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Full-Text Articles in Engineering

Feasibility Of Using Ultra-High-Performance Concrete (Uhpc) As A Repair Material Durability Performance, Rebar Coating, And Bond Characterization, Haitham Hussein Aug 2022

Feasibility Of Using Ultra-High-Performance Concrete (Uhpc) As A Repair Material Durability Performance, Rebar Coating, And Bond Characterization, Haitham Hussein

All Dissertations

Ultra-High Performance Concrete can be a very good material for use in repair works. The ability of chloride ions to pass through repaired concrete layers is suppressed if an impermeable concrete like UHPC is used. However, thickness of the UHPC layer and the orientation of the repair layer relative to the direction of chloride ingress may influence its effectiveness. This study is an attempt to evaluate the effect of varying thicknesses and cross sections areas of UHPC over a precast concrete and the direction of the UHPC layers relative to the direction of chloride ion movement on the resistance offered …


Development Of Ultra High Performance Composite Impact Panels Using Emaa, Jeffrey Hollstein Aug 2022

Development Of Ultra High Performance Composite Impact Panels Using Emaa, Jeffrey Hollstein

Electronic Theses and Dissertations

UHPC with the addition of fibers is recognized for its increased impact resistance compared to typical strength concrete. To further increase the resilience, recent studies have been conducted to reinforce the UHPC with CFRTP on the front and rear face to create sandwich panels. These studies used PETg/E-glass CFRTP bonded to the UHPC using EMAA (Surlyn) in a stamp thermoforming process. Impact tests conducted on these panels have shown that delamination has been the initial and detrimental failure to the sandwich composite. Increasing the composites resistance to debonding will increase the impact energy required to debond the composite. In this …


For The Improvement Of Mechanical And Microstructural Properties Of Uhpc With Fiber Alignment Using Carbon Nanotube And Graphite Nanoplatelet, Huanghuang Huang, Le Teng, Kamal Khayat, Xiaojian Gao, Fazhou Wang, Zhichao Liu May 2022

For The Improvement Of Mechanical And Microstructural Properties Of Uhpc With Fiber Alignment Using Carbon Nanotube And Graphite Nanoplatelet, Huanghuang Huang, Le Teng, Kamal Khayat, Xiaojian Gao, Fazhou Wang, Zhichao Liu

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

This paper investigates the influence of carbon nanotube (CNT) and graphite nanoplatelet (GNP) on the microstructure and mechanical characteristics of UHPC with steel fiber alignment. The content of CNT and GNP ranged from 0 to 0.3%, by mass of binder. Predominant fiber alignment was manipulated using a flow-induced casting method during UHPC placement. Experiment results indicated that the increase of CNT and GNP content from 0 to 0.3% led to 15%, 40%, and 50% improvement in compressive strength, flexural strength, and T150 (dissipated energy) of UHPC, respectively. Fiber alignment was shown to increase flexural strength and T150 by 30% and …


Use Of Saturated Lightweight Sand To Improve The Mechanical And Microstructural Properties Of Uhpc With Fiber Alignment, Huanghuang Huang, Le Teng, Xiaojian Gao, Kamal Khayat, Fazhou Wang, Zhichao Liu May 2022

Use Of Saturated Lightweight Sand To Improve The Mechanical And Microstructural Properties Of Uhpc With Fiber Alignment, Huanghuang Huang, Le Teng, Xiaojian Gao, Kamal Khayat, Fazhou Wang, Zhichao Liu

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

This paper studied the influence of pre-saturated lightweight sand (LWS) on the mechanical and microstructural properties of UHPC cast with steel fiber alignment. The changes in hydration kinetics, porosity, nano-mechanical, and mechanical properties were studied. The LWS was used at 0–50% replacement volumes of total sand. Predominant fiber alignment was favored through a flow-induced casting method during casting of flexural prisms. Experiment results showed that the 28-d autogenous shrinkage was decreased from 450 to 275 μm/m with the LWS content increasing from 0 to 50%. The addition of 20% LWS led to maximum increases of 15%, 15%, and 20% in …


Effect Of Carbon Nanotube And Graphite Nanoplatelet On Composition, Structure, And Nano-Mechanical Properties Of C-S-H In Uhpc, Huanghuang Huang, Le Teng, Xiaojian Gao, Kamal Khayat, Fazhou Wang, Zhichao Liu Apr 2022

Effect Of Carbon Nanotube And Graphite Nanoplatelet On Composition, Structure, And Nano-Mechanical Properties Of C-S-H In Uhpc, Huanghuang Huang, Le Teng, Xiaojian Gao, Kamal Khayat, Fazhou Wang, Zhichao Liu

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

This paper studied the influence of carbon nanotube (CNT) and graphite nanoplatelet (GNP) used at 0 to 0.3%, by mass of binder, on composition, structure, and nano-mechanical characteristics of C-S-H of ultra-high performance concrete (UHPC). Hydration kinetics, pore structure, and mechanical properties of UHPC were also investigated. The non-proprietary UHPC was proportioned with 17% lightweight sand for internal curing. Test results indicated that the addition of 0.3% CNT or GNP led to approximately 20 MPa increase in compressive strengths of non-fibrous UHPC mortar and fibrous UHPC (2% steel fibers), compared to those prepared without any nanomaterial. Such enhancement is attributed …


Simplified Analytical Model To Assess Key Factors Influenced By Fiber Alignment And Their Effect On Tensile Performance Of Uhpc, Le Teng, Huanghuang Huang, Kamal Khayat, Xiaojian Gao Mar 2022

Simplified Analytical Model To Assess Key Factors Influenced By Fiber Alignment And Their Effect On Tensile Performance Of Uhpc, Le Teng, Huanghuang Huang, Kamal Khayat, Xiaojian Gao

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

The increase in single-fiber pullout strength usually improves tensile strength and toughness of UHPC. An increase in fiber orientation angle (θ) up to 45° to the direction of pullout load was found to enhance the single-fiber pullout strength. However, such increase in predominant θ value along tensile strength specimens led to a reduction in tensile strength of UHPC. In order to elucidate this controversial observation, analytical models combined with experiments were carried out to assess the key factors influencing the tensile properties of UHPC due to variations of fiber orientation. The test parameters involved the evaluation of the effect of …


Tension-Stiffening Effect Consideration For Modeling Deflection Of Cracked Reinforced Uhpc Beams, Le Teng, Rongling Zhang, Kamal Khayat Jan 2022

Tension-Stiffening Effect Consideration For Modeling Deflection Of Cracked Reinforced Uhpc Beams, Le Teng, Rongling Zhang, Kamal Khayat

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

Tension-stiffening effects can significantly influence the flexural performance of cracked reinforced concrete specimens. Such effect is amplified for fiber-reinforced concrete, given the fact that fibers can bridge the cracks. The objective of this study was to develop a model to predict the deflection of cracked reinforced ultra-high performance concrete (R-UHPC) beam elements. The modeling approach characterized the average bending moment of inertia by combining the existing model used for conventional reinforced concrete and the analytical model of stress distribution of UHPC along the cross-section. The finite element analysis (FEA) was employed to evaluate the flexural deflection based on the average …


Field Implementation And Monitoring Of An Ultra-High Performance Concrete Bridge Deck Overlay, Craig Newtson, Brad Weldon, William Toledo, Andres Alvarez, Mark Manning Dec 2021

Field Implementation And Monitoring Of An Ultra-High Performance Concrete Bridge Deck Overlay, Craig Newtson, Brad Weldon, William Toledo, Andres Alvarez, Mark Manning

Data

This project focused on field implementation of an ultra-high performance concrete (UHPC) overlay during rehabilitation of an existing concrete bridge (No. 7032) deck in Socorro, New Mexico, USA. Bridge 7032 is a two-lane bridge that is approximately 300 ft. (91.4 m) long and 54 ft. (16.5 m) in width. Rehabilitation of bridge 7032 included removal of deteriorated concrete from the existing deck, installation of a high-performance deck (HPD) leveling course, and installation of a 1 in. (25 mm) UHPC overlay. An UHPC mixture with a 19.5 ksi (134 MPa) compressive strength developed in previous research was selected for this project. …


Field Implementation And Monitoring Of An Ultra-High Performance Concrete Bridge Deck Overlay, Craig Newtson, Brad Weldon, William Toledo, Andres Alvarez, Mark Manning Dec 2021

Field Implementation And Monitoring Of An Ultra-High Performance Concrete Bridge Deck Overlay, Craig Newtson, Brad Weldon, William Toledo, Andres Alvarez, Mark Manning

Publications

This project focused on field implementation of an ultra-high performance concrete (UHPC) overlay during rehabilitation of an existing concrete bridge (No. 7032) deck in Socorro, New Mexico, USA. Bridge 7032 is a two-lane bridge that is approximately 300 ft. (91.4 m) long and 54 ft. (16.5 m) in width. Rehabilitation of bridge 7032 included removal of deteriorated concrete from the existing deck, installation of a high-performance deck (HPD) leveling course, and installation of a 1 in. (25 mm) UHPC overlay. An UHPC mixture with a 19.5 ksi (134 MPa) compressive strength developed in previous research was selected for this project. …


Development Of Novel Ultra-High Performance Engineered Cementitious Composites (Uhp-Ecc) For Durable And Resilient Transportation Infrastructure, Gabriel A. Arce, Marwa Hassan, Daniel E. Game Sep 2021

Development Of Novel Ultra-High Performance Engineered Cementitious Composites (Uhp-Ecc) For Durable And Resilient Transportation Infrastructure, Gabriel A. Arce, Marwa Hassan, Daniel E. Game

Data

The objective of this study was to develop novel UHP-ECC materials utilizing readily available ingredients in Region 6 for the construction and repair of transportation infrastructure. Phase one of this study focused on the development of ultra-high strength cementitious matrices by evaluating the effects of ingredient selection and mixture proportioning on the materials’ compressive strength. Variables evaluated included the mass ratios of silica fume to fly ash (SF/FA), supplementary cementitious materials to cement (SCMs/C), and ordinary sand to microsilica sand (OS/MS). Phase two of the study focused on the development of UHP-ECC materials. To this end, based on the knowledge …


Development Of Novel Ultra-High Performance Engineered Cementitious Composites (Uhp-Ecc) For Durable And Resilient Transportation Infrastructure, Gabriel A. Arce, Marwa Hassan, Daniel E. Game Sep 2021

Development Of Novel Ultra-High Performance Engineered Cementitious Composites (Uhp-Ecc) For Durable And Resilient Transportation Infrastructure, Gabriel A. Arce, Marwa Hassan, Daniel E. Game

Publications

The objective of this study was to develop novel UHP-ECC materials utilizing readily available ingredients in Region 6 for the construction and repair of transportation infrastructure. Phase one of this study focused on the development of ultra-high strength cementitious matrices by evaluating the effects of ingredient selection and mixture proportioning on the materials’ compressive strength. Variables evaluated included the mass ratios of silica fume to fly ash (SF/FA), supplementary cementitious materials to cement (SCMs/C), and ordinary sand to microsilica sand (OS/MS). Phase two of the study focused on the development of UHP-ECC materials. To this end, based on the knowledge …


Development Of Hybrid Ultra-High Performance Concrete Thermoplastic Composite Panels For Blast And Ballistic Protection, Alyssa M. Libby May 2021

Development Of Hybrid Ultra-High Performance Concrete Thermoplastic Composite Panels For Blast And Ballistic Protection, Alyssa M. Libby

Electronic Theses and Dissertations

In recent years, ultra-high performance concrete (UHPC) has become a material of interest for structures needing resistance to impact and blast loadings. These types of loadings have induced brittle flexural failure in UHPC due to punching shear from the impactor. One way to improve the impact resistance, energy absorption, and ductility of UHPC is by adding fiber-reinforced polymer (FRP) skins to the front and rear faces of the concrete, resulting in a sandwich configuration. In this study, E-glass fiber-reinforced thermoplastic laminates were bonded to UHPC panels using a heated consolidation process known as stamp thermoforming. The bond between the UHPC …


Ultra-High Performance Concrete (Uhpc) Deck-To-Girder Connection For Accelerated Bridge Construction, Mostafa Abo El-Khier Apr 2021

Ultra-High Performance Concrete (Uhpc) Deck-To-Girder Connection For Accelerated Bridge Construction, Mostafa Abo El-Khier

Department of Construction Engineering and Management: Dissertations, Theses, and Student Research

Precast concrete deck systems have been successfully used for Accelerated Bridge Construction. In most systems, special deck-to-girder connections are designed to achieve structurally composite sections. These connections require tight production/erection tolerances that complicate deck and girder fabrication and compromise the economics of these systems. This study presents a new precast concrete deck-to-girder connection that takes advantage of the excellent mechanical, workability, and durability properties of ultra-high performance concrete (UHPC) to simplify precast concrete deck and girder fabrication and erection. Typical girder shear reinforcement is terminated below the soffit of deck panels to eliminate any conflicts with deck reinforcement and relax …


Use Of Uhpc Stay-In-Place Shells In Bridge Column Construction For Accelerated Bridge Construction, Nerma Caluk Mar 2020

Use Of Uhpc Stay-In-Place Shells In Bridge Column Construction For Accelerated Bridge Construction, Nerma Caluk

FIU Electronic Theses and Dissertations

This research utilizes Ultra-High Performance Concrete (UHPC), durable material that can be used to construct unique structural elements, to construct prefabricated shells that act as stay-in-place forms for circular bridge columns. These innovative structural elements are intended to (1) eliminate conventional formworks, (2) reduce the on-site construction time, (3) reduce life cycle costs by providing maintenance-free columns, and (4) improve the structural performance of bridge columns. The UHPC shell is placed around the column reinforcement that has been assembled using conventional methods, after which a UHPC step portion is cast at the column-to-footing interface to connect the UHPC shell with …


Precast Concrete Deck-To-Girder Connection Using Uhpc, George Morcous, Mostafa Abo El-Khier Dec 2019

Precast Concrete Deck-To-Girder Connection Using Uhpc, George Morcous, Mostafa Abo El-Khier

Nebraska Department of Transportation: Research Reports

The implementation of ultra-high-performance concrete (UHPC) in bridge construction has been growing rapidly in the last two decades due to its excellent mechanical properties, workability, and durability. This report presents a new UHPC connection between precast concrete deck panels and bridge girders that eliminates changes to the design and production of girder shear connectors commonly used in conventional cast-in-place concrete deck construction. In conventional construction, girder shear reinforcement or studs are extended into the cast-in-place concrete deck to transfer interface shear and create composite section. In the new connection, girder shear reinforcement or studs are kept underneath the deck panels, …


Uhpc Shear Keys In Concrete Bridge Superstructures, Craig Newtson, Brad Weldon, Elsy Flores, Jordan Varbel, William Toledo Aug 2019

Uhpc Shear Keys In Concrete Bridge Superstructures, Craig Newtson, Brad Weldon, Elsy Flores, Jordan Varbel, William Toledo

Data

Corresponding data set for Tran-SET Project No. 18CNMS01. Abstract of the final report is stated below for reference:

"This research investigated the use of locally produced ultra-high performance concrete (UHPC) as a grouting material to repair deteriorated shear keys. Shear keys are used in adjacent girder superstructures to produce monolithic behavior and load transfer across the structure. Shear key durability is a concern since shear key degradation can jeopardize the integrity of the structure. Transportation agencies have reported that 75% of distress in adjacent girder bridges is due to cracking and de-bonding along shear keys. Previous research has shown that …


Workforce Development Symposiums For Uhpc, Brad Weldon, Craig Newtson, Grace Mcmurry, Leticia Davila Aug 2019

Workforce Development Symposiums For Uhpc, Brad Weldon, Craig Newtson, Grace Mcmurry, Leticia Davila

Data

Corresponding data set for Tran-SET Project No. 18TTNMS02. Abstract of the final report is stated below for reference:

"Ultra-high performance concrete (UHPC) is a cementitious material with a dense microstructure that contributes to high compressive strengths as well as enhanced durability properties. UHPC also possesses significant post-cracking strength and ductility due to the addition of fibers. These characteristics produce a material that provides advantages over conventional concrete; however, high costs attributed to materials and production, lack of industry familiarity and knowledge, and the absence of standardized design procedures have impeded its widespread use. To help disseminate knowledge on UHPC, two …


Uhpc Shear Keys In Concrete Bridge Superstructures, Craig Newtson, Brad Weldon, Elsy Flores, Jordan Varbel, William Toledo Aug 2019

Uhpc Shear Keys In Concrete Bridge Superstructures, Craig Newtson, Brad Weldon, Elsy Flores, Jordan Varbel, William Toledo

Publications

This research investigated the use of locally produced ultra-high performance concrete (UHPC) as a grouting material to repair deteriorated shear keys. Shear keys are used in adjacent girder superstructures to produce monolithic behavior and load transfer across the structure. Shear key durability is a concern since shear key degradation can jeopardize the integrity of the structure. Transportation agencies have reported that 75% of distress in adjacent girder bridges is due to cracking and de-bonding along shear keys. Previous research has shown that locally produced UHPC has excellent mechanical and durability properties. UHPC has also been shown to have good bonding …


Workforce Development Symposiums For Uhpc, Brad Weldon, Craig Newtson, Grace Mcmurry, Leticia Davila Aug 2019

Workforce Development Symposiums For Uhpc, Brad Weldon, Craig Newtson, Grace Mcmurry, Leticia Davila

Publications

Ultra-high performance concrete (UHPC) is a cementitious material with a dense microstructure that contributes to high compressive strengths as well as enhanced durability properties. UHPC also possesses significant post-cracking strength and ductility due to the addition of fibers. These characteristics produce a material that provides advantages over conventional concrete; however, high costs attributed to materials and production, lack of industry familiarity and knowledge, and the absence of standardized design procedures have impeded its widespread use. To help disseminate knowledge on UHPC, two workforce development symposiums on UHPC were held in Las Cruces, New Mexico. The symposiums consisted of presentations and …


Retrofitting Of Bridge Elements Subjected To Predominantly Axial Load Using Uhpc Shell, Mahsa Farzad Apr 2019

Retrofitting Of Bridge Elements Subjected To Predominantly Axial Load Using Uhpc Shell, Mahsa Farzad

FIU Electronic Theses and Dissertations

In the United States, ~30% of the ~600,000 highway bridges are categorized as structurally deficient or functionally obsolete. These bridges should be replaced or upgraded to sustain the transportation needs of the growing public and private sectors of the U.S. economy. It is not uncommon for structures to have advanced levels of corrosion-induced damage where major repair and maintenance works are required. However, the transportation infrastructure may undergo disruption during rehabilitation causing interruption to critical economic public, civil and commercial activities. This mandates the development of new techniques and materials for accelerated rehabilitation and resilience. To address this issue, a …


Bridge Deck Overlays Using Ultra-High Performance Concrete, Craig Newtson, Brad Weldon Dec 2018

Bridge Deck Overlays Using Ultra-High Performance Concrete, Craig Newtson, Brad Weldon

Data

Corresponding data set for Tran-SET Project No. 17CNMS01. Abstract of the final report is stated below for reference:

"This study investigated the use of a locally produced ultra-high performance concrete (UHPC) as an alternative to typical overlay materials. Several bond strength tests including slant-shear, splitting tension, and direct tension tests were performed to assess the bond strength between UHPC and normal strength concrete (NSC) substrate with varying surface textures. Tests were also conducted to assess the early-age and longer-term shrinkage behavior and coefficient of thermal expansion of the UHPC as well as rapid chloride permeability testing. Good bond between UHPC …


New Connection Details To Connect Precast Cap Beams To Precast Columns Using Ultra High Performance Concrete (Uhpc) For Seismic And Non-Seismic Regions, Mohamadreza Shafieifar Oct 2018

New Connection Details To Connect Precast Cap Beams To Precast Columns Using Ultra High Performance Concrete (Uhpc) For Seismic And Non-Seismic Regions, Mohamadreza Shafieifar

FIU Electronic Theses and Dissertations

Several connection details have been developed for the connection of precast cap beams to precast columns in Accelerated Bridge Construction (ABC) applications. Currently, the suggested details involve some form of either reinforcement or portion of the precast column to penetrate inside the cap beam. Such details present many challenges in the field, such as necessitating bundling of reinforcement in the cap beam or creating a congested reinforcement arrangement. Furthermore, closer inspection of some of the test data indicates that for currently used details, cap beams could sustain some damages during major seismic events, whereas they are designed to be capacity …


Evaluation Of Ultra-High Performance Concrete (Uhpc) In Joints Of Bridge Girders, Saipavan Rallabhandhi Jan 2016

Evaluation Of Ultra-High Performance Concrete (Uhpc) In Joints Of Bridge Girders, Saipavan Rallabhandhi

Masters Theses

"Joints are often considered as the weak link in a structure and often deterioration of the structure initiates from the joints. Joints transfer the stresses from super-structure to sub-structure and in this process are subjected to large transfer stresses. Not much attention is given to the design of joints as they are positioned in low moment regions and typically a 4 to 6 ksi (28 to 41 MPa) concrete is used to fill the joints. One of the solution to this problem is Ultra-high performance concrete (UHPC). In the recent past significant research has been done to use UHPC in …


Proportioning And Properties Of Ultra-High Performance Concrete Mixtures For Application In Shear Keys Of Precast Concrete Bridges, Zhengqi Li Dec 2015

Proportioning And Properties Of Ultra-High Performance Concrete Mixtures For Application In Shear Keys Of Precast Concrete Bridges, Zhengqi Li

All Dissertations

Ultra-high performance concrete (UHPC) is defined as a cementitious based composite material with compressive strengths above 150 MPa, pre-and post-cracking tensile strengths above 5 MPa, and enhanced durability. To achieve desired properties, UHPC is typically produced with low water-cementitious materials (w/cm) ratio (i.e. w/cm < 0.25), high cementitious materials content (i.e. >1000 kg/m3), high quality aggregate, high dosage of high-range water reducing admixture (HRWRA) and reinforcing fibers. UHPC has distinct advantages in applications where narrow formwork and dense reinforcement are inevitable, high compressive strength concrete material is required and the surrounding environment is aggressive. The construction of shear keys in precast bridges is one of the important …


Material Characterization Of Ultra-High Performance Fiber Reinforced Concrete At Elevated Temperatures, Richard T. Way Feb 2013

Material Characterization Of Ultra-High Performance Fiber Reinforced Concrete At Elevated Temperatures, Richard T. Way

Master's Theses

With the recent development of Ultra High Performance Fiber Reinforced Concrete (UHPFRC), there has been limited investigation into the mechanical and material properties of this composite at elevated temperatures. At elevated temperatures concrete is shown to undergo several material changes which affect the residual mechanical properties. Additionally, fast heating rates are known to cause a phenomenon called explosive spalling. This research investigates the effect of high temperature on the residual mechanical properties and chemical degradation of two types of UHPFRC. This was accomplished by casting and testing two different UHPFRC mixes and exposing them to elevated temperatures at two rates …


Determing The Effect Of Thermal Treatment Timing On Ultra-High Performance Concrete Beams, Christopher H. Mullen Jan 2013

Determing The Effect Of Thermal Treatment Timing On Ultra-High Performance Concrete Beams, Christopher H. Mullen

Dissertations, Master's Theses and Master's Reports - Open

The loss of prestressing force over time influences the long-term deflection of the prestressed concrete element. Prestress losses are inherently complex due to the interaction of concrete creep, concrete shrinkage, and steel relaxation. Implementing advanced materials such as ultra-high performance concrete (UHPC) further complicates the estimation of prestress losses because of the changes in material models dependent on curing regime.

Past research shows compressive creep is "locked in" when UHPC cylinders are subjected to thermal treatment before being loaded in compression. However, the current precasting manufacturing process would typically load the element (through prestressing strand release from the prestressing bed) …


Preliminary Investigation Of Ultra-High Performance Concrete Behavior At High Strain Rates Using The Split-Hopkinson Pressure Bar, Jacob Clark Jan 2013

Preliminary Investigation Of Ultra-High Performance Concrete Behavior At High Strain Rates Using The Split-Hopkinson Pressure Bar, Jacob Clark

Dissertations, Master's Theses and Master's Reports - Open

Ultra-high performance concrete (UHPC) displays several enhanced material properties compared to normal strength concrete (NSC). In past research, Split-Hopkinson pressure bar (SHPB) tests have been used for normal strength concrete to determine material behavior at high strain rates. The behavior of advanced concrete materials, such as UHPC, under high strain rates has not been thoroughly investigated. While it is generally accepted that concrete materials experience increases in compressive strength under increasing strain rates, a preliminary investigation was conducted to gain insight into the compressive behavior of UHPC under high strain rate SHPB testing.

In this research, 50 specimens were tested …