Engineering Commons^™

Fabrication And Testing Of Catalyst-Infused Filament For 3d Printing Of Ignition-Augmented Hybrid Rocket Fuels, Kurt C. Olsen

All Graduate Theses and Dissertations, Spring 1920 to Summer 2023

This thesis describes and addresses the need for reliable ignition in small satellite hybrid propulsion systems using higher density oxidizers. It describes methods of creating custom 3D printing ABS plastic based filaments that contain small amounts of catalysts. These catalysts lead to a more reliable and energy-efficient ignition of a hybrid rocked propulsion system using catalyst-infused ABS and nitrous oxide and oxygen blend called Nytrox, commonly known as ”laughing gas.” The ”laughing gas” has a higher density and can therefore provide more ”miles per gallon” in a hybrid propulsion system on a small satellite when compared to gaseous oxygen (GOX). …

Out-Of-Plane Load-Bearing And Mechanical Energy Absorption Properties Of Flexible Density-Graded Tpu Honeycombs, Ibnaj Anamika Anni, Kazi Zahir Uddin, Nicholas Pagliocca, Nand Singh, Oyindamola Rahman, George Youssef, Behrad Koohbor

Henry M. Rowan College of Engineering Faculty Scholarship

Honeycomb structures are widely used in applications that require excellent strain energy mitigation at low structural weights. The load-bearing and energy absorption capacity of honeycomb structures strongly depend on their cell wall thickness to edge ratios. This work studies the mechanical response and strain energy absorption characteristics of hexagonal honeycomb structures with various cell wall thicknesses in response to out-of-plane loading conditions. Honeycomb structures with various nominal densities are first additively manufactured from flexible thermoplastic polyurethane (TPU). A comprehensive experimental study characterized the mechanical strength, energy absorption performance, and the strain recoverability of the structures. Density-graded structures are then fabricated …

Additive Manufacturing Of Aluminum Alloy By Metal Fused Filament Fabrication (Mf3)., Luke J. Malone

Electronic Theses and Dissertations

This research studies metal-fused filament fabrication (MF3) for manufacturing aluminum alloy parts. An aluminum alloy powder-based feedstock with a polymer-binder system was extruded via capillary rheometry to form a filament. The filament was used to print green parts that were involved in a two-step debinding process combining solvent and thermal extraction of the polymer binder, then sintered in a partial vacuum. Resulting grain structure, sintered density, and mechanical properties will be characterized and compared to metal injection molded (MIM) specimens. The main objective is to gain an understanding of the MF3 process characteristics and the ensuing material properties and microstructure …

Flow In Additively Manufactured Super-Rough Channels, Samuel Altland, Xiaowei Zhu, Stephen Mcclain, Robert Kunz, Xiang Yang

Mechanical and Materials Engineering Faculty Publications and Presentations

Metal additive manufacturing has enabled geometrically complex internal cooling channels for turbine and heat exchanger applications, but the process gives rise to large-scale roughness whose size is comparable to the channel height (which is 500 μm). These super-rough channels pose previously unseen challenges for experimental measurements, data interpretation and roughness modelling. First, it is not clear if measurements at a particular streamwise and spanwise location still provide accurate representation of the mean (time- and plane-averaged) flow. Second, we do not know if the logarithmic layer survives. Third, it is unknown how well previously developed rough-wall models work for these large-scale …

Influence Of Aluminum Addition On The Laser Powder Bed Fusion Of Copper-Aluminum Mixtures, Nada Kraiem, Loic Constantin, A. Mao, Fei Wang, Bai Cui, Jean-François Silvain, Yongfeng Lu

Department of Electrical and Computer Engineering: Faculty Publications

The high optical reflectivity of copper (Cu) in the near infrared (NIR) domain and its elevated heat dissipation make Cu a challenging metal for laser powder bed fusion (LPBF), even with high energy densities (EDs). In this study, we demonstrated that adding aluminum (Al) powder by as little as 0.75, 1.5, and 3 wt.% substantially enhances Cu processability, leading to denser (up to 98%) and smoother (Ra = 3.3 𝜇m) Cu-Al parts as compared to 95% and 18 𝜇m, respectively, for the parts printed using pure Cu. In addition, this method reduces the ED required by a factor of two …

In-Situ Infrared Thermographic Inspection For Local Powder Layer Thickness Measurement In Laser Powder Bed Fusion, Tao Liu, Cody S. Lough, Hossein Sehhat, Yi Ming Ren, Panagiotis D. Christofides, Edward C. Kinzel, Ming-Chuan Leu

Mechanical and Aerospace Engineering Faculty Research & Creative Works

The laser powder bed fusion (LPBF) process is strongly influenced by the characteristics of the powder layer, including its thickness and thermal transport properties. This paper investigates in-situ characterization of the powder layer using thermographic inspection. A thermal camera monitors the temperature history of the powder surface immediately after a layer of new powder is deposited by the recoating system. During this process, thermal energy diffuses from the underlying solid part, eventually raising the temperature of the above powder layer. Guided by 1D modeling of this heat-up process, experiments show how the parameterized thermal history can be correlated with powder …

Experimental Characterization Of Additively Manufactured Multi-Feather Wingtip Devices, Patricio Garzon

Doctoral Dissertations and Master's Theses

Soaring birds have evolved to fly for long periods of time without flapping their wings. Inspired by the flight of these birds, the proposed thesis presents an experimental investigation focused on wingtip devices designed based on biomimicry. The overarching engineering objective was to reduce the induced drag as a means to improve the fuel efficiency via these experimental wingtips. An associated secondary objective was to establish a method for manufacturing complex structures suitable for wing tunnel testing. A manufacturing technique that involved using composite weaves to reinforce additively manufactured structures was developed. This technique has the potential to reduce manufacturing …

Additive Manufacturing Of Sub-Micron Features And Mechanical Linkages, David K. Limberg

Doctoral Dissertations

In recent years material constraints have become the limiting factor in several fields, including batteries, robotics, and medicine, and these needs have prompted the development of materials with programmable properties. To this end, much effort has been dedicated to designing metamaterials that have unprecedented optical, mechanical, and thermal properties, along with systems for additive manufacturing to build their complex structures with high precision and throughput. The field of additive manufacturing has proved to be a platform for innovation across many industries yet is still limited with regards to feature sizes, print rates, and diversity of materials. Mechanical devices like linkages …

Controlled Pre-Wetting Of Spread Powder And Its Effects On Part Formation And Printing Parameters In Binder Jetting Additive Manufacturing, Colton G. Inkley

Theses and Dissertations

Binder jetting is an additive manufacturing process that layer by layer builds a 3D model by selectively binding regions of powder using binder deposited though an inkjet printhead. The process offers several advantages over other additive manufacturing processes including fast build rates, vast material selection, decreased cost, and part resolution. The main disadvantage of binder jetting is poor mechanical properties, stemming from a poor understanding of the process physics. Porosity in final parts is not uncommon, but there is little understanding of where the porosity originates. The purpose of this thesis is to report the investigation of increased powder bed …

Effect Of Additively Manufactured Padding On The Mechanical And Thermal Comfort Of Mtb-Backpacks, Frank I. Michel, Stefanie Zelt, Dominik Krumm, Andreas Knöchel, Stefan Schwanitz

International Sports Engineering Association – Engineering of Sport

No abstract provided.

Tini-Based Bi-Metallic Shape-Memory Alloy By Laser-Directed Energy Deposition, Yitao Chen, Cesar Ortiz Rios, Braden Mclain, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In this study, laser-directed energy deposition was applied to build a Ti-rich ternary Ti–Ni–Cu shape-memory alloy onto a TiNi shape-memory alloy substrate to realize the joining of the multifunctional bi-metallic shape-memory alloy structure. The cost-effective Ti, Ni, and Cu elemental powder blend was used for raw materials. Various material characterization approaches were applied to reveal different material properties in two sections. The as-fabricated Ti–Ni–Cu alloy microstructure has the TiNi phase as the matrix with Ti2Ni secondary precipitates. The hardness shows no high values indicating that the major phase is not hard intermetallic. A bonding strength of 569.1 MPa was obtained …

Performance Study Of Post-Processed Additively Manufactured Low Thrust Nozzles, Tyler W. Gerhold

Theses and Dissertations

This research explores metal post-processing techniques to effectively reduce the large anomalous protrusions found in small additively manufactured low thrust rocket nozzles. Research has found that nozzles of this kind can experience losses in thrust of over 40%. Analytic theory of adiabatic nozzle flow with viscous losses for additively manufactured nozzles does not align with what has been found when tested experimentally. Compressible flow losses, such as shock wave formation inside the nozzle diverging cone, are likely the leading causes of such loss. Reduction in nozzle irregularities can likely yield results seen in analytic theory with similar performance to traditional …

On The Effects Of Additive Manufacturing Process Parameters On The Performance Of Hastelloy-X: A Neutron Diffraction Experiment And Crystal Plasticity Finite Element Model, Ahmed Aburakhia

Electronic Thesis and Dissertation Repository

Additive manufacturing (AM) is increasingly becoming one of the favourable manufacturing techniques in various industries, such as transportation and energy. The reason for the extensive use of AM lies in the ability to use a wide range of process parameters for manufacturing engineering parts with complex geometries that cannot be effectively manufactured using traditional methods such as casting or forging. Understanding the role of process parameters is crucial for developing predictive models, as well as for manufacturing engineering components with the desired properties.

This research aims to characterize the influence of AM process parameters on the deformation mechanisms of Hastelloy-X, …

Multi-Material 3d-Printed Silicone Vocal Fold Models, Clayton Adam Young

Theses and Dissertations

Self-oscillating synthetic vocal fold (VF) models are often used to study human voice production. In this thesis, a method for fabricating multi-layer self-oscillating synthetic VF models using silicone 3D printing is presented. Multi-material 3D printing enables faster fabrication times with more complex geometries than traditional casting methods and builds a foundation for producing VF models with potentially more life-like geometries, materials, and vibratory characteristics. The printing method in this study used a custom dual extruder and slicing software to print UV-curable liquid silicone into a gel-like support matrix. The extruder was fabricated using high-torque stepper motors with high resolution leadscrews …

Particle Formation And Thermal Radiation In Laminar Diffusion Flames With Applications To Energy And Materials, Phillip Irace

McKelvey School of Engineering Theses & Dissertations

Fossil fuels supply over 80% of the world’s primary energy, and if current policy and technology trends continue, global energy and energy-related carbon dioxide (CO2) emissions are predicted to increase for at least several decades owing to population and economic growth, leading to serious concerns regarding global warming. Natural gas releases less CO2 than other fossil fuels (e.g., coal and oil) and can help meet future CO2 emission targets. Natural gas combustion, however, has poor radiation heat transfer when compared to other fossil fuels owing to its low propensity for soot formation, making it difficult to use as a drop-in …

Additive Manufacturing Of Variable Contrast Computed Tomography Anatomical Phantoms Using A Single Feedstock In Fused Filament Fabrication, Cory J. Darling

University of New Orleans Theses and Dissertations

Anatomical phantoms used in biomedical education and training benefit greatly from Fused filament fabrication’s (FFF) ability to rapidly produce complex and unique models. Current materials and methods used in FFF have limited ability to accurately produce phantoms that can mimic the radiological properties of multiple biological tissues. This research demonstrates that the CT contrast of FFF produced models can be modified by varying the concentration of bismuth oxide in acrylonitrile butadiene styrene (ABS) filaments and a tunable CT contrast that mimics the CT contrast ranging from fatty tissue to cortical bone using a single composite filament without introducing artificial image …

Single Asperity Fretting Corrosion Of Traditional And Additively Manufactured Metallic Biomaterials: Quantitative Analysis From Acetabular Tapers To Micron And Nanometer Scale Tribocorrosion, Annsley Mace

All Dissertations

Mechanically assisted crevice corrosion (MACC) of metallic biomaterials continues to be a significant degradation mode. This is, in part, due to a lack of understanding of fundamental micron- and sub-micron scale mechanisms of metal degradation in biological environments. Metal-metal (or metal-hard) load bearing surfaces of hip arthroplasties are subjected to fretting crevice corrosion (FCC, one form of MACC). Current work in tribocorrosion involves large contact area tests with multiple asperities, with a distribution of load and wear that changes over time. A more systematic and controlled study of the FCC micro- and nanomechanics is needed.

Therefore, the goal of this …

Effects Of Sizing Agents On Mechanical Properties Of Carbon Fiber–Polymer Composites Via Fused Filament Fabrication Additive Manufacturing., Benjamin D. Mitchell

Electronic Theses and Dissertations

This study demonstrated the effects of changing the sizing agent parameter during the preparation of carbon fibers on the mechanical properties of composite made with acrylonitrile butadiene styrene (ABS) as the matrix material and carbon fibers as the fiber material. Three types of sizing agents produced by Allnex were used to coat three different batches of carbon fibers that were mixed with a torque rheometer and extruded with a barrel-style melt extruder into continuous spools of 1.75 mm filament for use with commercial 3D printers. Tensile tests were conducted on the filaments and tensile bars printed from the materials. Results …

Autonomous Material Refill For Swarm 3d Printing, William C. Jones

Mechanical Engineering Undergraduate Honors Theses

3D printing currently offers robust and cheap rapid prototyping solutions. While standard 3D printing remains at the periphery of mass production, the technology serves as a starting point for the development of swarm manufacturing. Since swarm manufacturing is predicated upon autonomy, swarm technology companies such as AMBOTS are seeking to minimize human involvement in the swarm’s functions. At present, the 3D printing swarm consists of the printers, a transporter which can take them between job sites, and the floor tiles which provide power and support the build surfaces. To add to this ecosystem, this project is focused on the design …

Additive Manufacturing Of Sensors For Extreme Environments, Kiyo Tiffany Fujimoto

Boise State University Theses and Dissertations

Advanced manufacturing based direct-write technologies have emerged as the predominant enabler for the fabrication of active and passive sensors for use in harsh operating environments. The ability to directly write and integrate electronic components onto physical packaging can be achieved with additive manufacturing (AM) methods such as direct write technologies (DWT) which include aerosol jet printing (AJP), Ink Jet Printing (IJP), Plasma Jet Printing (PJP), and Micro-Dispense Printing (MDP). In this work, we investigate the use of these methods to accelerate, modernize, and enhance the functionality of sensors and instrumentation to achieve the goal of improving the safety and efficiency …

Multistage Modeling Of Fatigue Of Ti-6al-4v Fabricated By Different Additive Manufacturing Techniques, Lionardo Lado, Saeed Ataollahi, Mohammad J. Mahtabi

Honors Theses

Thanks to its high strength-to-weight ratio and corrosion resistance, Ti-6Al-4V has gained a lot of attention in additive manufacturing (AM) of complex parts with aerospace and medical applications. The realistic loading condition in these applications is mostly cyclic. However, the main challenge with AM of this alloy - and in general AM of metallic parts - is fatigue resistance and durability of the part, which has been reported to be much lower than the conventional materials. In this study, fatigue life performance of three additive manufacturing methods was compared using the Multistage Fatigue model (MSF). MSF model predicts the fatigue …

Effects Of Fiber Orientation On The Coefficient Of Thermal Expansion Of Fiber-Filled Polymer Systems In Large Format Polymer Extrusion-Based Additive Manufacturing, José Luis Colón Quintana, Lucinda Slattery, Jon Pinkham, Joanna Keaton, Roberto A. Lopez-Anido, Keith Sharp

Civil Engineering Faculty Scholarship

Large format polymer extrusion-based additive manufacturing has been studied recently due to its capacity for high throughput, customizable bead size and geometry, and ability to manufacture large parts. Samples from three fiber-filled amorphous thermoplastic materials 3D printed using a Masterprint 3X machine from Ingersoll Machine Tools were studied, along with their neat counterparts. Characterization techniques included thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and thermo-mechanical analysis (TMA). TGA results showed that the fillers decreased the degradation temperature for most of the materials investigated, with a 30°C decrease for polycarbonate (PC) and a 12°C decrease for polyethylene terephthalate glycol (PETG). For …

Optical Observation Of Large Area Projection Sintering, Derek Black

Theses and Dissertations

Polymer powder bed fusion (PBF/P) is one of many additive manufacturing (AM) processes utilized for producing polymer parts from digital 3D models. AM is preferred over traditional manufacturing methods in many applications due to advantages including tool-less manufacturing, high geometric complexity, short lead times, and reduced material waste. However, many industries that stand to benefit the most from AM are limited in their ability to use AM parts in large part due to low confidence in AM part quality. Among the polymer AM processes, PBF/P processes show significant promise for these applications due to their comparatively high isotropy and mechanical …

Effects Of Varied Oxygen Levels, Laser Powers, And Scanning Speeds On Manufactured Components By Laser-Based Powder Bed Fusion, Amelia Mcnamee

Honors College Theses

This project addresses the effects of oxygen concentration, laser power, and scanning speed on the melt pool geometry of laser-based powder bed fusion (L-PBF) additively manufactured components. A parametric analysis using the substrate alone was conducted to determine a range of desirable laser powers and scanning speeds. The parameter with the more significant effect will be decided upon based on the depth-to-width ratios (D/W) of the resultant laser weld bead. A range of oxygen levels and scan speeds was selected for the next phase. These samples were then be analyzed for depth-to-width ratios. It was expected that higher oxygen concentrations …

Development Of The Uhpc Mix For 3d Printing, Buse Ilayda Oz

FIU Electronic Theses and Dissertations

This thesis utilizes the development of Ultra-High-Performance Concrete mix design for 3-Dimensional (3D) Printing purposes. 3D concrete printing offers many advantages such as the improvements in safety, quality, and productivity. Moreover, it holds a great advantage for the construction of structural elements that are difficult to construct by conventional methods. These advantages carry a huge potential for solving the aforementioned challenges.

Seven UHPC mixes have been designed and analyzed using various test setups for comparison purposes. Extrudability, flowability, buildability, and open time were measured using the fresh properties of the UHPC mixes. Mechanical properties were measured using compression test setups. …

Elimination Of Extraordinarily High Cracking Susceptibility Of Aluminum Alloy Fabricated By Laser Powder Bed Fusion, Holden Hyer, Le Zhou, Sharon Park, Thinh Huynh, Abhishek Mehta, Saket Thapliyal, Rajiv S. Mishra, Yongho Sohn

Mechanical Engineering Faculty Research and Publications

Using the calculation of phase diagrams approach and Scheil solidification modeling, the Al-2.5Mg-1.0Ni-0.4Sc-0.1Zr alloy was designed, intentionally with an extraordinarily high cracking susceptibility, making it prime for solidification cracking during laser powder bed fusion. This study demonstrates the ability to mitigate even the most extreme solidification cracking tendencies in aluminum alloys with only minor alloying additions of Sc and Zr, 0.5 wt.% max. Furthermore, by employing a simple direct ageing heat treatment, good tensile mechanical properties were observed with a yield strength of 308 MPa, an ultimate tensile strength of 390 MPa, and a total elongation of 11%.

Cost-Effective Non-Destructive Testing Of Biomedical Components Fabricated Using Additive Manufacturing, Santiago Fabian Cobos

Electronic Thesis and Dissertation Repository

Biocompatible titanium-alloys can be used to fabricate patient-specific medical components using additive manufacturing (AM). These novel components have the potential to improve clinical outcomes in various medical scenarios. However, AM introduces stability and repeatability concerns, which are potential roadblocks for its widespread use in the medical sector. Micro-CT imaging for non-destructive testing (NDT) is an effective solution for post-manufacturing quality control of these components. Unfortunately, current micro-CT NDT scanners require expensive infrastructure and hardware, which translates into prohibitively expensive routine NDT. Furthermore, the limited dynamic-range of these scanners can cause severe image artifacts that may compromise the diagnostic value of …

Critical Evaluation Of Construction Industry-Related Additive Manufacturing Research: A Scientometric Analysis, Tyler J. Brunjes

Theses and Dissertations

Review of construction-related AM literature is used to identify the advantages, challenges, and current trends of the research. Using a scientometric analysis of 522 bibliographic records, this research systematically analyzed construction related AM research to determine the key research areas and trends. Results showed that starting in 2015, the field has been growing at an exponential rate. Recent AM research focused on materials and reinforcement topics, which matched the most notable challenges of AM, which are material rheology, reinforcement, and lacking construction standards. This study provides an insight into AM research and identifies areas requiring more innovation before its commercial …

Formulation And Processing Of Dual Functional Adsorbent/Catalyst Structured Monoliths Using An Additively Manufactured Contactor For Direct Capture/Conversion Of Co2 With Cogeneration Of Ethylene, Shane Lawson, Khaled Baamran, Kyle Newport, Fateme Rezaei, Ali A. Rownaghi

Chemical and Biochemical Engineering Faculty Research & Creative Works

Utilizing CO₂ as a mild oxidant for oxidative dehydrogenation of ethane (ODHE) is an attractive way of recycling this greenhouse contaminant. Typically, CO₂ capture and conversion processes are performed in separate beds, however, combining these processes into one bed incurs advantages of lower thermal gradient and reduced energy costs. This study formulated the first generation of structured dual-functional materials (DFMs) by directly 3D printing metal-oxide-CaO/ZSM-5 inks into monolithic contactors. Specifically, we 3D-printed monoliths with V, Ga, Ni, or Ti dopants to perform metal screening and determine which metal generates the best structured DFM for combined CO₂ capture …

Investigation Of Additively Manufactured Molybdenum-Tungsten-Rhenium Alloys, Randolph T. Abaya

Theses and Dissertations

The process of creating metal components through additive manufacturing is changing the way different industries can avoid the shortcomings of traditional metal production. Metals such as tungsten, molybdenum, and rhenium have many advantages for different applications, especially when alloyed together. In this study, an additively manufactured alloy containing 70% molybdenum, 25% tungsten, and 5% rhenium (70Mo-25W-5Re) is tested for its strength, ductility, hardness, and porosity. The 70Mo-25W-5Re alloy is printed through Laser Powder Bed Fusion (LPBF) under different conditions such as printing speed and printing atmosphere. Additionally, the effects of post printing heat treatment are conducted to understand the advantages …