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Boise State University Theses and Dissertations

Theses/Dissertations

Tungsten

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Spark Plasma Sintering Of Tungsten And Tungsten-Ceria: Microstructures And Kinetics, Jeffrey Bryce Perkins Dec 2011

Spark Plasma Sintering Of Tungsten And Tungsten-Ceria: Microstructures And Kinetics, Jeffrey Bryce Perkins

Boise State University Theses and Dissertations

Tungsten casting is impractical, and tungsten compacts are most often produced by press-and-sinter or by hot pressing. The temperatures typically required to sinter tungsten above 90% dense are above 1800 ºC, and sintering times are typically hours. Alternatively, spark plasma sintering (SPS) can be used to consolidate materials to high densities at lower temperatures and shorter times than traditional sintering techniques. In this study, pure tungsten and tungsten with 1, 4, 10, 15, and 20 weight percent ceria were spark plasma sintered at varying pressures, temperatures, and times to investigate the microstructures and the kinetics of sintering.

Densification of tungsten …