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Synthesis Of Epoxy Monoethanolamide From Bauhinia Monandra Seed Oil, Adewale Adewuyi, Rotimi A. Oderinde
Synthesis Of Epoxy Monoethanolamide From Bauhinia Monandra Seed Oil, Adewale Adewuyi, Rotimi A. Oderinde
Makara Journal of Technology
In this study, we synthesized epoxidised monoethanolamide (EMA) from Bauhinia monandra seed oil (BMO) via a simple reaction route. In this process, BMO was transesterified to obtain a mixture of methyl esters, which was subjected to a urea adduct complexation reaction. The unsaturated methyl esters (BME) from the urea adduct complexation reaction were then epoxidised using performic acid produced in situ in a one-pot reaction system. The epoxidised methyl esters were converted to EMA by reacting them with monoethanolamine (1:10). The progression of the reaction was monitored using Fourier transform infrared spectroscopy and proton nuclear magnetic resonance spectroscopy, and the …