Materials Science and Engineering Commons^™

Properties Of Rice Husk Particle Boards Bonded By A Blend Of Tannin-Cnsl Resin, J. V. Tesha

Tanzania Journal of Engineering and Technology (TJET)

There are vast quantities of agricultural residues available in Tanzania. Rice husk being amongst those residues is reported to have low resistance to alkalis, high silica content, and have short fibres. These factors have made rice husks not attractive raw materials in panels’ production. However, it has been demonstrated that rice husks can be used to develop panel products of low cost and good performance if appropriate indigenous technologies and affordable binders that can bind siliceous materials are used.

This paper provides a summary on the study of the effectiveness of the binding characteristics of a blend of natural adhesive …

Iodat Analysis Content In Cooking Ingredients Using Iodometry And X-Ray Fluorescence Methods., Nelson Saksono

Makara Journal of Technology

Iodat Analysis Content in Cooking Ingredients Using Iodometry and X-ray Fluorescence Methods. Salt iodization program using iodine fortification into salt method is the best method that is effective and economical to overcome the problems caused by iodine deficiency. However in, its development there are some issues clamed that the use of iodized salt is ineffective since iodine content reduces, even disappear when the salt mix with other cooking ingredients. In order to investigated the existence of iodine in cooking ingredients, a research applying iodometry and X-ray fluorescence methods was carry out. The result obtained by iodometry method showed decreases in …

Emission Gas Reducer On Motor Vehicle, Automobile, Light Engine Of Boat And Stationary Combustion Engine., I Gusti Bagus Wijaya Kusuma

Makara Journal of Technology

Emission gas reducer on motor vehicle, automobile, light engine of boat and stationary combustion engine. The use of motor vehicle should be followed by protection against damages on the environment, since the exhaust gas from combustion engine has significantly affect on air and environmental pollution. One method to solve the problems in air pollution has been done by using a re-heater designed in Mechanical Engineering Department, University of Udayana. In accordance to the test on the re-heater, it can be seen very clear that the re-heater has significantly reduce the CO emission of about 54%. It also reduces the CO2 …

Application Of Remote Sensing For Mapping Soil Organic Matter Content, Bangun Muljo Sukojo, Wahono Wahono

Makara Journal of Technology

Application of Remote Sensing for Mapping Soil Organic Matter Content. Information organic content is important in monitoring and managing the environment as well as doing agricultural production activities. This research tried to map soil organic content in Malang using remote sensing technology. The research uses 6 bands of data captured by Landsat TM (Thematic Mapper) satellite (band 1, 2, 3, 4, 5, 7). The research focuses on pixels having Normalized Difference Soil Index (NDSI) more than 0.3. Ground-truth data were collected by analysing organic content of soil samples using Black-Walkey method. The result of analysis shows that digital number of …

Optimation Model Of Planning Investment Dockyard With Approach Multi Objective Goal Programming, Ali Azhar

Makara Journal of Technology

Optimation model of planning investment dockyard with approach multi objective goal programming. The purpose of this research is to determine decision variable, goal function, alternative priority and achievement function in investment planning. From this optimation component, the model of ship yard investment planning could be achieved. The model of developed model in this research was the optimation of ship yard investment planning using multi objective goal programming approach. The model consist of 5 decision variable, 11 goal function, 2 alternative priority and 11 achievement functions. The model implementation was done toward PT ASSI investment planning. The calculation using from Quantitative …

Self-Ignition Properties Of Peat, Palm Shell Fibre And Woods, Yulianto Sulistyo Nugroho

Makara Journal of Technology

Self-ignition properties of peat, palm shell fibre and woods. Forest fire is one of the greatest environmental problems faced by Indonesia. Forest fires have destroyed million hectares of forest and land which cause economic loss, social problems including smoke related diseases and environmental disaster with long time consequences. The exothermic reactions of forest fuels that lead to fire can be initiated by a piloted flame and low-temperature oxidation mechanism. This paper presents the results of low temperature oxidation studies using forests fuel samples i.e. palm shell fibre, peat, woods and low-rank coal. The measured values of the critical oven temperatures …

The Use Of 2d Plastic Grating For Surface Profile And Dimension Manufacture Product Measurements By Using Ndt Moiré Technique, Retno Wigajatri P., Dini Andiani

Makara Journal of Technology

The Use of 2D Plastic Grating for Surface Profile and Dimension Manufacture Product Measurements by Using NDT Moiré Technique. Research of measuring the shape and dimension of object using the moiré technique have been done. Measurement have been made by observing the moiré space as a result of interaction between grating and its shadow casted on the object’s surface caused by the projector lamp with CCD camera. The acquired data was further processed by way of off-line. By successive phase shifts that is π/2, π dan 3π/2 towards the table tennis ball at the distance of 48 cm from the …

Nonstoichiometry And Electrical Transport In Sc-Doped Zirconia, Igor Kosacki, Harlan U. Anderson, Yasunobu Mizutani, Kenji Ukai

Materials Science and Engineering Faculty Research & Creative Works

The results of electrical conductivity measurements on ZrO₂: Sc (ScSZ) ceramics as a function of oxygen activity and temperature are presented. The influence of the microstructure on electrical transport is discussed and the experimental data for dense microcrystalline specimens have been compared with those obtained for dense nanocrystalline thin films. From these results the electronic and ionic contribution to the electrical transport has been determined and correlated with microstructure. It has been found that nanocrystalline ScSZ films possess quite different nonstoichiometry compared with that observed for microcrystalline specimens in the fact that the electronic conductivity is enhanced so …

Phase Diagram For Stripes In Yba2cu3o6+X Superconductors, Herbert A. Mook, Fatih Dogan

Materials Science and Engineering Faculty Research & Creative Works

Neutron scattering has been used to measure the charge and spin structure in the YBa₂Cu₃O_6+x superconductors. Incommensurate static charge ordering is found at low doping levels while only charge fluctuations are found at higher doping. The spin structure is complex with both a commensurate resonance and incommensurate structure observed at low temperatures. The scattering results are used to construct a phase diagram for stripes in the YBa₂Cu₃O_6+x system.

The Effect Of Convection On Disorder In Primary Cellular And Dendritic Arrays, R. Trivedi, P. Mazumder, Surendra N. Tewari

Chemical & Biomedical Engineering Faculty Publications

Directional solidification studies have been carried out to characterize the spatial disorder in the arrays of cells and dendrites. Different factors that cause array disorder are investigated experimentally and analyzed numerically. In addition to the disorder resulting from the fundamental selection of a range of primary spacings under given experimental conditions, a significant variation in primary spacings is shown to occur in bulk samples due to convection effects, especially at low growth velocities. The effect of convection on array disorder is examined through directional solidification studies in two different alloy systems, Pb-Sn and Al-Cu. A detailed analysis of the spacing …

Metastable Phases Of Mgo-Tio2 Solid Solutions, Liang-Chieh Ma

Masters Theses

Magnesium titanium oxide powders were synthesized by the sol-gel method using alkoxides of magnesium and titanium with different ratios. Matastable phases of qandilite, Mg₂TiO₄, were found with Mg:Ti ratios down to 1.52:1 in lower temperature 600 °C than in the equilibrium condition which is above 1200 °C. Powder samples were examined by neutron powder diffraction and X-ray photoelectron spectroscopy (XPS) for analysis of structure and oxidation states. Also, samples were tested for the Mg:Ti ratios by induced coupled plasma atomic emission spectrometry. The structure refinements of the samples were done by General Structure Analysis System (GSAS) …

Electrical Properties Of Srbi₂Ta₂O₉ Ferroelectric Thin Films At Low Temperature, Pingxiong Yang, David L. Carroll, John Ballato, Robert W. Schwartz

Mechanical and Aerospace Engineering Faculty Research & Creative Works

The temperature dependence of electrical properties for SrBi2Ta2O9 thin film capacitors with platinum electrodes (Pt/SBT/Pt) on silicon wafers was studied from 10 to 300 K. with a decrease in temperature from 300 to 200 K, the remanent polarization of the thin films shows about an 11% reduction from its 300 K value; however, it is reduced by about 87% reduction from its 200 K value when the temperature drops from 200 to 100 K. with a decrease to 200 K, the polarization fatigue was significant, and the capacitor shows an approximate 29% reduction in polarization from its initial value following …

Development Of Water-Based Ink System For Braille Printing, Saurabh Varma

Masters Theses

The most commonly used system of writing by and for blind persons is called Braille, named after its French inventor, Louis Braille (1809-1952). Braille is comprised of a rectangular six-dot cell on its end, with up to 63 possible combinations using one or more of the six dots. Braille is the only reliable method of literacy for blind persons, because it enables them to read and write by touch¹.

Currently, Braille is printed by special embossers that serve as a printing press. These embossers create Braille output when it is attached appropriately to computers. The speed of these …

Investigation Of The Corrosion Of Steel By Lead-Bismuth Eutectic (Lbe) Using Scanning Electron Microscopy And X-Ray Photoelectron Spectroscopy, Daniel Koury

UNLV Theses, Dissertations, Professional Papers, and Capstones

Lead Bismuth Eutectic (LBE) has been proposed for use in programs for accelerator transmutation of waste. LBE is the leading candidate material as a spallation target and an option for the sub-critical blanket coolant. The corrosion of 316 and 316L stainless steels by LBE has been studied using UNLV's facilities for Scanning Electron Microscopy (SEM) and X-ray Photoelectron Spectroscopy (XPS). We have compared exposed and unexposed samples and studied the differences. Some amount of surface contamination is present on the samples and has been removed by ionbeam etching. The unexposed samples reveal typical stainless steel characteristics: a chromium oxide passivation …

A Simple Method For Indexing Powder Diffraction Patterns Of Cubic Materials:(1) Using The Θ-Values Of Reference, Me Kamwaya

Tanzania Journal of Science

From the values of sin2θ taken from powder photographs of the cubic crystal system, a variable constant, K, which is a multiple of (h2 + k2 + l2) can be determined. The smallest value of sin2θ1 gives rise to a multiple of one, two, or three which corresponds to the smallest value of Σhl2 for the primitive, bcc and fcc crystals, respectively. The old assumption that when indexing, the occurrence of numbers of the form (h2 + k2 + l2) = 8n + 7, where n = 0.1.2.3… should cause each of (h2 + k2 + l2) to be multiplied …

Mechanistic Study Of Oxidation Of Hypophosphite On Pt Electrodes By Sniftirs, Tai-Xiang Jiang, Hui-Huang Wu

Journal of Electrochemistry

The oxidation of hypophosphite on a polycrystalline platinum electrode was studied by SNIFTIRS and cyclic voltammetry, the in-situ IR spectra were analyzed as a function of Pt electrode potentials in the solution of 0.5 mol/L H₂SO₄+0.1 mol/L NaH₂PO₂. It was found that the dissociative adsorption of hypophosphite ions occurs on Pt surface, and the oxidation product is H₃PO₄, rather than H₂PO₃^- which was considered to produce on Ni electrodes, thereby a new insight into mechanism of hypophosphite oxidation on Pt in acidic media was …

Preparation And Electrochemical Lithium Intercalation Performance Of Different Shaped Carbon Nanotube, Mao-Hui Chen, Zhen-Cai Huang, Guo-Tao Wu, Jin-Kua You, Zu-Geng Lin

Journal of Electrochemistry

In the present work, different shaped carbon nanotubes were produced by the general CVD and the template method at different temperature (600 ℃,700 ℃) with the reaction gas of acetylene. The morphology, structure and the electrochemical lithium intercalation performance were comparatively studied and characterized by TEM, HRTEM, SEM, XRD, Raman techniques and Charge/Discharge Test. It was found that the different preparation methods and temperatures all had an obvious effect on these properties of carbon nanotubes. In our samples, with the increase of preparation temperature, the degree of crystallinity decreased, and the reversible specific capacity increased respectively.

Improvement Of The Low Temperature Electrochemical Performance Of Ab5-Type Hydrogen Storage Alloy, Hui Ye, Zhu Wu, Zhi-Lin Li, Hong Zhang

Journal of Electrochemistry

Optimizing the rare earth composition and doping with boron have been used to improve the low temperature performance of AB₅ hydrogen storage alloy. The results show that Ce-rich alloy with a proper amount of boron is suitable for Ni/MH battery with the lower-limit temperature down to 238 K under smaller current density (≤120 mA/g). The improvement of low temperature performance of hydrogen storage alloy is well consistent with its microstructure, thermodynamic and kinetic properties.

Nano-Sized Cobalt-Based Oxides As Negative Electrode For Lithium-Ion Batteries, Feng Huang, Zheng-Yong Yuan, Yun-Hong Zhou, Ju-Tang Sun

Journal of Electrochemistry

Nanosized cobalt-based oxide (Co₃O₄, CoB_1.36O_2.8 and CoB_0.5Al_0.1O_1.5) samples were prepared by rheological phase method and were tested as anodes in secondary lithium batteries. The cells were cycled between 0.01V and 3.00 V. The best electrochemical performance was obtained from the Co₃O₄ cell, which retained 95% of its initial capacity (931 mAh/g) after 30 cycles. The doping of B, Al reduced the reversible capacity during the first discharge/charge cycle, and the quantity of reversible capacity reduced with B, Al increasing. The modifying structures at difference …

Lithium Intercalation Performance Of P-Doped Phenolic Resin Pyrolysis Carbon, Bao-Hua Li, Kai-Xi Li, Yonggen Lv, Chun-Xiang Lv, Dong Wu, Li-Cheng Ling

Journal of Electrochemistry

Phosphorus-doped phenolic resin carbon was prepared by low temperature (700 ℃) pyrolysis of thermoplastic phenolic resin containing different amounts of phosphorus pentoxide after curing. X-ray diffraction pattern and the constang-current charge-discharge properties of phenolic resin carbon were studied. The results showed that the phenolic resin carbon microstructure became out of order with increasing of content phosphorus pentoxide, otherwise, the first discharge reversible capacities increased firstly and then decreased. The first discharge reversible capacity of phenolic resin carbon containing 9wt% phosphorus pentoxide was 528 mA·h·g^-1 which was higher than that of non-phosphorus doped phenolic resin carbon(230 mA·h·g^-1) did.

Studies On The Inhibition Of Yki-05 Corrosion Inhibitor To 907a Steel In Different Immersed Environments, Hui Yu, Jian-Hua Wu, Hong-Ren Wang, Jian-Hua Qian, Guang-Zhang Chen

Journal of Electrochemistry

The inhibition of YKI-05 Corrosion inhibitor in different conditions was studied using potentiodynamic polarization technique. The resuled shown that (i) the inhibitor film layer was formed stably on the surface of 907A steel electrode when it was persistently immersed in static seawater and the inhibition efficiency reached 90% or so. The inhibition mechanism is negative catalytic effect. (ii) the inhibitior film layer was not stable when the electrode was periodically immersed in seawater and was destroyed more significantly with the increase of electrode exposing time. The film was only a covered layer on the surface of electrode and it retarded …

Steady State Simulation Of Ysz Intermediate-Temperature Fuel Cell, Zi-Jing Lin, Ye Gu, Xiao-Hua Zhang

Journal of Electrochemistry

With a coupled 2D electrochemical and thermal modeling software, the characteristics of the steady state operation of the intermediate-temperature fuel cell with thin yttria-stabilized zirconia(YSZ) electrolyte was analyzed. The parameters of I-V equation were obtained from fitting the experiment results and the choice of grid points was determined by balancing the accuracy requirement and computational efficiency. The temperature fields at different operation circumstances such as flow designs, material choices for interconnect, were examined. The dependences of the output power and cell efficiency on the operating voltage at different temperatures were studied. Based upon the analysis of the temperature profile, it …

Preparation And Performance Of Lifeo2 Coated Nickel Oxide Cathode For Molten Carbonate Fuel Cells, Chun-Ming Wang, Fei Li, Ke-Ao Hu

Journal of Electrochemistry

A novel cathode for molten carbonate fuel cells was prepared by coating LiFeO₂ over the surface of porous NiO cathode by a simple combustion process. The analytical results of X-ray diffraction (XRD), energy dispersive analysis of X-ray (EDAX), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) indicated that the LiFeO₂ coating on the surface of NiO particles consisted of nonometer-sized LiFeO₂ grains and sintered tightly with the NiO particles. The LiFeO₂ coating dramatically reduced the contacting area of NiO with the carbonate melts, thus the solubility of NiO in the carbonate melts was decreased. Meanwhile, …

Review Of Mathematical Model For Proton Exchange Membrane Fuel Cell, Shan-Hai Ge, Bao-Lian Yi, Hua-Min Zhang

Journal of Electrochemistry

In the review with 49 references, the mathematical models for proton exchange membrane fuel cell (PEMFC) were summarized. The mechanistic model and empirical model were introduced. Transfer in the membrane, catalyst layer, diffusion layer and flow field of PEMFC were described. The importance of water and heat management was analyzed. The dimension, complexity and solving methods of the PEMFC model were discussed. The importance and validity to develop a model with time dimension are put forward.

Properties Of Domestic Natural Graphite Used For Li-Ion Batteries, Cui-Wei Du, Yu-Juan Zhao, Gang Zhang, Yin-Shun Wu, Qing-Guo Liu

Journal of Electrochemistry

The structure, physical characteristics and electrochemical properties of the natural graphite produced in Shandong province have been studied. The result of X-ray diffraction showed that the graphite consisted of hexagonal structure and rhombic structure (30% rhombic structure). It was fine crystal graphite. Used as a negative material of Lithium ion battery, the natural graphite showed excellent voltage and high energy capacity, but poor compatibility with electrolyte solution containing propylene carbonate (PC) for its own structure limitation.

Effect Of Dissolved Oxygen On The Corrosion Behavior Of Coalesced Copper And Stainless Steel-206 In Acetic Solutions, Rong-Zong Hu, Xiong-Cao Zhao, Yu-Hua Weng, Chang-Jian Lin

Journal of Electrochemistry

Linear sweeping technique and dissolving oxygen sensor were used to study the effect of dissolved oxygen and relating factors on the corrosion behavior of coalesced copper and stainless steel-206 in acetic solutions. It was found: 1. The existing of dissolved oxygen is one of the important factors, which strongly influenced the corrosion behavior of coalesced copper and stainless steel-206 in acetic solution. 2. The existing of dissolved oxygen is benefitial to the preventing stainless steel-206 from corrosion in acetic solutions, but damage to the preventing coalesced copper from corrosion. 3. At the high temperature since the dissolved oxygen was escaping …

Electrocatalytic Oxidation Of Formic Acid On Molybdate-Modified Platinum Electrode, Jun-Hua Du, Xue-Hui Xu, Hong Li, Hong-Yu Cheng, Wei-Shan Li

Journal of Electrochemistry

The electrochemical behavior of molybdates on a platinum electrode in H₂SO₄ solutions with different H₂SO₄ concentrations was studied by cyclic voltammetry and double chronoamperometry. Molybdates were reduced to adsorb hydrogen molybdenum bronzes on the platinum electrode in H₂SO₄ solutions during cathodically potential sweep. The hydrogen molybdenum bronzes were oxidized to different forms of hydrogen molybdenum bronzes with less hydrogen, depending on the H₂SO₄ concentration. Platinum electrode was modified by these hydrogen molybdenum bronzes. However, this modified electrode was not stable in H₂SO₄ solutions. The modified …

Manufacture Of 1 Kw Molten Carbonate Fuel Cell Stack, Sheng Sui, Xin-Jian Zhu, Zheng-Yu Fan, Guang-Yi Cao

Journal of Electrochemistry

A molten carbonate fuel cell stack with an active area of 240 mm×140 mm consisted of 30 cells. The gas feed system works via interior manifolds, and the stack placed in a couple of self-chest, coupled with a heater at the bottom and other fours surrounded,to keep uniformity of temperature.Under ambient pressure and 650 ℃, fed with hydrogen and air as anode and cathode gases respectively, the stack gave a current density of 150 mA/cm² at an average cell voltage of 0.7 V. The peak output of the stack was 1.06 kW during its performance of 300 h.

Coarsening Dynamics Of Biaxial Nematic Liquid Crystals, Nikolai V. Priezjev, Robert A. Pelcovits

Mechanical and Materials Engineering Faculty Publications

We study the coarsening dynamics of two- and three-dimensional biaxial nematic liquid crystals, using Langevin dynamics. Unlike previous work, we use a model with no a priori relationship among the three elastic constants associated with director deformations. Biaxial nematics possess four topologically distinct classes of defects, three of which have half-integer charge, while the fourth, which plays a minor role in coarsening, is of integer charge. We find a rich variety of coarsening behavior, including the presence of one, two, or three of the half-integer classes at late times, depending on the relative values of the elastic constants and the …

Student Perceptions Of Institutional And Instructor Based Techniques For Dealing With Academic Dishonesty, Donald D. Carpenter, Trevor S. Harding, Susan M. Montgomery, Nicholas H. Steneck, Eric Dey

Materials Engineering

Research suggests that a large percentage of engineering students engage in some form of academic dishonesty. To investigate this very serious concern, the authors have undertaken a research project on the Perceptions and Attitudes toward Cheating among Engineering Students (PACES). The premise of this research is that a combination of pressures, rather than malicious motivations, account for most student cheating. This paper focuses on a portion of the PACES survey; student opinions on what actions might prevent cheating. The authors examined data collected from approximately 350 engineering and pre-engineering undergraduate students at 5 institutions. In the survey, the students were …