Engineering Commons^™

Microwave Hyperthermia Application With Bioimplant Single Slot Coaxial Antennadesign For Mouse Breast Cancer Treatment, Ahmet Ri̇fat Görgün, Cem Baytöre, Selçuk Çömlekçi̇, Mehmet İbrahi̇m Tuğlu, Adnan Kaya

Turkish Journal of Electrical Engineering and Computer Sciences

In this study, a novel animal model for the breast cancer treatment which contains hyperthermia is proposed. For this main purpose a low cost, interstitial, bioimplant antenna by short ended single slot design is proposed to heat the cancerous tissues. Both the theoretical background of the proposed system and the simulation and measurement results of antenna design are presented. An artificial tissue phantom model has been created under laboratory conditions and then the utility of the proposed antenna has been tested on this model. Artificial tissues have been heated by 25W to (41-44 ? C) in a short time like …

Development Of Novel Membranes For Nanocarbon Enhanced Separation With Application In Biofuels And Solvent Recover, Oindrila Gupta

Dissertations

Pharmaceutical industries historically have had one of the highest amounts of solvent waste generated per unit of drug manufactured. Energy requirements and carbon footprint of current solvent recycling processes tend to be quite high, and the incineration of the solvents for waste disposal produces toxic air emissions. Also, rapidly increasing demand for energy and strict regulation on engine pollutant emissions have necessitated the use of alcohol as carbon-neutral fuels. Thermal distillation is one of the most common methods for the separation of alcohol-water mixtures. However, its application is limited due to energy requirements and high operating costs, and heating to …

Microwave Self-Healing Technology As Airfield Porous Asphalt Friction Course Repair And Maintenance System, Amir Tabakovic, Declan O'Prey, Drew Mckenna, David Woodward

Articles

A problem increasingly faced by airport authorities is the maintenance of runways. Due to their large aircraft loadings associated with take-off and landing operations, runways experience surface deterioration. Poor quality runway surfaces cannot be tolerated in such an environment. Maintenance issues must be carried out to maximise safety and minimise the risk of aircraft damage. A recent development has been the introduction of self-healing technologies such as rejuvenator encapsulation, induction and microwave heating to address these issues. This paper summarises a laboratory investigation to determine the effectiveness of microwave self-healing for crack repair of Porous Friction Course (PFC) used for …

Design Optimization Using Dielectric Slab For Efficient Microwave Heating, Sofiya Ali Mekonnen, Si̇bel Yeni̇kaya

Turkish Journal of Electrical Engineering and Computer Sciences

In this paper, usage of a dielectric slab on the top and bottom sides, on the top side, and on the bottom side of a clay sample was presented as a means of improving heating efficiency in multimode applicator. In order to accomplish the optimization procedure, we used four different dielectric slab types having different thickness values. The simulated results show that by using additional dielectric slab it is possible to increase the electric field intensity inside the applicator and obtain higher power absorption rates within the sample and high-efficiency designs.

Microwave-Assisted Synthesis Of Palladium Nanoparticles Supported On Copper Oxide In Aqueous Medium As An Efficient Catalyst For Suzuki Cross-Coupling Reaction, Hany A. Elazab, M. A. Sadek, Tamer T. El-Idreesy

Chemical and Biochemical Engineering Faculty Research & Creative Works

We report here a reliable green method for the synthesis of palladium nanoparticles supported on copper oxide as a highly active and efficient catalyst for Suzuki cross-coupling reaction. The experimental synthetic approach is based on microwave-assisted chemical reduction of an aqueous mixture of palladium and copper salt simultaneously using hydrazine hydrate as reducing agent. The catalyst was fully characterized using various techniques showing well-dispersed palladium nanoparticles. The catalytic activity and recyclability of the prepared catalyst were experimentally explored in the ligand-free Suzuki cross-coupling reaction with a diverse series of functionalized substrates. The synthesized Pd/CuO catalyst shows many advantages beside its …

Microwave-Assisted Synthesis Of Palladium Nanoparticles Supported On Copper Oxide In Aqueous Medium As An Efficient Catalyst For Suzuki Cross-Coupling Reaction, Hany A. Elazab, M. A. Sadek, Tamer T. El-Idreesy

Chemical Engineering

We report here a reliable green method for the synthesis of palladium nanoparticles supported on copper oxide as a highly active and efficient catalyst for Suzuki cross-coupling reaction. The experimental synthetic approach is based on microwave-assisted chemical reduction of an aqueous mixture of palladium and copper salt simultaneously using hydrazine hydrate as reducing agent. The catalyst was fully characterized using various techniques showing well-dispersed palladium nanoparticles. The catalytic activity and recyclability of the prepared catalyst were experimentally explored in the ligand-free Suzuki cross-coupling reaction with a diverse series of functionalized substrates. The synthesized Pd/CuO catalyst shows many advantages beside its …

Green Synthesis Of Copper Oxide Nanoparticles In Aqueous Medium As A Potential Efficient Catalyst For Catalysis Applications, Hany A. Elazab Dr

Chemical Engineering

In this research, we have developed a reliable green method for the synthesis of copper oxide nanoparticles as a potential efficient catalyst for several catalysis applications. In our experimental approach, microwave-assisted synthesis technique was used in order to perform chemical reduction of copper salt using hydrazine hydrate as a strong reducing agent. The prepared catalyst was characterized using various techniques showing the formation of well dispersed copper oxide nanoparticles. The synthesized Copper oxide catalyst shows many advantages including the use of environmentally benign solvent systems,

The Continuous Synthesis Of Pd Supported On Fe3o4 Nanoparticles: A Highly Effective And Magnetic Catalyst For Co Oxidation, Hany A. Elazab, Sherif Moussa, Kendra W. Brinkley, B. Frank Gupton, M. Samy El-Shall

Chemical and Biochemical Engineering Faculty Research & Creative Works

We report a facile approach used for the simultaneous reduction and synthesis of a well dispersed magnetically separable palladium nanoparticle supported on magnetite (Pd/Fe₃O₄ nanoparticles) via continuous flow synthesis under microwave irradiation conditions, using a Wave Craft's microwave flow reactor commercially known as Arrhenius One, which can act as a unique process for the synthesis of highly active catalysts for carbon monoxide (CO) oxidation catalysis. The prepared catalysts are magnetic, which is an advantage in the separation process of the catalyst from the reaction medium. The separation process is achieved by applying a strong external magnetic field …

The Effect Of Graphene On Catalytic Performance Of Palladium Nanoparticles Decorated With Fe3o4, Co3o4, And Ni (Oh)2: Potential Efficient Catalysts Used For Suzuki Cross—Coupling, Hany A. Elazab, Sherif Moussa, Ali R. Siamaki, B. Frank Gupton, M. Samy El-Shall

Chemical and Biochemical Engineering Faculty Research & Creative Works

Abstract: In this research, we report a scientific investigation of an efficient method used for the synthesis of highly active Palladium Nanoparticles decorated with Fe₃O₄, Co₃O₄, and Ni (OH)2 Supported on Graphene as Potential Efficient Catalysts for Suzuki Cross—Coupling. Pd/Fe₃O₄ nanoparticles supported on graphene nanosheets (Pd/Fe₃O₄/G) showed an excellent catalytic activity for Suzuki coupling reactions and recycled for up to four times without loss of catalytic activity. An efficient magnetic catalyst has been successfully synthesized using a simple, reproducible fast and reliable method using microwave …

The Effect Of Graphene On Catalytic Performance Of Palladium Nanoparticles Decorated With Fe3o4, Co3o4, And Ni (Oh)2: Potential Efficient Catalysts Used For Suzuki Cross—Coupling, Hany A. Elazab Dr

Chemical Engineering

In this research, we report a scientific investigation of an efficient method used for the synthesis of highly active Palladium Nanoparticles decorated with Fe3O4, Co3O4, and Ni (OH)2 Supported on Graphene as Potential Efficient Catalysts for Suzuki Cross—Coupling. Pd/Fe3O4 nanoparticles supported on graphene nanosheets (Pd/ Fe3O4/G) showed an excellent catalytic activity for Suzuki coupling reactions and recycled for up to four times without loss of catalytic activity. An efficient magnetic catalyst has been successfully synthesized using a simple, reproducible fast and reliable method using microwave irradiation conditions. The prepared catalysts are magnetic as in case of iron and cobalt oxides …

Green Synthesis Of Copper Oxide Nanoparticles In Aqueous Medium As A Potential Efficient Catalyst For Catalysis Applications, Waad Mohsen, M. A. Sadek, Hany A. Elazab

Chemical and Biochemical Engineering Faculty Research & Creative Works

In this research, we have developed a reliable green method for the synthesis of copper oxide nanoparticles as a potential efficient catalyst for several catalysis applications. In our experimental approach, microwave-assisted synthesis technique was used in order to perform chemical reduction of copper salt using hydrazine hydrate as a strong reducing agent. The prepared catalyst was characterized using various techniques showing the formation of well dispersed copper oxide nanoparticles. The synthesized Copper oxide catalyst shows many advantages including the use of environmentally benign solvent systems, green synthetic approach, and mild reaction conditions.

Behavior Of Metamaterial-Based Microwave Components For Sensing And Heating Of Nanoliter-Scale Volumes, Muhammed Sai̇d Boybay

Turkish Journal of Electrical Engineering and Computer Sciences

Metamaterial-based microwave components are among the state-of-the-art heater and sensor designs for microfluidic systems. The miniaturization and energy-focusing abilities of the metamaterial-based components make it possible to adopt microwave components operating at wavelengths in the order of 10 cm for microfluidic systems. Microwave systems are particularly advantageous for point-of-care and high-throughput applications due to their high speed of operation, very low instrumentation cost, ability to selectively and internally heat specimens, and ability of label-free sensing. In this study, the efficiency and behavior of microwave components designed for heating and sensing small volumes in the scale of nanoliters are studied. In …

Multiphysics Modeling To Enhance Understanding Of Microwave Heating Of Food In Domestic Ovens, Jiajia Chen

Department of Biological Systems Engineering: Dissertations and Theses

Nonuniform heating is the biggest issue in the microwave heating of prepared meals. Multiphysics based models are promising tools to improve microwave heating uniformity by properly designing the food product. However, limited availability of accurate temperature-dependent material properties, inadequate model prediction accuracy, and high computational power and complexity in model development are three gaps that greatly limited the application of these models in the food industry.

To fill in the gaps, firstly, we developed a multitemperature calibration protocol to measure temperature-dependent dielectric properties (dielectric constant and loss factor). The temperature-dependent dielectric and thermal (thermal conductivity and specific heat capacity) properties …

Effect Of Microwave Frequency On Dielectric Properties Of Oil Palm Shell (Ops) And Ops Char Synthesized By Microwave Pyrolysis Of Ops

Faculty of Engineering University of Malaya

Microwave heating is considered to be a potential, efficient and fast method for thermal treatment of biomass. Therefore, elemental understanding of dielectric properties of biomass is necessary before irradiating it with microwave radiations. Dielectric properties along with penetration depth, relaxation time and static permittivity of oil palm shell COPS) and OPS char were investigated in the frequency ranging between 0.5 and 20 GHz at room temperature. At low frequencies, dielectric constant of UPS was higher than that of UPS char while at higher frequencies, vice versa is observed. Penetration depth for UPS char was higher than that of UPS at …

Thermo-Catalytic Upgrading Of Pyrolysis Vapors Using Electromagnetic Heating, Pranjali Devidas Muley

LSU Doctoral Dissertations

Electromagnetic heating offers several advantages such as rapid heating rates, accurate temperature control and energy efficiency over conventional reactors. The goal of this study was to design an effective and energy efficient catalytic reactor for pyrolysis vapor upgrading. An induction based catalytic reactor was designed for upgrading of pyrolysis vapors. The effect of catalyst bed temperatures (290°, 330° and 370°C) and biomass to catalyst ratios of 1, 1.5 and 2 was studied. The results were compared to conventional heating reactor. Induction heating reactor performance exceeded that of conventional heater. The biomass to catalyst ratio of 2 in combination with the …

Composite Films With Magnetic Nanorods: Fundamentals, Processing And Applications, Yu Gu

All Dissertations

This Dissertation is centered on studying the composite films with magnetic nanorods. In recent years, one-dimensional magnetic nanostructures, such as magnetic nanorods, chains of magnetic nanoparticles, and nanotubes filled with magnetic nanoparticles have caught great attentions due to the breadth of applications. Their unique magnetic and geometrical features open new avenues of studies in medicine, sensors, optofluidics, magnetic swimming, and microrheology. In particular, they offered great opportunities for design of multifunctional devices and for manufacturing of anisotropic nano- and microstructures with unprecedented magnetic and mechanical properties. However, the strategy for nanorod alignment in both Newtonian and complex fluids has not …

Effect Of Microwave Heating On The Migration Of Additives From Ps, Pp And Pet Container Into Food Simulants, Ruoyin Cai

Theses

Microwave food packaging has become a tremendous element in the food manufacturing process. The purpose of any food packaging regulations concerned with the safety of the food is to control and limit the migration of substances from the packaging into the food. The main objective of this thesis is to test three different microwaving packaging materials that are the most common material in the market, viz. polystyrene (PS), polypropylene (PP), and polyethylene terephthalate (PET), migrated into four food simulant solutions. Four different simulant solutions were used based on the food type and FDA recommendations and regulations. These food simulants include …

Coupled Electromagnetic And Heat Transfer Model For Microwave Heating In Domestic Ovens, Krishnamoorthy Pitchai, Sohan Birla, Jeyamkondan Subbiah, D. D. Jones, Harshanardhan Thippareddi

Department of Food Science and Technology: Faculty Publications

Microwave ovens are used extensively for heating a variety of not-ready-to-eat food products. Non-uniform heating of foods in microwave ovens is a major concern in assuring microbiological safety of such products. The non-uniform heating of foods is attributed by complex interaction of microwaves with foods. To understand this complex interaction, a comprehensive model was developed to solve coupled electromagnetic and heat transfer equations using finite-difference time-domain based commercial software. The simulation parameters, cell size, heating time step, and number of iterations for steady state electromagnetic field were optimized. The model was validated by 30 s heating profile of a cylindrical …

Electromagnetic And Heat Transfer Modeling Of Microwave Heating In Domestic Ovens, Krishnamoorthy Pitchai

Department of Food Science and Technology: Dissertations, Theses, and Student Research

Microwave (MW) ovens are used extensively for heating a variety of not-ready-to-eat food products. It is vital to achieve target temperature uniformly throughout the food to inactivate foodborne pathogens to assure safety. Non-uniform heating of foods in microwave ovens is the major concern in assuring microbiological safety of such products. The non-uniform heating of foods in domestic microwave ovens is due to complex interactions of microwaves with foods. A comprehensive coupled electromagnetic and heat transfer model was developed using finite-difference time-domain based numerical method to understand the complex interaction of microwaves with foods. Simulation parameters such as cell size, heating …

Effect Of Magnetron Frequency On Heating Pattern In Domestic Oven, Sohan Birla, Krishnamoorthy Pitchai, Jeyamkondan Subbiah, David D. Jones

Department of Biological Systems Engineering: Conference Presentations and White Papers

In this study a computer model was developed to simulate microwave heating of a model food with a range of magnetron frequencies. The range was decided upon performing the frequency spectrum analysis of microwave leakage from the microwave oven. Simulation results showed that the magnetron input as sinusoidal frequency from 2.44 GHz to 2.48 GHz generates different heating profiles. The simulated heating profiles were compared with experimental heating profiles obtained by using an IR camera. None of simulations with individual frequency exactly matches with experimental temperature profile. The closet match between simulated and observed temperature profiles was found with 2.46 …

Development Of Novel Microwave Cooking Model For Not-Ready-To Eat Foods, Sohan Birla, Krishnamoorthy Pitchai, Jeyamkondan Subbiah, David D. Jones

Department of Biological Systems Engineering: Conference Presentations and White Papers

Recently safety of microwave cooked food has come under scrutiny because of recent outbreak and recalls associated with some of these not-ready-to-eat (NRTE) frozen foods. Heating uniformity of these foods is paramount in rendering the foods safe for consumption. Degree of uneven microwave heating is influenced by both microwave oven and characteristics of food load which decides the electric field distribution within the food load. Given the complexity of parameters, a computer model is always desirable to optimize heating uniformity by proper selection of food shape, proportions, plating, packaging selection and more. Earlier many researchers have made one or more …

The Thermal Model Of The Rat Under Hemorrhagic Shock Hypothermia With Microwave Intervention, Liu Zhe

Theses

A whole body thermal model simulating heat distribution and temperature regulation in rats during hemorrhagic shock and during post-shock microwave core rewarming period was developed. An electrical circuit was used to simulate the thermal system and a software named PSpice? was used to analyze the circuit. The temperature regulation as the result of the simulation is demonstrated to match the measured temperature histories of rats in hemorrhagic shock and the microwave rewarming experiment.

The blood pressure drop and cardiac output decrease were considered in the simulation and the so called "set point temperature" was investigated in the model. Linear decrease …