 7050 aluminum samples were tested to confirm if the measurements by the hole-drilling method at the surface of a plate is indicative of the stress throughout. The different stress relief methods included: two water quenched samples at temperature ranges of 60°-90°F and 120°-130°F and two samples plastically deformed by forging at room temperature 1% and 3%. …
Evaluation Of High Phosphorus Electroless Nickel Platings To Protect Carbon Steel Heat Exchangers In Seawater Service, Nathan Brink
Evaluation Of High Phosphorus Electroless Nickel Platings To Protect Carbon Steel Heat Exchangers In Seawater Service, Nathan Brink
Materials Engineering
The purpose of this project was to determine the suitability of using a high phosphorus electroless nickel (HPEN) coating to prevent corrosion in carbon steel heat exchangers in seawater service. 1 in. x 4 in. samples were cut from ¼ in. SA-516-70 pressure vessel plate, pickled to remove mill scale, dressed with 300 grit sand paper and sent out for plating with 2 mils of HPEN. Due to a clerical error during plating, samples were plated to a significantly lesser extent than requested. Samples were plated with approximately 0.6 mils of HPEN versus the 2 mils requested, however this was …
Mechanical Properties And Microstructures Of Incoloy 909 Rolled Rings Subjected To A Modified Forging Cycle, Colin Lee Elliott Glaves
Mechanical Properties And Microstructures Of Incoloy 909 Rolled Rings Subjected To A Modified Forging Cycle, Colin Lee Elliott Glaves
Materials Engineering
The microstructure of rolled rings of Incoloy 909 nickel-iron-cobalt superalloy subjected to a standard customer solution and aging treatment exhibited unacceptably large grains. Samples cut from a failed ring were mounted and polished for analysis. The samples were etched with a modified Kalling’s waterless reagent and metallographic analysis was done to identify characteristic large grain structures distributed among the desired smaller grain structures. The large grains were identified and noted for comparison to later samples. Two test rings were forged out of Incoloy 909 using revised forging procedures involving reduced soak temperatures before each forging step. Metallographic samples were cut …
Evaluation Of Forging Strain For Maximum Grain Size In Open-Die Forged 6061 Aluminum, Eric Strehl
Evaluation Of Forging Strain For Maximum Grain Size In Open-Die Forged 6061 Aluminum, Eric Strehl
Materials Engineering
In an effort to maximize grain growth of open-die forged 6061 aluminum alloy parts, samples from three of Weber Metals’s suppliers (Hidal Co-Almex USA Inc., TST Inc., and Vista Metals Corp.; to be called Supplier H, Supplier T, Supplier V respectively) were cut into cylinders with diameters of 0.75˝ and heights of 2˝, and put through a simulated forging process and heat treatment. It is possible that additional alloying elements may be promoting or inhibiting grain growth in the final part. Maximizing grain growth for aluminum alloy parts results in improved resistance to intergranular corrosion. Samples from each vendor had …
Characterization And Analysis Of Low Room Temperature Ductility Nickel-Based Superalloy 718 Plus For Aircraft Engine Forgings, Jonathon Bracci
Characterization And Analysis Of Low Room Temperature Ductility Nickel-Based Superalloy 718 Plus For Aircraft Engine Forgings, Jonathon Bracci
Materials Engineering
Schlosser Forge Co. forges low pressure turbine (LPT) cases from the nickel based superalloy 718 Plus using the ring rolling forging process. Schlosser has been experiencing low room temperature ductility problems in a number of their 718 Plus LPT cases. LPT cases are required to pass a 4D tensile test at room temperature with a minimum of 15 percent elongation. The ductility problem was reduced by increasing the forging temperature from 1825˚F to 1850˚F. Analysis was performed on 718 Plus samples taken from forged LPT cases that failed the room temperature ductility requirement and ones that passed the requirement. The …
Discontinuous Grain Boundaries Of Forged René 41, Steven Crump
Discontinuous Grain Boundaries Of Forged René 41, Steven Crump
Materials Engineering
Forged components must pass a grain size specification (grain size, distribution) for acceptance in an application. The varying amounts of plastic deformation during forging can lead to abnormally large recrystallized grain sizes in certain regions of the part, which will not pass specification. The question exists whether these abnormally coarse grains are truly comprised of poly crystalline fine grains with grain boundaries resistant to etching techniques. To investigate this abnormal grain size effect, a cross section of a forged René 41 nickel-based superalloy aircraft engine ring was cut and sectioned into six segments. Those segments were then prepared for microstructural …
Effect Of Heating Temperature, Heating Time And Initial Microstructure On Recrystallization Of Waspaloy During Heating For Forging, Marissa Hill
Materials Engineering
A fine, uniform grain size is required for creep limited Waspaloy in aircraft engine applications. Upon heating, Waspaloy does not always recrystallize in a uniform manner resulting in occasional large grains with a majority of the grains meeting the grain size requirements. Waspaloy’s microstructure was analyzed with different heat treatments and in the as-forged condition. The strengthening mechanism is the gamma prime phase. The gamma prime solvus temperature is 1908°F so the different heat treatments were determined around that temperature, as well as the forging temperature range of 1800-2150°F. At the 1850°F heat treatment, the microstructure recrystallized with small grains, …
Morphology And Roughness Of Al2o3 On Ferritic Stainless Steel Foil For Diesel Catalytic Converter Applications, Megan Butala
Morphology And Roughness Of Al2o3 On Ferritic Stainless Steel Foil For Diesel Catalytic Converter Applications, Megan Butala
Materials Engineering
The improved thermal properties of metal-substrate catalytic converters enable effective catalysis sooner after ignition than traditional ceramic monoliths, resulting in less harmful emissions. ACAT Global, a manufacturer of stainless steel catalytic converters, uses ferritic stainless steel substrates for low temperature catalytic converters for diesel automobiles. Production begins with an oxidizing heat treatment to increase surface roughness. The success of the second production step, the application of catalyst-containing ceramic slurry (washcoat), depends on the surface roughness that results from oxidation. Formation of the primary oxide of interest, alumina (Al2O3), is controlled by the stainless steel foil composition, …
Microstructural Characterization Of Ti-6al-4v And Its Relationship To Sample Geometry, Blake Gaspar
Microstructural Characterization Of Ti-6al-4v And Its Relationship To Sample Geometry, Blake Gaspar
Materials Engineering
A problem exists with a part produced by forging made by Shultz Steel of Ti-6Al-4V in the variance of properties throughout the part. There is one specific region that exhibits the most variance. The purpose of the report is to determine any microstructural differences within the region of interest in the part. When microstructures of the inner section and outer section of the part were looked at it was determined that they exhibited a martensitic structure. There was a noticeable difference in the lath structure between sections. The outer region contained larger more widely spread laths of an average length …
Characterization Of Positive Macrosegregation At The Subsurface Of Direct-Chill Cast 7050 Aluminum Forging Billets, Aaron Youril
Characterization Of Positive Macrosegregation At The Subsurface Of Direct-Chill Cast 7050 Aluminum Forging Billets, Aaron Youril
Materials Engineering
Segregation of alloying elements during casting of forging billets may persist to the final forged component leading to unacceptable surface appearance. Determination of the elements or compounds that segregate is the essential first step to solving this problem. Differential Scanning Calorimetry (DSC) was used to determine a composition profile of the macrosegregation occurring at the subsurface of an as-cast 7050 aluminum alloy billet. Data collection was carried out by separating 10 to 20 mg samples from the outer centimeter along the radius of the billet, as well as samples from the bulk interior of the billet for comparison with the …
Characterization Of The Relationship Between The Microstructure And Tensile Strength Of Annealed Ti-6al-4v, Aldo Corona
Characterization Of The Relationship Between The Microstructure And Tensile Strength Of Annealed Ti-6al-4v, Aldo Corona
Materials Engineering
Tensile coupons of Ti-6Al-4V were heat treated at varying annealing temperatures from 1200°F (648°C) to 1450°F (787°C) at 50°F (23°C) increments for 1 hour. The samples were air cooled to room temperature or furnace cooled to 800°F (426°C) followed by air cooling to room temperature. Four tensile coupons were treated at each annealing temperature and cooling rate. Alpha case was observed to form on the surface of the samples post heat treatment with a maximum depth of 25 µm (.001 in). Samples were tensile tested for their ultimate tensile strength, yield strength, and percent elongation. Samples across all annealing temperatures …